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A kind of method that utilizes waste plastic bottle to prepare super imitation cotton fabric

A technology of super imitation of cotton and fabrics, applied in the field of preparation of environmental protection materials, can solve problems such as negative effects, visual pollution, environmental pollution, etc., and achieve the effects of reducing disposal load, reducing pollution, and avoiding visual pollution.

Active Publication Date: 2016-09-07
DALIAN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If it is not handled properly, it will bring negative effects to the environment and cause serious environmental pollution.
These waste plastic packaging will not only cause "visual pollution", but even produce an ecological crisis

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] (1) Collect polyester beverage bottles, clean and classify, and crush into flakes; dissolve the sorted polyester bottle flakes in a mixed solvent of phenol and tetrachloromethane with a mass ratio of 1:1, and use Ubbelohde's viscosity Measure its intrinsic viscosity with a meter, record as material A for polyester bottle flakes with intrinsic viscosity greater than 0.63dL / g, and record as material B for polyester bottle flakes with intrinsic viscosity less than 0.63dL / g;

[0029] (2) Add 38.5 parts of ethylene glycol to 20.4 parts of material B, carry out alcoholysis reaction at 220°C for 2 hours, add 30.63 parts of terephthalic acid to the alcoholysis product, and add 5.2 parts of 3,5-isophthalic acid at the same time Sodium sulfur, 0.63 parts of maleic anhydride, 38.5 parts of ethylene glycol and 3.7 parts of polyethylene glycol 400, after esterification reaction at 255 ° C for 3 hours, the reaction product was poured into a polymerization kettle with a temperature of ...

Embodiment 2

[0034] (1) Collect polyester beverage bottles, clean and classify them, and crush them into flakes; dissolve the sorted polyester bottle flakes in a mixed solvent of phenol and tetrachloromethane with a mass ratio of 1:1, and use an Ubbelohde viscometer Measure its intrinsic viscosity, record as material A for polyester bottle flakes with intrinsic viscosity greater than 0.63dL / g, and record as material B for polyester bottle flakes with intrinsic viscosity less than 0.63dL / g;

[0035] (2) Add 38.5 parts of ethylene glycol to 31.2 parts of material B, carry out alcoholysis reaction at 210°C for 3 hours, add 20.8 parts of terephthalic acid to the alcoholysis product, and add 6 parts of 3,5-isophthalic acid at the same time Sodium sulfur, 0.8 parts of maleic anhydride, and 3.8 parts of polyethylene glycol 400, after the esterification reaction at 250°C for 4 hours, put the reaction product into a polymerization kettle with a temperature of 265°C, and wait for the temperature of t...

Embodiment 3

[0040] (1) Collect polyester beverage bottles, clean and classify, and crush into flakes; dissolve the sorted polyester bottle flakes in a mixed solvent of phenol and tetrachloromethane with a mass ratio of 1:1, and use Ubbelohde's viscosity Measure its intrinsic viscosity with a meter, record as material A for polyester bottle flakes with intrinsic viscosity greater than 0.63dL / g, and record as material B for polyester bottle flakes with intrinsic viscosity less than 0.63dL / g;

[0041] (2) Add 39 parts of ethylene glycol to 25.5 parts of material B, carry out alcoholysis reaction at 230° C. for 2 hours, and carry out alcoholysis. Add 25.5 parts of terephthalic acid to the alcoholysis product, add 5.7 parts of 3,5-sulfur sodium isophthalate, 0.8 parts of maleic anhydride and 3.8 parts of polyethylene glycol 400 at the same time, carry out esterification reaction at 250 ° C for 3 h Finally, put the reaction product into a polymerization kettle with a temperature of 265°C, and s...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention discloses a production method of super-imitation cotton fabric using waste polyester bottles. The method includes classifying the waste polyester bottles, and subjecting recycled polyester with intrinsic viscosity of less than 0.63g / dl to alcoholysis and esterification to obtain copolyester with a good hydrolytic function; subjecting recycled polyester with intrinsic viscosity of greater than 0.63g / dl and the copolyester to blending, fusion and spinning to obtain blend fibers; spinning the blend fibers to obtain fabric, performing treatment with dilute alkali solution to remove material C before drying, and subjecting the dried fabric in impregnating solution composed of polyethylene glycol monoester maleate and potassium persulfate to immersion treatment to obtain novel polyester fabric with super-imitation-cotton performance. According to the method, the waste plastic bottles are utilized to prepare the novel super-imitation cotton fabric, thus visual pollution can be avoided, resources can be recycled, pollution can be reduced, burden on municipal solid waste disposal can be relieved, land consumption can be saved , and good economic benefits can be achieved.

Description

technical field [0001] The invention belongs to the technical field of preparation of environment-friendly materials, and in particular relates to a method for preparing super-cotton imitation fabrics by using waste polyester bottles. Background technique [0002] In recent years, China's national economy has maintained a steady and rapid development, and environmental protection and resource regeneration have become an important part of my country's new economy and harmonious society construction. my country is one of the top ten plastic products producing and consuming countries in the world. A large number of plastic products are produced and consumed every year. If it is not handled properly, it will bring negative effects to the environment and cause serious environmental pollution. These waste plastic packaging will not only cause "visual pollution", but even produce an ecological crisis. [0003] Super-imitation cotton looks like cotton (visual), feels like cotton ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M15/27D01F8/14C08G63/676
Inventor 郭静张渤李星尧刘元法管福成张森
Owner DALIAN POLYTECHNIC UNIVERSITY
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