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50results about How to "Wrap implementation" patented technology

High-nickel single-crystal ternary cathode material with low surface residual alkali content and preparation method thereof

InactiveCN110436531AIn-situ encapsulationUniform coating in situCell electrodesSecondary cellsLithium hydroxideSingle crystal
The invention discloses a high-nickel single-crystal ternary cathode material with low surface residual alkali content and a preparation method thereof. The preparation method comprises the followingsteps: weighing lithium hydroxide, an oxide additive and a nickel-cobalt-manganese ternary precursor, and carrying out uniform mixing through a dry high-speed mixing process so as to prepare a mixed material; subjecting the mixed material to first sintering so as to obtain a first sintered material; crushing the first sintered material, and carrying out sieving so as to obtain a first crushed material; weighing the first crushed material, a coating agent and deionized water, and carrying out water washing under stirring so as to prepare a slurry, wherein the coating agent comprises an elementX which is one or more selected from the group consisting of B, Al, Ba, Zr, Mg, Ca, Ti, Si, V, Sc, Nb, Ta and Z; drying the slurry under a vacuum condition through a dynamic rotary drying process so as to obtain a dry material; subjecting the dry material to secondary sintering so as to obtain a secondary sintered material; and crushing the secondary sintered material, and carrying out sieving soas to obtain a product. The high-nickel single-crystal ternary cathode material and the preparation method thereof provided by the invention has the following advantages: alkali reduction by water washing and in-situ coating by a wet process can be synchronously completed; the process is simple; high compaction density is realized; and the content of residual alkali is low.
Owner:ZHEJIANG MEIDU HITRANS LITHIUM BATTERY TECHNOLOGY CO LTD

Modification method of lithium nickelate, cobaltate and manganate ternary material

The invention provides a modification method of a lithium nickelate, cobaltate and manganate ternary material. The method comprises the step that after a lithium nickelate, cobaltate and manganate material is subjected to vapor phase deposition under the conditions of carbon source gas and protective gas, a carbon-coated modified lithium nickelate, cobaltate and manganate material is obtained. The modification method provided by the invention has the benefits that carbon deposits on the surface of the lithium nickelate, cobaltate and manganate ternary material through a vapor phase deposition method, so that carbon coating is realized; by adopting simpler processes, with the aid of the protective gas, the ternary material is carbon-coated, so that the problem of lithium nickelate reduction in the coating process of a traditional ternary material is effectively solved, and the coating of a carbon layer on the surface of the ternary material is realized; through the lithium nickelate, cobaltate and manganate ternary material coating carbon, the first-time charging and discharging efficiencies are improved, the lithium ion diffusion coefficients and the electronic conductivity of the material are improved, and the electrochemical performance of the NCM material is improved. According to the modification method provided by the invention, equipment is relatively simple, the process is less, and the structure is controllable; the material has higher battery capacity, cycle performance and rate capability.
Owner:GREE ELECTRIC APPLIANCES INC

Preparation method of photocatalytic functional fabric based on titanium dioxide/magnesium oxide core-shell nanorod

The invention discloses a preparation method of a photocatalytic functional fabric based on a titanium dioxide / magnesium oxide core-shell nanorod. The preparation method comprises the following steps: preparing MgO and TiO2 precursor spinning solution, respectively putting into injectors, adding 18 kV voltage between a coaxial spinneret and a receiving pole plate, controlling the extrusion rate of the respective injectors and collecting the spinning solution onto an aluminum film in a disordered state to form a composite fiber membrane; putting the membrane into a muffle furnace for sintering, cooling, obtaining a TiO2 / MgO core-shell nanometer fiber membrane, adding into absolute ethyl alcohol and carrying out ultrasonic treatment to obtain a TiO2 / MgO core-shell nanometer rod photocatalyst; and preparing nanorod slurry with a mass percentage of 60 percent by using a polyester non-woven fabric as a load fabric and taking self-crosslinking acrylic emulsion as a bonding agent and fixing the photocatalyst on the load fabric by adopting a rolling-drying-baking process. The functional fabric has the advantages of environmental friendliness, recycling capability and large-scale production and can be widely used for treatment of sewage in the industries of printing and dyeing, papermaking and the like.
Owner:ZHEJIANG SCI-TECH UNIV

High-speed molding device and preparation method for conductive foam cotton

ActiveCN107225751ASticky stickersImprove qualityLocalised screeningAdhesiveTextile
The invention provides a high-speed molding device and preparation method for conductive foam cotton, and aims at solving the technical problems that the production efficiency is low, and the quality can not be guaranteed when conductive foam cotton is produced through human assistance. According to the technical scheme, the needed conductive foam cotton is obtained by conducting a series of treatment on a conductive cloth and a sponge strip through a cladding molding device, a heating device, a cooling device, a backing adhesive pasting drawing device and a cutting device; in the cladding molding device, by using a side wall curling structure for a guiding frame and a cladding part, the purpose of cladding the conductive cloth and the sponge strip after aligning the conductive cloth with the sponge strip is achieved, not only can subsequent backing adhesive pasting be convenient, but also a backing adhesive can be aligned at the preconceived conductive cloth attaching portion for sealing, and then the quality of the conductive foam cotton is improved; in addition, cladding of the sponge strip by the conductive cloth can be achieved through the guiding frame and the cladding part without artificial participation, therefore, labor is saved, and the production efficiency is improved.
Owner:深圳市金世冠不干胶制品有限公司

Preparation method of dopamine stabilized Pickering emulsion and application thereof on immobilized enzymes

The invention relates to a preparation method of a dopamine stabilized Pickering emulsion and application thereof on immobilized enzymes. The preparation method is characterized by that hydrophobic modified SiO2 particles are used as a stabilizer, n-heptane is used as an oil phase, a Tris buffer is used as an aqueous phase, and a high speed homogenizer is used for stirring to obtain a SiO2 particle stabilized Pickering emulsion; dopamine is added into the SiO2 particle stabilized Pickering emulsion, and the obtained emulsion is incubated in a water bath shaker at room temperature to produce ablack Pickering emulsion stabilized by both SiO2 and polydopamine. Enzymes are immobilized in an emulsion aqueous phase to determine the stability and application performance of the Pickering emulsion. The prepared dopamine stabilized Pickering emulsion consists of SiO2 nanometer particles and a polymer coating layer, so that the stability is good, and coating of various enzymes can be realized, thereby making the immobilized enzymes have very good thermal stability, storage stability and reusability; and the Pickering emulsion is low in cost, and the preparation method is easy for operation,so that the Pickering emulsion has very good economic feasibility and practicality.
Owner:TIANJIN UNIV

Preparation method of carbon-coated nano tin balls and products and application thereof

The invention discloses a preparation method of carbon-coated nano tin balls and products and application thereof. The preparation method includes: preparing tin oleate mixed liquid, adding the tin oleate mixed liquid into a crystal template, sufficiently stirring and dispersing to enable tin oleate to effectively cover the surface of the crystal template; transferring a mixture of tin oleate andthe crystal template into a tubular furnace, calcining in an atmosphere of protective gas to obtain solid powder, washing the solid powder, and drying to finally obtain a carbon/tin nano composite material. By the preparation method, preparation of a nanocrystal/carbon material is realized through only one step of direct heating, and obtained tin balls are small in nanocrystal size and complete incarbon coating; the preparation method is simple in step and process and easy to control. The products are conducive to shortening lithium ion transmission path and can inhibit volume expansion of tin in the process of charging and discharging and can avoid the problem of agglomeration of tin in the process of intercalation and deintercalation, lithium storage performance of tin is improved effectively, and the tin balls have great application potential in lithium ion battery electrode materials.
Owner:SHANGHAI NAT ENG RES CENT FORNANOTECH

Foam glass prepared from fly ash as well as preparation method and application thereof

The invention discloses foam glass prepared from fly ash as well as a preparation method and application of the foam glass, and belongs to the technical field of foam glass preparation. Fly ash and glass powder are adopted as raw materials and mixed with a foaming agent, then a PVB alcoholic solution is added for granulation, and after molding, high-temperature foaming is conducted through two times of heating, so that the foam glass is obtained. Through two times of heating and heat preservation, part of dioxin can be effectively decomposed, and meanwhile, the formation amount of a high-temperature melt phase is promoted so as to effectively coat residual dioxin, high chlorine, high calcium and heavy metal components. According to the method, the high-temperature melt effectively coats the high chlorine, high calcium, heavy metal components and residual dioxin, the heavy metal elements are left to stand in water for a long time, leakage of the high calcium and high chlorine componentsis little, and harm of the components to the environment is avoided. The method is simple in process and suitable for large-scale production, the fly ash is adopted as the raw material, and the problem of environmental pollution is solved while the low-cost raw material is obtained.
Owner:SHAANXI UNIV OF SCI & TECH

Display panel and display device

The invention discloses a display panel and a display device. The display panel comprises: an array substrate, a light-emitting functional layer positioned on the array substrate, and a packaging structure covering the light-emitting function layer, wherein the packaging structure comprises a first inorganic layer tightly combined with the light-emitting function layer, and the first inorganic layer at least comprises a coating sub-layer used for coating particles on the surface of the light-emitting function layer. The light-emitting device is especially sensitive to water and oxygen in the air; particles or defects can be formed in the evaporation process of the light-emitting device. Water and oxygen invasion is caused by particles and defects; therefore, the failure of the light-emitting device can be caused by long-time exposure in the air; according to the display panel, the problems that the service life of the device is influenced due to the fact that the first inorganic layeris coated with the coating sub-layer are solved, the coating sub-layer of the packaging structure has good particle coating capacity and certain water-oxygen blocking capacity, water-oxygen invasion caused by the existence of particles of the first inorganic layer can be well prevented, packaging failure is caused, and then the service life of the display panel is prolonged.
Owner:KUNSHAN GO VISIONOX OPTO ELECTRONICS CO LTD

Full-automatic infusion device packaging machine with material lacking reminding function

The invention discloses a full-automatic infusion device packaging machine with a material lacking reminding function. The full-automatic infusion device packaging machine with the material lacking reminding function comprises an operation table, a fixing frame, a bracket and a bottom film fixing column; the fixing frame is fixed to one side of the operation table; the bracket is fixed to one endof the operation table; the bottom film fixing column is fixed to the other side of the operation table; an upper film fixing column is fixed to one side of the fixing frame; a tensioning adjusting rod is fixed to one side of the upper film fixing column; a power supply panel is fixed to the top of the fixing frame through a rotating rod; an alarming device is fixed to the top of the rotating rod;a discharging port is fixed to one side of the bracket; a conveying belt is fixed to the surface of the operation table; and an infrared sensor is fixed to one side of the conveying belt and locatedon the surface of the operation table. The full-automatic infusion device packaging machine with the material lacking reminding function is reasonable and novel in deign, convenient to operate and useand high in infusion device packaging efficiency, an operator can be reminded in time during material lacking, waste of upper films and bottom films is wasted, high practicability is achieved, and the full-automatic infusion device packaging machine with the material lacking reminding function is suitable for wide use and popularization.
Owner:浙江圣利机械设备有限公司

Method for cladding nanometer starch microspheres through atomic layer deposition

The invention belongs to the technical field of nanometer starch microsphere modification, and particularly relates to a method for cladding nanometer starch microspheres through atomic layer deposition. The nanometer starch microspheres are placed into an ultrasonic vertical fluidizing atomic layer deposition device, ultrasonic vibration is started, under a proper reaction temperature and pressure, properly-active and vapor-pressure precursors are selected to be alternately introduced, a single layer of chemical adsorption is formed and self-limiting chemical semi-reaction is completed on thesurfaces of the nanometer starch microspheres through exchanging of active functional groups to generate compact thin films, and cladding is performed on all the parts of the surfaces through the thin films with uniform and consistent thickness. The nanometer thin films generated through an atomic layer deposition technology are high in cladding uniformity, especially uniform cladding can be performed on the small-grained nanometer starch microspheres, the formed nanometer thin films are compact in structure and have the uniform thickness and excellent consistency, and due to the characteristics of a reacting mechanism of the thin films, the cladding of the nanometer starch microspheres of different grain sizes can be realized.
Owner:HUST WUXI RES INST

Continuous manufacturing machine capable of synchronously realizing polymer wire coating and metalizing

The invention provides a continuous manufacturing machine capable of synchronously realizing polymer wire coating and metalizing. The continuous manufacturing machine is sequentially equipped with a pay-off device, a coating device, an oxidization-reduction device, a cleaning device and a take-up device from left to right, wherein the coating device comprises a solution slot in the lower part anda gas flow reaction chamber positioned on the upper part; the solution slot is separated from the gas flow reaction chamber through a baffle plate; a gas flow compression heater is arranged on the outer part of the coating device; the left side of the coating device is equipped with a wire inlet hole and the right side of the coating device is equipped with a wire outlet; a plurality of sets of circulating roller groups are arranged in the coating device from left to right; each set of circulating roller groups comprises a roller group arranged in the solution slot and a roller group which isarranged in the gas flow reaction chamber in an adjacent mode; a wire inlet is formed in the left side wall of each of the oxidization-reduction device and the cleaning device, a wire outlet is formed in the right side wall of each of the oxidization-reduction device and the cleaning device, and a roller wheel used for supporting the polymer wire is arranged inside each of the oxidization-reduction device and the cleaning device. The continuous manufacturing machine has the characteristics of simple coating equipment and a simple coating method, a short coating process, good coating and metalizing effect, and the like.
Owner:WUHAN UNIV OF TECH

Environment-friendly ink-jet printing dye ink for artificial cotton and preparation method of environment-friendly ink-jet printing dye ink

The invention discloses a preparation method of environment-friendly inkjet printing dye ink for artificial cotton, which comprises the following steps: adding water and a benzyl vinyl trimethyl ammonium chloride solution into a reactor, adding styrene and butyl acrylate, adding a 2, 2 '-azobis [2-methylpropylamidine]-dihydrochloride solution, and stirring for reaction to prepare a polymer microsphere dispersion liquid; adding caffeic acid, copper chloride and sodium perborate into the polymer microsphere dispersion liquid, heating, stirring and reacting to obtain modified dispersion liquid; adding a reactive dye solution and water into a reactor, adding the modified dispersion liquid, and purifying the mixed liquid through dialysis to prepare a reactive dye/polymer microsphere compound; the reactive dye/polymer microspheres, a dispersing agent, a defoaming agent and water are mixed and added into a mixer for grinding treatment, a viscosity regulator and a pH regulator are added, and the environment-friendly ink-jet printing dye ink for artificial cotton is prepared through stirring. The prepared ink is good in dispersity, high in degree of dyeing and good in color fastness when being used for artificial cotton printing.
Owner:绍兴舜锦纺织品有限公司

A kind of nickel-cobalt-manganese ternary positive electrode material and its preparation method and application

The invention provides a nickel-cobalt-manganese ternary positive electrode material and a preparation method and application thereof. The nickel-cobalt-manganese ternary positive electrode material is LiNi<0.8>Co<0.1>Mn<0.2>O<2>, and the surface with primary particles of the nickel-cobalt-manganese ternary positive electrode material is coated with lithium boron oxide. The preparation method comprises the following steps: dispersing a nickel-cobalt-manganese ternary precursor into an alcohol solution, and performing stirring and mixing to form a solution A; adding boric acid into water, and stirring until the boric acid is completely dissolved to form a solution B; adding the solution B into the solution A, stirring, heating and drying by distillation to obtain solid powder; and mixing the solid powder with lithium salt, and calcining to obtain the nickel-cobalt-manganese ternary positive electrode material. The coating substance H3BO3 is dissolved in an aqueous solution, enters gaps of secondary particles of the ternary precursor, is separated out among the primary particles in the solvent evaporation drying process, and is then fired, so that coating of the primary particles is realized, generation of microcracks of the primary particles can be effectively inhibited, and the cycle stability of a battery is improved.
Owner:CENT SOUTH UNIV

A silicon nanowire, its preparation method and its application for preparing carbon-coated silicon nanowire anode material

The invention discloses a silicon nanowire, a preparation method thereof and an application for preparing a carbon coated silicon nanowire anode material. The method for preparing the silicon nanowire comprises the steps of compacting mixed powder of silicon dioxide and sodium chloride into a cathode slice; carrying out low temperature sintering on the cathode slice; fixing the obtained cathode slice on a iron chrome alloy silk as a cathode, taking high purity graphite as an anode, and carrying out electrolysis in a molten salt system of CaCl <2 > under a high purity argon atmosphere, thereby obtaining the silicon nanowire; carrying out ball milling on enough acetylene black and the silicon nanowire; and sintering the powder obtained through ball milling in an inert atmosphere, thereby obtaining the carbon coated silicon nanowire anode material. The silicon nanowire provided by the invention is good in shape, the carbon coated silicon nanowire anode material is prepared by taking the silicon nanowire as a precursor, and the material is assembled into the cell; the cell has very good cell circulation performance, the electrochemical performance is stable, and the energy density is high; and the preparation method provided by the invention is simple, the production cost is low, and the raw material utilization ratio is high.
Owner:NORTHEASTERN UNIV LIAONING
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