Inorganic nano photo-crosslinking promoter and nano composite photo-crosslinking EVA adhesive film as well as preparation method thereof
An inorganic nano- and nano-composite technology, applied in adhesives, flat products, adhesive additives, etc., can solve the problems of poor light transmission of IR holes or cursor holes, difficult to remove bubbles, and no light transmission, so as to achieve safety protection The effects of not being harsh, easy to operate, excellent mechanical properties and electrical properties
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Embodiment 1-21
[0039] Prepare inorganic nano photocrosslinking accelerator as follows:
[0040] (1) Pre-dry an inorganic nanopowder in a vacuum box at 100-120°C for more than 4 hours, then weigh a certain amount (100g or less) of the inorganic nanopowder and put it into a 100ml anhydrous In a wide-mouthed bottle of ethanol, use ultrasonic dispersion for 10-30 minutes to obtain a powder-liquid mixture; then transfer the powder-liquid mixture to a four-necked flask, and stir evenly in a constant temperature water bath at 70-80°C. During the stirring process, pass Put the coupling agent mixed uniformly with absolute ethanol into the powder-liquid mixture drop by drop (the quality of the coupling agent is 1-3% of the mass of the inorganic nano-powder), and react for 3-5 hours to obtain the reaction mixture. . The anhydrous ethanol in the reaction mixture is removed by distillation under reduced pressure, and the reaction mixture after removing the solvent is placed in a vacuum oven at 100-120° ...
Embodiment 22
[0048] This embodiment provides a method for preparing an inorganic nano photocrosslinking accelerator, the preparation method is basically the same as that of Example 1, the only difference is: before mixing the inorganic nano powder with absolute ethanol, no drying treatment is performed, That is, directly weigh the inorganic nanopowder and put it into a jar filled with 100ml of absolute ethanol, and disperse it by ultrasonic wave for 10-30min to obtain a powder-liquid mixture. After obtaining the powder-liquid mixture, the follow-up operation is carried out according to the method of Example 1, and finally an inorganic nano-photocrosslinking accelerator is obtained, which is denoted as 22 .
Embodiment 23
[0050] This example provides a method for preparing an inorganic nano-photocrosslinking accelerator, which is basically the same as that of Example 1, except that the reaction mixture after solvent removal is dried in a vacuum oven at 100°C After 0.5h, the modified inorganic nanopowder was obtained. After obtaining the modified inorganic nano-powder, the subsequent operation is carried out according to the method of Example 1, and finally an inorganic nano-photocrosslinking accelerator is obtained, denoted as 23 .
[0051] Respectively apply the inorganic nano-photocrosslinking accelerator as prepared by the above-mentioned embodiment 1 -as 23 Prepare nanocomposite EVA film according to the following method, and the prepared EVA film is respectively marked as EVA 1 -EVA 23 .
[0052] Take respectively 12g of inorganic nano photocrosslinking accelerator, photoinitiator f 6 20g, fast crosslinker c 2 20g, multifunctional auxiliary crosslinking agent d 1 8g, graft coupling...
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