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Preparation technology of calcium lime absorbent for carbon dioxide in anesthesia respirator

A carbon dioxide and preparation technology, applied in inorganic chemistry, alkali metal oxides/hydroxides, alkali metal compounds, etc., can solve the problems of unfavorable multiple absorption and repeated utilization, limited calcium lime absorption capacity, and pore structure damage , to achieve excellent thermal stability, not easy to soften and damage, maintain the effect of porosity and absorption rate

Inactive Publication Date: 2015-07-29
HENAN AINASHENG MEDICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Medical calcium lime is often placed in the ventilator to absorb carbon dioxide. It does not produce harmful substances such as carbon monoxide and formaldehyde, and has low dust. However, the existing calcium lime has limited absorption capacity, and the absorption effect is significantly reduced during high-temperature regeneration, and the pore structure is destroyed. The surface area changes greatly, which is not conducive to repeated absorption and repeated use

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Embodiment 1: The absorbent of this embodiment is made by the following steps: at first nanoscale nitric acid is dissolved in deionized water, is mixed with the solution that concentration is 0.1g / ml; Nanoscale calcium bicarbonate powder is dissolved in deionized water Water is prepared into a solution with a concentration of 0.01g / ml; then the solutions obtained in the first two steps are mixed, and 1% of the dispersant polyethylene glycol 600 of the aforementioned nanoscale zirconium nitrate and nanoscale calcium salt mass sum is added. Sonicate in an ultrasonic water bath at 60-80°C for 30 minutes; after ultrasonication, add a weak base solution to adjust the pH to 11, so that the calcium in the solution can be completely precipitated, stir evenly until the pH is stable; then centrifuge and filter Evaporate and dehydrate until the product is gel or paste, wash with ethanol, dry and grind to the required mesh size, such as 200 mesh, 300 mesh; calcinate the dry and grou...

Embodiment 2

[0030] Embodiment 2: The absorbent of this embodiment is made by the following steps: first dissolving nano-scale zirconium nitrate in deionized water, and being mixed with a solution with a concentration of 0.1g / ml; dissolving nano-scale calcium bicarbonate powder in deionized water Ionized water is prepared into a solution with a concentration of 0.01g / ml; then the solutions obtained in the first two steps are mixed, and the dispersant polyethylene glycol 1000 of 1% of the total mass of the aforementioned nanoscale zirconium nitrate and nanoscale calcium salt is added, Sonicate in an ultrasonic water bath at 60-80°C for 30 minutes; after ultrasonication, add a weak base solution to adjust the pH to 12, so that the calcium in the solution can be completely precipitated, stir evenly until the pH is stable; then centrifugally filter After evaporation and dehydration until the product is in the form of gel or paste, it is washed with ethanol and then dried and ground to the desir...

Embodiment 3

[0031] Embodiment 3: The absorbent of this embodiment is prepared by the following steps: first, nano-sized zirconium nitrate is dissolved in deionized water to prepare a solution with a concentration of 0.1g / ml; nano-sized calcium chloride powder is dissolved in deionized water Ionized water is prepared into a solution with a concentration of 0.01g / ml; then the solutions obtained in the first two steps are mixed, and the dispersant polyethylene glycol 1000 of 1% of the total mass of the aforementioned nanoscale zirconium nitrate and nanoscale calcium salt is added, Sonicate in an ultrasonic water bath at 60-80°C for 30 minutes; after ultrasonication, add a weak base solution to adjust the pH to 12, so that the calcium in the solution can be completely precipitated out, stir evenly until the pH value is stable; then centrifugally filter After evaporation and dehydration until the product is gel or paste, it is washed with ethanol and then dried and ground to the desired mesh si...

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PUM

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Abstract

The invention belongs to the technical field of medical carbon dioxide absorption and particularly relates to a preparation technology of a calcium lime absorbent for carbon dioxide in an anesthesia respirator. The preparation technology is characterized by comprising the following steps: a nanoscale zirconium nitrate solution with the concentration of 0.1 g / ml is prepared; a calcium salt solution with the concentration of 0.01 g / ml is prepared; the two solutions are mixed, a dispersing agent accounting for 1%-3% of the mass sum of nanoscale zirconium nitrate and calcium salt is added, and the mixture is subjected to ultrasonic processing for 30 min-60 min at the temperature of 60-80 DEG C; a weak base solution is added to regulate the pH to be alkaline; a product is subjected to centrifugal filtration and evaporating dehydration until the product is gelatinous or pasty, and the product is washed with ethanol and dried and ground to the required mesh number; the product after drying and grinding is calcined for 30-40 min at the temperature of 700-1,000 DEG C to prepare the absorbent. The preparation technology has the benefits as follows: obtained calcium lime has large specific surface area and good absorption effect and can keep higher carbon dioxide absorption rate after repeated calcination and recovery.

Description

technical field [0001] The invention belongs to the technical field of medical carbon dioxide absorption, and in particular relates to a preparation process of a calcium lime absorbent for anesthesia ventilator carbon dioxide. Background technique [0002] An anesthesia ventilator is a device that provides gas anesthesia and respiratory management functions for patients. In actual clinical use, the supply of oxygen and anesthetics are operated by doctors. Due to the different conditions of each patient, patients also need different supplies in different stages of the disease. In the case of dyspnea, the patient will Carbon dioxide uptake is especially important. Medical calcium lime is often placed in the ventilator to absorb carbon dioxide. It does not produce harmful substances such as carbon monoxide and formaldehyde, and has low dust. However, the existing calcium lime has limited absorption capacity, and the absorption effect is significantly reduced during high-temper...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/04B01J20/28B01J20/30B01D53/02B01D53/14
CPCY02A50/20Y02C20/40
Inventor 陈顺俊陈宁
Owner HENAN AINASHENG MEDICAL TECH CO LTD
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