Preparation method and product of Bi12TiO20 micro-spheres
A technology of microspheres and precursor solutions, applied in chemical instruments and methods, nanotechnology, nanotechnology, etc., to achieve the effects of easy control, simple preparation process, and simple preparation process
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Embodiment 1
[0036] 1) Weighing 6 mmol of tetrabutyl titanate and dissolving it in ethylene glycol methyl ether to finally obtain an ethylene glycol methyl ether solution with a tetrabutyl titanate concentration of 0.4 mol / L.
[0037] 2) In a state of stirring, ammonia water is added dropwise to the ethylene glycol methyl ether solution of tetrabutyl titanate prepared in step 1) to hydrolyze the tetrabutyl titanate to obtain titanium oxyhydroxide precipitates. Thereafter, wash and filter with deionized water more than 3 times.
[0038] 3) Weigh 8mmol of ammonium bismuth citrate, dissolve it in deionized water, and finally obtain an aqueous solution of ammonium bismuth citrate with a concentration of 0.4mol / L;
[0039]4) Under stirring, disperse the precipitated titanium oxyhydroxide prepared in step 2) in the aqueous solution of ammonium bismuth citrate prepared in step 3), forming a suspension solution containing titanium oxyhydroxide and ammonium bismuth citrate.
[0040] 5) Weigh 0.12 ...
Embodiment 2
[0047] 1) Weighing 6 mmol of tetrabutyl titanate and dissolving it in ethylene glycol methyl ether to finally obtain an ethylene glycol methyl ether solution with a tetrabutyl titanate concentration of 0.5 mol / L.
[0048] 2) In a state of stirring, ammonia water is added dropwise to the ethylene glycol methyl ether solution of tetrabutyl titanate prepared in step 1) to hydrolyze the tetrabutyl titanate to obtain titanium oxyhydroxide precipitates. Thereafter, wash and filter with deionized water more than 3 times.
[0049] 3) Take 8mmol of ammonium bismuth citrate, dissolve it in deionized water, and finally obtain an aqueous solution of ammonium bismuth citrate with a concentration of 0.5mol / L;
[0050] 4) Under stirring, disperse the precipitated titanium oxyhydroxide prepared in step 2) in the aqueous solution of ammonium bismuth citrate prepared in step 3), forming a suspension solution containing titanium oxyhydroxide and ammonium bismuth citrate.
[0051] 5) Weigh 0.10 ...
Embodiment 3
[0055] 1) Weigh 6 mmol of tetrabutyl titanate, dissolve it in ethylene glycol methyl ether, and finally obtain an ethylene glycol methyl ether solution with a tetrabutyl titanate concentration of 0.7 mol / L.
[0056] 2) In a state of stirring, ammonia water is added dropwise to the ethylene glycol methyl ether solution of tetrabutyl titanate prepared in step 1) to hydrolyze the tetrabutyl titanate to obtain titanium oxyhydroxide precipitates. Thereafter, wash and filter with deionized water more than 3 times.
[0057] 3) Weigh 8mmol of ammonium bismuth citrate, dissolve it in deionized water, and finally obtain an aqueous solution of ammonium bismuth citrate with a concentration of 0.7mol / L;
[0058] 4) Under stirring, disperse the precipitated titanium oxyhydroxide prepared in step 2) in the aqueous solution of ammonium bismuth citrate prepared in step 3), forming a suspension solution containing titanium oxyhydroxide and ammonium bismuth citrate.
[0059] 5) Weigh 0.13 mol o...
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