Xylose preparation method
A xylose and equipment technology, applied in the field of xylose preparation, can solve the problems of large sewage discharge, high steam consumption, large water consumption, etc. Effect
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Embodiment 1
[0026] (1) Corn cob hydrolysis
[0027] Take corncobs, add sulfuric acid solution with a mass concentration of 2.5%, heat at 135°C for 3 hours, and obtain xylose liquid. The dry matter content in the xylose liquid is 7% by mass, and the light transmittance is 3.2%.
[0028] (2) One decolorization
[0029] Add activated carbon according to 4% of the dry matter mass in the xylose solution, keep it warm at 86°C for 20 minutes, filter and remove the activated carbon, and obtain a xylose primary decolorization solution with a light transmittance of 65%.
[0030] (3) Protection filter
[0031] Filter the xylose primary decolorization solution through a gauze bag to remove solid impurities and protect the electrodialysis membrane.
[0032] (4) Membrane ultrafiltration
[0033] After protecting and filtering the xylose liquid, use the acid-resistant roll-type membrane ultrafiltration with a membrane pore size of 5000 to remove the colloidal impurities that cannot be removed by acti...
Embodiment 2
[0041] (1) Corn cob hydrolysis
[0042] Take corncobs, add sulfuric acid solution with a mass concentration of 1.7%, heat at 115°C for 2.5 hours, and obtain xylose liquid. 7% of the dry matter mass in the liquid was added with activated carbon, kept at 70°C for 33 minutes, and filtered to remove the activated carbon to obtain a xylose primary decolorization liquid with a light transmittance of 75%.
[0043] (2) Electrodialysis desalination
[0044] A homogeneous electrodialysis membrane is used to filter the xylose primary decolorization solution to remove sulfuric acid, salts and other electrolytes, and the conductivity of the xylose solution is reduced to 605 μs / cm.
[0045] (3) Membrane concentration
[0046] The xylose liquid after desalination by electrodialysis is concentrated by the material reverse osmosis membrane, and the mass percentage of dry matter in the concentrated xylose liquid is 18.3%.
[0047] (4) Concentration, decolorization, ion exchange, concentration,...
Embodiment 3
[0050] (1) Steam Explosion Corn Stalks
[0051] Crush 500g of corn stalks into small pieces of about 1cm square, add 8000ml of 1.1% hydrochloric acid solution by weight, soak at room temperature for 17 hours, and separate the solid and liquid to obtain the acidified corn stalks. Put the acidified corn stalks into the steam explosion equipment During the process, the steam was boosted to 1.1Mpa, and the pressure was maintained for 4.5min. The steam-exploded corn stalk mud obtained was washed with hot water for many times, and the washing liquid was combined to obtain the xylose liquid. The dry matter mass percentage was 4.1%.
[0052] (2) One decolorization
[0053] Add activated carbon according to 10% of the dry matter mass in the xylose solution, keep it warm at 50°C for 10 minutes, filter and remove the activated carbon, and obtain a xylose primary decolorization solution with a light transmittance of 72%.
[0054] (3) Membrane ultrafiltration
[0055] Utilize the ac...
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