Tobacco extract and electronic cigarette liquid for electronic cigarette without sweet and greasy feeling
A technology of tobacco extract and electronic cigarette liquid, which is applied in the directions of tobacco, tobacco treatment, and smoker's products, etc., can solve the problems of reducing the aroma of tobacco and affecting the permeability of tobacco aroma, and achieves good permeability and strong aroma of tobacco. , taste clean and comfortable effect
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Embodiment 1
[0024] 1 kg of flue-cured tobacco raw material was weighed, and the content of reducing sugar in the raw material was determined by continuous flow method. The content of reducing sugar in flue-cured tobacco was determined to be 14%. Assuming that the reducing sugar was all glucose, the molar amount of reducing sugar was calculated to be 0.78 mol. Put the raw material in a SY-III-A experimental tobacco processor, spray ammonia and seal it for 12 h (the molar ratio of ammonia to reducing sugar is 1:1, that is, the amount of ammonia is 0.78 mol) to fully absorb it; then Heat to 80 o Bake for 1.5 h.
[0025] After the pretreated raw material is pulverized, 95% ethanol is added, and solvent extraction is used for extraction. The ratio of solid to liquid is 1:10, and the extraction temperature is 25 o C, the extraction time is 12 h and extracted twice; after the extraction, filter the extract with a 400-mesh filter cloth, and concentrate the extract under reduced pressure until th...
Embodiment 2
[0027] 1 kg of oriental tobacco raw material was weighed, and the content of reducing sugar in the raw material was determined by continuous flow method. Put the raw material in the SY-III-A experimental tobacco processor, spray glycine aqueous solution and seal it for 24 h (the amount of glycine is 0.5 times the molar amount of reducing sugar, and the concentration of aqueous solution is 40%) to make it fully absorbed; then Heat up to 100 o Bake for 1 h.
[0028] Crush the pretreated raw material, weigh a certain amount of raw material, wrap it with filter paper, put it in a 1L Soxhlet extractor, add 6 times the mass of petroleum ether (60-90°C), and connect it to the bottom of the Soxhlet extractor. 2 L round bottom flask, the upper end is connected with a condensing device, heated and refluxed for 8 h to extract once; after the extraction is completed, the extract is cooled to room temperature, and concentrated under reduced pressure until there is no solvent to obtain tob...
Embodiment 3
[0030] Weigh 1 kg raw material of sun-cured yellow tobacco, and use continuous flow method to determine the content of reducing sugar in the raw material. Put the raw material in the SY-III-A experimental tobacco processor, spray the proline aqueous solution and seal it for 48 hours (the dosage is 3 times the molar amount of reducing sugar, and the concentration of the aqueous solution is 70%) to make it fully absorbed; Then heat to 120 o Bake at C for 0.5 h.
[0031] Crush the pretreated raw material, weigh a certain amount of raw material, wrap it with filter paper, put it in a 1L Soxhlet extractor, add 8 times the mass of ethyl acetate, and connect a 2 L round bottom flask under the Soxhlet extractor , the upper end is connected to a condensing device, heated and refluxed for 4 h to extract twice; after the extraction is completed, the extract is cooled to room temperature, and concentrated under reduced pressure until there is no solvent to obtain tobacco extract; add 8 t...
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