Insulation packaging material of high capacity film capacitor
A technology for packaging materials and film capacitors, applied in the field of packaging materials, can solve problems such as high thermal conductivity and low stress, and achieve the effects of improving thermal conductivity, reducing thermal stability, and good thermal shock resistance.
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[0028] Example 1
[0029] (1) First, prepare flexible polyurethane: After removing water from polyethylene glycol 400, add TDI to the reaction kettle, pass nitrogen protection, and react at 60°C for 7 hours until the viscosity no longer increases. Cool down to 30°C and filter out. , To obtain self-made hydroxy-terminated flexible polyurethane;
[0030] (2) Preparation of component A: epoxy resin (bisphenol A epoxy resin E-51 accounts for 75%, alicyclic epoxy resin ERL-4221 accounts for 25%), self-made flexible polyurethane, needle-like silica fume Stone powder and antifoaming agent BYK-A530 are mixed according to mass percentage, added to the reactor, heated to 90°C and stirred for 90 minutes, cooled to 60°C, filtered and discharged to obtain component A;
[0031] (3) Preparation of component B: Methyltetrahydrophthalic anhydride, self-made flexible polyurethane, needle-like wollastonite powder, modified imidazole, BYK-430, 2,6-di-tert-butyl-4-methylphenol according to the quality ...
Example Embodiment
[0033] Example 2
[0034] (1) First, prepare flexible polyurethane: After removing water from polytetrahydrofuran ether glycol 250, add IPDI to the reaction kettle, pass nitrogen protection, and react at 65°C for 6 hours until the viscosity no longer increases. Cool down to 35°C and filter out To obtain self-made hydroxy-terminated flexible polyurethane;
[0035] (2) Preparation of component A: mix bisphenol A epoxy resin E-51, self-made flexible polyurethane, silicon micropowder, and defoamer BYK-A530 according to mass percentages, add them to the reactor, heat up to 90°C and stir for 100 minutes, Cool to 55°C, filter and discharge to obtain component A;
[0036] (3) Preparation of component B: the mixture of methylhexahydrophthalic anhydride and polyazelaic anhydride, self-made flexible polyurethane, silicon powder, DMP-30, BYK-430, tetrakis(4-hydroxy-3,5-tert-butyl (Phenylpropionic acid) pentaerythritol ester is mixed according to the mass percentage, added to the high-speed dis...
Example Embodiment
[0038] Example 3
[0039] (1) First, prepare flexible polyurethane: After removing water from polyethylene glycol 400, add HDI to the reaction kettle, pass nitrogen protection, react at 70°C for 4 hours until the viscosity no longer increases, cool to 40°C, and filter out. , To obtain self-made hydroxy-terminated flexible polyurethane;
[0040] (2) Preparation of component A: mix the alicyclic epoxy resin ERL-4221, self-made flexible polyurethane, alumina, and defoamer BYK-354 according to the mass percentage, add them to the reactor, heat up to 80℃ and stir for 120min, Cool to 50°C, filter and discharge to obtain component A;
[0041] (3) Preparation of component B: mix methyltetrahydrophthalic anhydride, self-made flexible polyurethane, silicon powder, modified imidazole, BYK-W995, and phenothiazine according to the mass percentage, add them to the high-speed dispersing kettle, and heat to 50°C for stirring 110min, filter out the material to obtain component B;
[0042] Mix compon...
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