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Boron carbide accurate grinding aid and use method thereof

A grinding aid, boron carbide technology, applied in chemical instruments and methods, other chemical processes, grain processing, etc., can solve problems such as lack of research

Active Publication Date: 2015-12-02
中硼科技(牡丹江)有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the prior art, there is a lack of research on the method of fine grinding of boron carbide. After research, the inventor provides a grinding aid that can improve the efficiency of fine grinding of boron carbide and reduce the difficulty of fine grinding.

Method used

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  • Boron carbide accurate grinding aid and use method thereof
  • Boron carbide accurate grinding aid and use method thereof
  • Boron carbide accurate grinding aid and use method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0064] Mix and stir 50kg of triisopropanolamine, 10kg of polyacrylamide, 10kg of calcium metaphosphate, 5kg of tributyl phosphate and 25kg of water to prepare a grinding aid.

[0065] Put the boron carbide raw material (D50 particle size is 19.43μm) into the ball mill according to the material ball water ratio = 1:2.5:0.5, wherein, the material refers to the boron carbide raw material, the ball refers to the abrasive ball in the ball mill, and the water is pre-added when starting the ball mill Water, in this embodiment, 100 kg of boron carbide raw material, 250 kg of abrasive balls, and 50 kg of water, that is, the solid content is 66.7%, and the target ball milling D50 particle size is 3.6 μm.

[0066] After the above mixture was ball milled for 8 hours, the grinding aid prepared in the above steps was added in an amount of 0.35% relative to the weight of the boron carbide powder, that is, 350 g.

[0067] During the ball milling process, due to the heat generated, a large amo...

Embodiment 2

[0069] Mix and stir 55kg of triisopropanolamine, 10kg of polyacrylamide, 12kg of sodium hexametaphosphate, 8kg of diethylethanol and 15kg of water to prepare a grinding aid.

[0070] Put the boron carbide raw material (D50 particle size is 20.27μm) into the ball mill according to the material ball water ratio = 1:2.8:0.6, wherein, the material refers to the boron carbide raw material, the ball refers to the abrasive ball in the ball mill, and the water is pre-added when starting the ball mill Water, in this embodiment, 100kg of boron carbide raw material, 280kg of abrasive balls, 60kg of water, that is, the solid content is 62.5%, and the target ball mill particle size D50 is 3.0 μm.

[0071] After the above mixture was ball milled for 6 hours, the grinding aid prepared in the above steps was added in an amount of 0.6% relative to the weight of the boron carbide powder, that is, 600 g.

[0072] During the ball milling process, due to the heat generated, a large amount of water...

Embodiment 3

[0074] Mix and stir 55kg of triethanolamine, 10kg of succinimide, 12kg of aluminum metaphosphate, 8kg of polyoxypropylene polyoxyethylene glyceryl ether and 15kg of water to prepare a grinding aid.

[0075] Put the boron carbide raw material (D50 particle size is 20.27μm) and the above-mentioned grinding aid into the ball mill according to the ratio of material, ball, water and grinding aid = 1:2.8:0.6:0.6%, wherein, the material refers to The boron carbide raw material, the ball refers to the abrasive ball in the ball mill, and the water is the water pre-added when starting the ball mill. In this embodiment, the boron carbide raw material is 100kg, the abrasive ball is 280kg, the water is 60kg, and the grinding aid is 600g, that is, the solid content is 62.5 %, the target ball mill particle size D50 is 3.0 μm.

[0076] During the ball milling process, due to the heat generated, a large amount of water evaporates. Therefore, it is necessary to properly replenish water to ensur...

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Abstract

The invention provides a boron carbide accurate grinding aid and a use method thereof. The accurate grinding aid is prepared by mixing an alcamines substance, an amide substance, inorganic salt, a defoaming agent and any parts of water. The boron carbide accurate grinding aid is added while accurate grinding, can improve slid content of slurry and ore grinding efficiency and enables particle size of the boron carbide to be distributed in a concentration manner.

Description

technical field [0001] The invention relates to the field of boron carbide fine grinding, in particular to a boron carbide fine grinding grinding aid and a use method thereof. Background technique [0002] Boron carbide is a superhard material, its hardness is second only to diamond and cubic boron nitride, so it is very difficult to finely grind boron carbide, and most of the mechanical energy is converted into heat energy during the fine grinding process of boron carbide, which is wasted , At the same time, as the fineness of boron carbide powder increases during the grinding process, the surface energy increases, and the fine particles will aggregate, resulting in a sharp drop in grinding efficiency. [0003] Therefore, there is an urgent need to develop a method that can improve the above phenomenon. [0004] In the prior art, there is a lack of research on the method of boron carbide fine grinding. After research, the inventors provide a grinding aid that can improve t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B02C23/06B02C17/10C09K3/14
Inventor 李鹏张继红杨金茹
Owner 中硼科技(牡丹江)有限公司
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