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Method utilizing calcium carbide slag as raw material to produce gypsum crystal whisker

A technology of gypsum whiskers and carbide slag, which is applied in the field of comprehensive utilization of solid waste, can solve the problems of complex reaction steps, high production cost, and long production cycle, and achieve the effect of cheap raw materials, low cost, and large operating flexibility

Inactive Publication Date: 2014-03-26
CHINA UNIV OF GEOSCIENCES (WUHAN)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0019] The above patents proposed different methods to prepare gypsum whiskers, basically using gypsum or other chemical reagents as raw materials, high production cost, complicated reaction steps, long production cycle and other defects

Method used

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  • Method utilizing calcium carbide slag as raw material to produce gypsum crystal whisker

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0045] A kind of method that is raw material production gypsum whisker with carbide slag, it comprises the steps:

[0046] (1) Dry carbide slag at 120°C for 3 hours, then ball mill for 10 minutes, and then calcined at 900°C for 1 hour;

[0047] (2) Mix the calcined calcium carbide slag with dilute sulfuric acid (the mass fraction of sulfuric acid is 50%) in a ratio of 1:3 by volume, stir evenly, and then react for 5 hours at a water bath temperature of 80°C. During the reaction process Magnetic stirring at a stirring speed of 1000 rpm; the reacted product was washed with water until the pH value was equal to 7, and then centrifuged (2000 rpm, 30 minutes) to obtain a solid product;

[0048] (3) Mix the solid obtained in the above step (2) with water, control the slurry concentration to 1% (mass ratio), add ethylene glycol (the mass is 0.5% of the solid mass in the slurry), and then transfer to hydrothermal Hydrothermal reaction at 110°C in the reactor for 10 hours; wash the pr...

Embodiment 2

[0051] A kind of method that is raw material production gypsum whisker with carbide slag, it comprises the steps:

[0052] (1) Dry carbide slag at 70°C for 10 hours, then ball mill for 15 minutes, and then calcined at 500°C for 5 hours;

[0053] (2) Mix calcined calcium carbide slag and dilute sulfuric acid (25% sulfuric acid mass fraction) in a volume ratio of 1:5, stir evenly, and then react for 30 hours at a water bath temperature of 30°C. During the reaction Magnetic stirring at a stirring speed of 200 rpm; the reacted product was washed with water until the pH value was equal to 7, then centrifuged (4000 rpm, 5 minutes), and dried (60°C, 12 hours);

[0054] (3) Mix the solid obtained in the above step (2) with water, control the slurry concentration to 10% (mass ratio), add ethylene glycol (the mass is 3% of the solid mass in the slurry), and then transfer to hydrothermal Hydrothermal reaction at 180°C for 4 hours in the reactor; wash the product after the hydrothermal r...

Embodiment 3

[0057] A kind of method that is raw material production gypsum whisker with carbide slag, it comprises the steps:

[0058] (1) Dry carbide slag at 80°C for 5 hours, then ball mill for 5 minutes, and then calcined at 700°C for 3 hours;

[0059] (2) Mix the calcined calcium carbide slag with dilute sulfuric acid (35% sulfuric acid mass fraction) in a ratio of 1:1 by volume, stir evenly, and then react at a water bath temperature of 50°C for 10 hours. During the reaction Magnetic stirring at a stirring speed of 3000 rpm; the reacted product was washed with water until the pH value was equal to 7, then centrifuged (3000 rpm, 10 minutes) and dried (120°C, 5 hours);

[0060] (3) Mix the solid obtained in the above step (2) with water, control the slurry concentration to 5% (mass ratio), add ethylene glycol (the mass is 1% of the solid mass in the slurry), and then transfer to hydrothermal Hydrothermal reaction at 150°C for 5 hours in the reactor; wash the product after the hydrothe...

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Abstract

The invention relates to a method utilizing calcium carbide slag as a raw material to produce a gypsum crystal whisker, and belongs to the field of inorganic material preparation and solid waste comprehensive utilization. The method utilizing calcium carbide slag as the raw material to produce the gypsum crystal whisker is characterized by comprising the following steps: (1) drying, ball milling and calcining the calcium carbide slag; (2) enabling the obtained calcium carbide slag to react with dilute sulfuric acid after the calcining treatment step, and washing and centrifuging the precipitation product; (3) mixing the solid obtained in the step (2) with water to prepare size, adding a crystal aid with a certain mass fraction in the size, transferring the mixed solution in a hydrothermal reaction kettle to carry out hydrothermal reaction, and washing, centrifuging and drying the product after the hydrothermal reaction to obtain the gypsum crystal whisker product prepared by taking the calcium carbide as the raw material. The method is mild in reaction conditions, simple in process, flexible in operation, and easy for industrial production. The prepared gypsum crystal whisker is large in draw ratio and good in reinforcing performance.

Description

technical field [0001] The invention relates to a method for producing gypsum whiskers by using calcium carbide slag as a raw material, belonging to the fields of inorganic material preparation and solid waste comprehensive utilization. Background technique [0002] Carbide slag is calcium carbide (CaC) in industrial production of acetylene, polyvinyl chloride (PVC), polyvinyl alcohol (PVI), etc. 2 ) [0003] Industrial waste formed by hydrolysis. The main component of carbide slag is Ca(OH) 2 , in addition to containing Fe 2 o 3 , SiO 2 , MgO, Al 2 o 3 [0004] Such as metal oxides, hydroxides and a small amount of organic matter. The moisture content of calcium carbide slag is very high when it is just discharged, reaching 85%~ [0005] 90%, after the ash dam is deposited and accumulated, the moisture can be reduced to less than 50%, and it will be off-white after drying, with fine and uniform particles. [0006] Small specific gravity and loose structure. Sinc...

Claims

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Application Information

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IPC IPC(8): C30B7/10C30B29/62C30B29/46
Inventor 王永钱原骜雷殿俊原博李印昌马群雷新荣张锡军
Owner CHINA UNIV OF GEOSCIENCES (WUHAN)
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