Preparation method for magnetic nanoparticles coated with highly ordered mesoporous carbon
A magnetic nanoparticle, highly ordered technology, applied in the fields of nanotechnology, nanotechnology, nanotechnology, etc. for materials and surface science, can solve the problems of pore occupancy, magnetic nanoparticle exposure, etc., and achieve efficient separation and preparation steps Simple, exposure-avoiding effects
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[0033] Example 1
[0034] (1) Preparation of ferroferric oxide nanoparticles modified with polyacrylic acid: ferric chloride, sodium acetate, and sodium acrylate with a molar ratio of 1:10:10 are dissolved in a mixed solvent of ethylene glycol and diethylene glycol , After stirring, transfer to a hydrothermal reaction kettle, hydrothermally react for 12 hours to obtain ferroferric oxide magnetic nanoparticles;
[0035] (2) Disperse ferroferric oxide magnetic nanoparticles in deionized water, add cetyltrimethylammonium bromide (CTAB), the mass ratio of ferroferric oxide magnetic nanoparticles to CTAB is 3:7, stir After a certain period of time, add polyether F127 (PEO 106 PPO 70 PEO 106 ), the mass ratio of F127 to ferroferric oxide magnetic nanoparticles is 5, and a solution of ferroferric oxide magnetic nanoparticles coated with CTAB surface active organic template is obtained by stirring;
[0036] (3) Preparation of carbon source prepolymer: phenol and formaldehyde as raw material...
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[0039] Example 2
[0040] (1) Preparation of ferroferric oxide nanoparticles modified with oleic acid on the surface: mix ferric triacetylacetonate, ethylene glycol, oleic acid, and oleylamine in a certain proportion, dissolve and transfer to a hydrothermal reactor, and heat up to 200 ℃, hydrothermal reaction for 3 hours to prepare magnetic nanoparticles of ferroferric oxide;
[0041] (2) Disperse the above ferroferric oxide nanoparticles in chloroform, add F127 aqueous solution, stir for a certain period of time, heat up and volatilize to remove the chloroform, to obtain a surfactant-coated ferroferric oxide nanoparticle solution;
[0042] (3) Preparation of carbon source precursor: phenol, formaldehyde as raw materials, and NaOH as catalyst. The molar ratio of phenol and formaldehyde is 1:3. The reaction is carried out at 70°C for 30 minutes to obtain a carbon source precursor solution.
[0043] (4) Mix the ferroferric oxide nanoparticle solution coated with surfactant and the carb...
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[0045] Example 3
[0046] (1) Preparation of ferroferric oxide nanoparticles modified with octylamine on the surface: add ferric triacetylacetonate to a mixed solvent of octylamine and alcohol, transfer to a hydrothermal reactor, heat up to 240°C, and hydrothermally react for 2h to prepare Obtain ferroferric oxide magnetic nanoparticles;
[0047] (2) Disperse the above ferroferric oxide nanoparticles in chloroform, add F127 aqueous solution, stir for a certain period of time, heat up and volatilize to remove the chloroform, to obtain a surfactant-coated ferroferric oxide nanoparticle solution;
[0048] (3) Preparation of carbon source precursor: Resorcinol, formaldehyde as raw materials, and ammonia water as catalyst. The molar ratio of resorcinol to formaldehyde is 1:2. The reaction is conducted at 35°C for 30 minutes to obtain a carbon source precursor solution.
[0049] (4) Mix the ferroferric oxide nanoparticle solution coated with surfactant and the carbon source precursor solut...
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