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Preparation method of insulating high-thermal radiation coating suitable for various base materials

A heat-dissipating coating and high-radiation technology, applied in coatings, polyurea/polyurethane coatings, etc., can solve the problems of poor electrical insulation and chemical resistance, little research on radiation heat dissipation characteristics, and poor radiation heat dissipation effect. Excellent resistance to salt spray, broad market prospects, and the effect of improving service life

Active Publication Date: 2015-05-13
AEROSPACE RES INST OF MATERIAL & PROCESSING TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional heat dissipation coatings mainly rely on the addition of various high thermal conductivity fillers to achieve high thermal conductivity, generally using metals (such as Au, Ag, Cu, Al, Mg, etc.), or non-metallic materials (such as graphite, carbon black, etc.) As a filler, although this type of coating has high thermal conductivity, it also has some disadvantages: low emissivity, poor radiation heat dissipation effect, poor electrical insulation and chemical resistance, and high cost
[0003] At present, thermally conductive materials have been widely used in microelectronics, high-power heat generating appliances, automobiles and other fields. The United States, Japan and other countries have also applied thermally conductive materials to aircrafts, space capsules, etc. At the same time, there are not many studies on the characteristics of radiation heat dissipation, and there are few reports on coating materials with both insulation and high radiation heat dissipation functions.

Method used

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  • Preparation method of insulating high-thermal radiation coating suitable for various base materials
  • Preparation method of insulating high-thermal radiation coating suitable for various base materials
  • Preparation method of insulating high-thermal radiation coating suitable for various base materials

Examples

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preparation example Construction

[0028] The preparation method of insulating high radiation heat dissipation coating suitable for various substrates includes the following steps:

[0029] (1) Add the film-forming material, insulating and thermally conductive filler, solvent, wetting and dispersing agent, defoaming agent, leveling agent and drier into the container, and stir evenly to prepare a varnish slurry, each in parts by mass The group distribution is as follows:

[0030] 40-60 parts of film-forming material, 30-50 parts of insulating and thermally conductive filler, 40-70 parts of solvent

[0031] 0.3-2.0 parts of wetting and dispersing agent 0.2-1.0 parts of defoaming agent 0.1-0.8 parts of leveling agent

[0032] 0.02-0.1 parts of drier;

[0033] The film-forming substance is one or a combination of hydroxy acrylic resin, polyester modified hydroxy acrylic resin, or polyether modified hydroxy acrylic resin.

[0034] The insulating thermal conductive filler is a combination of a nitride thermal conductive filler...

Embodiment 1

[0040] This embodiment includes the following steps:

[0041] (1) Add 100g of hydroxy acrylic resin, 64g of aluminum nitride, 16g of α-alumina, 65g of butyl acetate, 30g of ethyl acetate, 1.8g of wetting and dispersing agent (Disponer 9250), and defoaming agent ( Defom5300) 1.2g, leveling agent (Levelol839) 0.8g, drier (dibutyltin dilaurate) 0.06g, stir and mix with a glass rod to prepare a paint slurry.

[0042] (2) Pour the paint slurry in step (1) slowly into a ball mill tank, and use a planetary ball mill to grind and disperse for 2 hours to obtain a uniformly dispersed paint slurry.

[0043] (3) Filter the uniformly dispersed paint slurry in step (2) with a 100 μm filter, pour it into a jar, add 24 g of the cross-linking curing agent HDI biuret, and stir evenly.

[0044] (4), using aluminum alloy plate, red copper sheet, ABS plate and tinplate (tinning amount is E 4 , Hardness grade is T52), as the object to be sprayed, sand it with 240# sandpaper, and wipe the surface of the sam...

Embodiment 2

[0050] This embodiment includes the following steps:

[0051] (1) Add 80 g of hydroxy acrylic resin, 35 g of polyester modified hydroxy acrylic resin, 40 g of silicon nitride, 36 g of aluminum nitride, 19 g of α-alumina, 40 g of xylene, 60 g of butyl acetate, and ethyl acetate into the paint mixing tank. Ester 25g, wetting and dispersing agent (BYK-110) 2.5g, defoaming agent (BYK-052) 1.3g, leveling agent (BYK-358) 0.9g, drier (dibutyltin dilaurate) 0.06g, Stir and mix with a glass rod to prepare a paint slurry.

[0052] (2) Pour the paint slurry in step (1) slowly into a ball mill tank, and use a planetary ball mill to grind and disperse for 2 hours to obtain a uniformly dispersed paint slurry.

[0053] (3) Filter the uniformly dispersed paint slurry in step (2) with a 100 μm filter, pour it into a jar, add 28 g of the crosslinking curing agent HDI biuret, and stir evenly.

[0054] (4) Using aluminum alloy plate, red copper sheet, ABS plate and tinplate (the amount of tin plating is...

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Abstract

The invention relates to a preparation method of an insulating high-thermal radiation coating suitable for various base materials. The paint of the coating comprises the following ingredients by mass: 40 to 60 parts of a film-forming material, 30 to 50 parts of an insulating heat conducting filler, 40 to 70 parts of solvents, 0.3 to 2.0 parts of a wetting dispersant, 0.2 to 1.0 part of a foam killer, 0.1 to 0.8 part of a leveling agent, 0.02 to 0.1 part of a drier, 5 to 15 parts of a cross-linked curing agent adopting isocyanate. The preparation method comprises the following steps: uniformly spraying the paint on the surface of a device in such a manner that the sprayed layer is 0.01 to 0.03 mm in thickness each time and the total thickness is 0.13 to 0.18 mm. The coating prepared according to the method is high in hemispherical emissivity, thermal conductivity and volume resistivity, and has excellent salt spray resistance, moisture and heat resistance and aging resistance.

Description

Technical field [0001] The invention relates to a method for preparing an insulating high-radiation heat dissipation coating suitable for a variety of substrates, and belongs to the technical field of functional coatings. Background technique [0002] With the advancement of technology and the rapid development of the electronics industry, LED lighting equipment, CPU circuit boards and high-power electronic equipment heat sinks have proposed high thermal conductivity, high radiation heat dissipation and high insulation properties compatible with the surface coating of electronic device heating devices. demand. Traditional heat dissipation coatings mainly rely on the addition of various fillers with high thermal conductivity to achieve high thermal conductivity, and generally use metals (such as Au, Ag, Cu, Al, Mg, etc.) or non-metallic materials (such as graphite, carbon black, etc.) As a filler, although this type of coating has a high thermal conductivity, it also has some dis...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D175/04C09D5/25C09D7/12
CPCC08K3/22C08K3/28C08K3/34C08K2003/2227C08K2003/282C09D5/00C09D7/61C09D7/69C09D175/04
Inventor 尹雨晨姜舟雷辉罗正平曾一兵卢鹉
Owner AEROSPACE RES INST OF MATERIAL & PROCESSING TECH
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