Glass film containing rare earth ion-doped Cs2LiYCl6 microcrystalline and preparation method of glass film
A technology of rare earth ions and glass films, which is applied in the field of glass films containing rare earth ions doped with Cs2LiYCl6 microcrystals and its preparation, can solve problems such as device limitations, achieve the effects of preventing decomposition and volatilization, and overcoming incomplete uniformity
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Embodiment 1
[0043] Cs doped with rare earth ions 2 LiYCl 6 The preparation method of the glass thin film of crystallite comprises following specific steps:
[0044] (1), prepare raw materials in molar ratio: tetraethoxygermanium: aluminum sec-butoxide: trimethyl phosphate: cesium chloride: lithium chloride: yttrium chloride: cerium chloride=71: 20: 20: 16 : 8: 8: 1, taking by weighing a total amount of 30 grams of analytically pure raw materials for each preparation, stand-by;
[0045] (2), the hydrolysis of tetraethoxygermanium: the tetraethoxygermanium weighed in the step (1) is dissolved in dehydrated alcohol, and the mol ratio of dehydrated alcohol and tetraethoxygermanium is 2: 1, fast Add acetylacetone, the volume ratio of acetylacetone to tetraethoxygermanium is 0.6:1, and carry out strong magnetic stirring, gradually drop distilled water, the molar ratio of distilled water to tetraethoxygermanium is 0.6:1, carry out hydrolysis at room temperature React for 1 hour to make soluti...
Embodiment 2
[0056] It is basically the same as Example 1, except that in the step (1), the raw materials are prepared according to the following molar ratios: tetraethoxygermanium: aluminum sec-butoxide: trimethyl phosphate: cesium chloride: lithium chloride: chloride Yttrium: europium chloride=75: 10: 10: 24: 12: 12: 3, each raw material is weighed respectively; In the step (8), the pulling speed of the glass substrate in the gel solution is controlled at 1 mm / s, Repeat the pulling 5 times, each time the pulling interval is 15 minutes; in step (9), heat up to 100°C at a rate of 50°C per hour, and then heat up the furnace to 340°C at a rate of 50°C per hour; In step (10), gradually raise the temperature of the furnace to 650 ° C, and react at this temperature for 2 hours, and finally obtain the Eu-containing 3+ Ion-doped Cs 2 LiYCl 6 Microcrystalline 75GeO 2 -5Al 2 o 3 -5P 2 o 5 -12Cs 2 LiYCl 6 -3EuCl 3 System glass film
[0057] For prepared Eu-containing 3+ Ion-doped Cs 2 L...
Embodiment 3
[0059] It is basically the same as Example 1, except that in the step (1), the raw materials are prepared according to the following molar ratios: tetraethoxygermanium: aluminum sec-butoxide: trimethyl phosphate: cesium chloride: lithium chloride: chloride Yttrium: terbium chloride=73: 16: 14: 20: 10: 10: 2, each raw material is weighed respectively; In the step (8), the pulling speed of the glass substrate in the gel solution is controlled at 0.6 mm / s, Repeat the pulling 3 times, each pulling interval is 15 minutes; in step (9), heat up to 100°C at a rate of 40°C per hour, and then heat up the furnace to 340°C at a rate of 40°C per hour; In step (10), gradually raise the temperature of the furnace to 640° C., and react at this temperature for 3 hours. Finally get Tb 3+ Ion-doped Cs 2 LiYCl 6 Microcrystalline 73GeO 2 -8Al 2 o 3 -7P 2 o 5 -10Cs 2 LiYCl 6 -2TbCl 3 System glass film
[0060] For prepared Tb-containing 3+ Ion-doped Cs 2 LiYCl 6 The microcrystalline ...
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