Preparation method of nano-composite membrane electrode material
A nanocomposite, membrane electrode technology, applied in battery electrodes, nanotechnology, nanotechnology, etc., can solve the problems of agglomeration, high lithium intercalation potential, poor electrical conductivity, etc., and achieve stable performance, uniform particle size, and improved electrical conductivity. Effect
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Embodiment 1
[0027] (1) dissolving manganese sulfate, tetrabutyl titanate, and polyacrylonitrile in N,N-dimethylformamide (DMF) is prepared into a uniform spinning solution, so that the concentration of manganese sulfate is 0.3mol / L, The concentration of tetrabutyl titanate is 1.0 mol / L, and the mass concentration of polyacrylonitrile is 10 wt%.
[0028] (2) Carry out electrospinning to described spinning solution, obtain nanofiber material, namely electrospun nanofiber precursor film, wherein the condition of electrospinning is, needle inner diameter 1mm, spinning voltage 12kV, receiving mode is drum receiving , the spinning solution flow rate is 0.5ml / h, the receiving distance is 20cm, and the spinning time is 3h.
[0029] (3) Carrying out pre-oxidation treatment to the nanofibrous material, the process is firstly keeping the temperature at 120° C. for 1 hour, and then keeping the temperature at 250° C. for 2 hours. After pre-oxidation treatment, in a nitrogen atmosphere, control the he...
Embodiment 2
[0031] (1) Dissolve manganese acetate, titanic acid, and polyvinyl alcohol in DMSO to prepare a uniform spinning solution, so that the concentration of manganese acetate is 0.1mol / L, the concentration of titanic acid is 0.1mol / L, and the mass of polyvinyl alcohol The concentration is 7 wt%.
[0032] (2) Electrospinning is carried out to described spinning solution, obtains nanofiber material, namely electrospun nanofiber precursor film, and wherein the condition of electrospinning is, needle inner diameter 0.6mm, spinning voltage 20kV, receiving mode is drum For receiving, the flow rate of the spinning solution is 0.3ml / h, the receiving distance is 30cm, and the spinning time is 2h.
[0033] (3) Carrying out pre-oxidation treatment to the nanofibrous material, the process is firstly keeping the temperature at 100° C. for 2 hours, and then keeping the temperature at 250° C. for 4 hours. After the pre-oxidation treatment, in a nitrogen atmosphere, control the heating rate at 3°...
Embodiment 3
[0035] (1) Dissolve manganese oxalate, isopropyl titanate, and polyvinylpyrrolidone in chloroform to prepare a uniform spinning solution, so that the concentration of manganese oxalate is 0.5mol / L, and the concentration of isopropyl titanate is 0.5mol / L, the mass concentration of polyvinylpyrrolidone is 15wt%.
[0036] (2) Electrospinning is carried out to described spinning solution, obtains nanofiber material, namely electrospun nanofiber precursor film, and wherein the condition of electrospinning is, needle inner diameter 2.0mm, spinning voltage 8kV, receiving mode is drum For receiving, the flow rate of the spinning solution is 1.5ml / h, the receiving distance is 10cm, and the spinning time is 6h.
[0037] (3) Pre-oxidize the nanofibrous material, the process is to first keep warm at 100° C. for 2 hours, and then keep the temperature at 250° C. for 2 hours. After the pre-oxidation treatment, in a helium atmosphere, control the heating rate at 5°C / min. When it reaches 100...
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