Interpenetrating network emulsion having high adhesive force to metal substrate material and synthetic method of interpenetrating network latex
A technology of interpenetrating network and metal substrate, applied in the field of interpenetrating network emulsion and its synthesis, to achieve high damping factor and good adhesion
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Embodiment 1
[0019] Embodiment 1: each raw material constitutes as follows by mass parts:
[0020] Nuclear layer:
[0021] 13.84 parts of methyl methacrylate
[0022] 7.16 parts of n-butyl acrylate
[0023] Ethylene glycol dimethacrylate 0.21 parts
[0024] Dipropylene glycol diacrylate 0.21 parts
[0025] Ammonium persulfate 0.0945 parts
[0026] 12.877 parts of water
[0027] Tridecyl alcohol polyoxyethylene ether sulfate sodium salt 0.252 parts
[0028] Allyl-containing special alcohol ether sulfate 0.504 parts
[0029] Shell:
[0030] 6.72 parts of methyl methacrylate
[0031] Butyl acrylate 14.28 parts
[0032] Polyethylene glycol methacrylate 0.42 parts
[0033] Ammonium persulfate 0.0945 parts
[0034] 20.23 parts of water
[0035] Bottom fluid:
[0036] 22.50 parts of water
[0037] Tridecyl alcohol polyoxyethylene ether sulfate sodium salt 0.504 parts
[0038] Sodium bicarbonate 0.06 parts
[0039] The preparation steps of the core-shell interpenetrating network em...
Embodiment 2
[0051] Embodiment 2: each raw material constitutes as follows by mass parts:
[0052] Nuclear layer:
[0053] 13.84 parts of methyl methacrylate
[0054] 7.16 parts of n-butyl acrylate
[0055] Ethylene glycol dimethacrylate 0.21 parts
[0056] Ammonium persulfate 0.0945 parts
[0057] 12.877 parts of water
[0058] Tridecyl alcohol polyoxyethylene ether sulfate sodium salt 0.252 parts
[0059] Allyl-containing special alcohol ether sulfate 0.504 parts
[0060] Shell:
[0061] 6.72 parts of methyl methacrylate
[0062] Butyl acrylate 14.28 parts
[0063] Polyethylene glycol methacrylate 0.42 parts
[0064] Alkyl acrylate phosphate 0.42 parts
[0065] Ammonium persulfate 0.0945 parts
[0066] 20 parts of water
[0067] Bottom fluid:
[0068] 22.26 parts of water
[0069] Tridecyl alcohol polyoxyethylene ether sulfate sodium salt 0.504 parts
[0070] Sodium bicarbonate 0.1 part
[0071] Example 2 Synthesis steps are the same as Example 1.
[0072] The detection ...
Embodiment 3
[0073] Embodiment 3: each raw material constitutes as follows by mass parts:
[0074] Nuclear layer:
[0075] 13.84 parts of methyl methacrylate
[0076] 7.16 parts of n-butyl acrylate
[0077] Ethylene glycol dimethacrylate 0.63 parts
[0078] Ammonium persulfate 0.0945 parts
[0079] 12.657 parts of water
[0080] Tridecyl alcohol polyoxyethylene ether sulfate sodium salt 0.504 parts
[0081] Allyloxypropyl alkyl alcohol polyether nonionic emulsifier 0.252 parts
[0082] Shell:
[0083] 6.72 parts of methyl methacrylate
[0084] Butyl acrylate 14.28 parts
[0085] Polyethylene glycol methacrylate 0.42 parts
[0086] Alkyl acrylate phosphate 0.63 parts
[0087] Ammonium persulfate 0.0945 parts
[0088] 20 parts of water
[0089] Bottom fluid:
[0090] 22 parts of water
[0091] Tridecyl alcohol polyoxyethylene ether sulfate sodium salt 0.504 parts
[0092] Sodium bicarbonate 0.2 parts
[0093] Embodiment 3 synthesis steps are the same as embodiment 1.
[0094...
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Abstract
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