Method for separating and recycling valuable metal in tungsten slag
A technology for the separation and recovery of valuable metals, applied in the direction of improving process efficiency, can solve the problems of single recovery species and high energy consumption, and achieve the effects of high production efficiency, low energy consumption, and easy realization
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[0036] Example 1:
[0037] A method for separating and recovering valuable metals in tungsten slag, comprising the following steps:
[0038] (1) The tungsten slag is subjected to wet ball milling to obtain fine powder slurry;
[0039] In the present invention, in step (1), the granularity of the fine powder ore pulp is -100 mesh.
[0040] (2) Add liquid caustic soda to the fine powder ore pulp prepared in step (1) to prepare 1N~3N alkaline ore pulp, start stirring, heat up to 80°C with steam, introduce ozone, keep the temperature not lower than 80°C, and react for 1 hour~ 2 hours;
[0041] (3) Carry out solid-liquid separation of the ore pulp after the ozone alkali leaching reaction in step (2), adjust the pH of the filtrate to 8-9 with hydrochloric acid or sulfuric acid, filter and remove silicon, and recover artificial scheelite with calcium chloride precipitation;
[0042] In the process of using ozone alkali leaching, ozone is used as an oxidant to oxidize the metal in ...
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