Method for preparing hyperdispersant by adopting oxidized graphene and application thereof
A hyperdispersant and graphene technology, applied in chemical instruments and methods, dyeing low-molecular organic compound treatment, inorganic pigment treatment, etc., to achieve the effects of high finish, improved mechanical properties, and improved dispersion performance
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Embodiment 1
[0016] The main raw materials for preparing hyperdispersant in this example: graphene oxide (self-made), ethylene triamine (industrial grade), stearic acid (industrial grade), sodium hydroxide (industrial grade), hydrochloric acid (industrial grade), p-toluenesulfonic acid (technical grade), toluene (technical grade).
[0017] The concrete steps that adopt graphene oxide to prepare hyperdispersant are:
[0018] (1) Add 3 grams of graphene oxide into a 500 ml three-necked flask, then add 250 grams of distilled water to start the vibration, and vibrate for 30 minutes in a 2000 Hz ultrasonic environment to form a uniformly dispersed graphene oxide mixture, and then add 10 grams of ethylene glycol Triamine and 8 grams of sodium hydroxide, and adjust the pH value to 7 with hydrochloric acid, continue ultrasonic dispersion for 3 hours at 90°C, cool to room temperature after the reaction, add water to precipitate, filter under reduced pressure, and wash the product with absolute etha...
Embodiment 2
[0024] The main raw materials for the preparation of hyperdispersants in this example: graphene oxide (self-made), ethylene triamine (industrial grade), stearic acid (industrial grade), sodium hydroxide (industrial grade), hydrochloric acid (industrial grade), p-toluenesulfonic acid (technical grade), toluene (technical grade).
[0025] The concrete steps that adopt graphene oxide to prepare hyperdispersant are:
[0026] (1) Add 6 grams of graphene oxide into a 500 ml three-necked flask, then add 300 grams of distilled water to start the vibration, and vibrate for 30 minutes in a 2000 Hz ultrasonic environment to form a uniformly dispersed graphene oxide mixture, and then add 16 grams of ethylene glycol Triamine and 8 grams of sodium hydroxide, adjust the pH value to 7 with hydrochloric acid, continue ultrasonic dispersion for 4 hours at 85°C, cool to room temperature after the reaction, add water to precipitate, filter under reduced pressure, and wash the product with absolut...
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