A method for reducing organochlorine and organophosphorus pesticide residues in ginseng extract
An organophosphorus pesticide and ginseng extraction technology, which is applied in the field of medicine and health, can solve problems such as economic loss, harm, ginseng application and export restrictions, and achieve the effect of extremely low pesticide residues and good preservation
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[0027] Example: Extraction and content determination of residual organochlorine pesticides and organophosphorus pesticides in ginseng (taking chlorobromoisocyanuric acid and dimethoate as examples)
[0028] 1 Determination of chlorobromoisocyanuric acid: high performance liquid chromatography, c18 chromatographic column;
[0029] (1) Instrument conditions:
[0030] Mobile phase: methanol-0.01% glacial acetic acid aqueous solution (pH 4.0) [V (methanol): V (glacial acetic acid aqueous solution) = 5:95], flow rate 0.5 mL / min; column temperature 30 ℃; detection wavelength 200 nm; The injection volume is 10 μL. Under these conditions, the retention time of chlorobromoisocyanuric acid is 6.9 min;
[0031] (2) Sample extraction: Weigh 10.0 g of the pretreated sample into a 250 mL ground-neck Erlenmeyer flask, add 20 mL of distilled water, shake lightly to wet the sample, add 80 mL of acetonitrile, and shake for 1 h with a rotary oscillator ,filter. Accurately measure 50 mL of th...
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