A method for preparing amorphous thin strip by single-roll rapid quenching with concave rotary table
A single-roller quick quenching and turntable technology, applied in the field of amorphous thin strip preparation, can solve the problems of difficult strip formation, rapid-setting thin strip melt droplet splashing, bubbles, etc., and achieve the effect of fast cooling speed
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Embodiment 1
[0050] A method for preparing a fast-quenched amorphous alloy thin strip, including batching, smelting, secondary smelting, strip spraying, and harvesting. The mass percentage of its chemical composition is: 21.57%Sm, 72.84%Fe, 1.66%Zr, 3.93%Co.
[0051] Using 99.5% metal samarium, industrial pure iron, metal cobalt, and metal zirconium as raw materials, it is melted in an intermediate frequency vacuum induction melting furnace. Before melting, the vacuum chamber is first vacuumed, and then high-purity argon is used as a protective gas to avoid alloy oxidation. . The melting temperature is 1600°C. Secondary melting is carried out in the induction ladle, and the spray belt pressure is established in the nozzle package, and the spray belt pressure is 0.05Mpa. The protective atmosphere pressure is 0.01Mpa.
[0052] Molybdenum is used to prepare concave disc rollers, and the interior of the concave disc rollers is cooled by circulating water. The diameter of the inner port of t...
Embodiment 2
[0060] In this example, the Sm 1.0 Zr 0.3 Fe 8.1 co 0.6 Rapidly quenched thin strip, the difference is that the angle between the conical slope surface and the central axis is 70°, and other parameters are as in Example 1.
[0061] Obtain Sm with a thickness of 13-14 microns and a surface roughness of less than 0.33 microns 1.0 Zr 0.3 Fe 8.1 co 0.6 Fast-setting thin strips, no splashing phenomenon in the process of throwing the strips, no α-Fe soft magnetic phase in the alloy, and Sm 1.0 Zr 0.3 Fe 8.1 co 0.6 N x , after being made into a bonded magnet, the magnetic property is B r =1.02T, (BH) max =22.5MGOe. Compared with the tape obtained when the angle between the conical slope surface and the central axis is 60°, the strip is slightly thicker and the uniformity is slightly worse. Choosing a suitable slope angle is the basis for obtaining a good strip.
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