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Thick coating polyether ether ketone composite coating and its preparation method and application

A technology of polyether ether ketone and composite coatings, which is applied in the direction of anti-corrosion coatings, coatings, and devices for coating liquid on the surface, etc. It can solve the problems of polyether ether ketone powder coatings such as sagging, and achieve excellent anti-corrosion performance and excellent spraying process. The effect of simplicity and simple preparation method

Active Publication Date: 2017-11-28
JILIN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The current problem is that too thick polyetheretherketone powder coatings will cause serious sagging when forming a coating

Method used

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  • Thick coating polyether ether ketone composite coating and its preparation method and application
  • Thick coating polyether ether ketone composite coating and its preparation method and application
  • Thick coating polyether ether ketone composite coating and its preparation method and application

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Polyether ether ketone containing alkyne group is synthesized by polymerization reaction, wherein x=0.1, y=0.9 in polyether ether ketone containing alkyne group; A solution is formed in formamide (DMF), and the mass percentage concentration of the solution is 1%; then the polyether ether ketone powder coating is added to the above solution for stirring or ultrasonic dispersion, wherein the average particle diameter of the polyether ether ketone powder coating is 30 μm , the melt index is 40g / 10min, the mass ratio of polyether ether ketone powder coating and alkyne group-containing polyetherether ketone solution is 1:1; the mixed solution is suction filtered and dried, dispersed to a particle size suitable for electrostatic spraying, Finally, a thick-coated polyether ether ketone composite coating is obtained.

Embodiment 2

[0030] The thick-coated polyetheretherketone composite coating prepared in Example 1 is used to prepare a polyetheretherketone thick coating, and the steps of the preparation method are as follows:

[0031] 1) Spray the thick-coated polyetheretherketone composite coating prepared in Example 1 on the conductive substrate by electrostatic spraying method;

[0032] 2) The substrate coated with the paint in step 1) is subjected to high temperature treatment, that is, the temperature is raised to 380° C. and maintained for 3 minutes;

[0033] 3) Recoating by thermal spraying method, that is, directly thermal spraying a thick-coated polyether ether ketone composite coating on the heat-treated substrate in step 2);

[0034] 4) Repeat the high-temperature treatment operation of step 2) for the base material obtained in step 3);

[0035] 5) If the coating thickness does not meet the requirements, repeat steps 3) and 4);

[0036] 6) The coating thickness meets the requirements, and th...

Embodiment 3

[0038]Polyether ether ketone containing alkyne group is synthesized by polymerization reaction, wherein x=0.5, y=0.5 in polyether ether ketone containing alkyne group; A solution is formed in acetamide (DMAC), and the mass percentage concentration of the solution is 10%; then the polyether ether ketone powder coating is added to the above solution for stirring or ultrasonic dispersion, wherein the average particle diameter of the polyether ether ketone powder coating is 150 μm , the melt index is 150g / 10min, the mass ratio of polyether ether ketone powder coating and alkyne group-containing polyetherether ketone solution is 20:1; the mixed solution is suction filtered and dried, dispersed to a particle size suitable for electrostatic spraying, Finally, a thick-coated polyether ether ketone composite coating is obtained.

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Abstract

The invention discloses a thick coating type polyether-ether-ketone composite coating and a preparation method and an application thereof, and belongs to the technical field of anti-corrosion coatings. The thick coating type polyether-ether-ketone composite coating is prepared from polyether-ether-ketone and alkynyl-containing polyether-ether-ketone as raw materials, and the thick coating type polyether-ether-ketone composite coating is sprayed on a conductive substrate by an electrostatic spraying method; the substrate coated with the coating is subjected to high-temperature treatment for 3-30 min at the temperature of 380-400 DEG C; the coating is repeatedly sprayed and recoated and subjected to high-temperature treatment by a thermal spraying method until the coating layer thickness meets requirements. The preparation methods of the thick coating type polyether-ether-ketone composite coating and a coating layer are simple, are convenient to operate, can be controlled reasonably, and are economical and practical; in the process of preparing the coating layer, a sagging phenomenon is avoided; the polyether-ether-ketone coating layer has excellent anticorrosion performance, can effectively reduce the corrosion of industrial equipment, improves the service life of industrial equipment, reduces the probability of accident generation due to equipment damage, thereby reducing the cost and saving resources.

Description

technical field [0001] The invention belongs to the technical field of anti-corrosion coatings, and in particular relates to a thick-coated polyetheretherketone composite coating and its preparation method and application. Background technique [0002] Corrosion of metal is usually the deterioration and destruction caused by chemical or electrochemical interaction with the surrounding medium in the natural environment or under working conditions. Generally speaking, the corrosion of steel and iron-based alloys is mainly rust, which is due to the formation of rust, a corrosion product mainly composed of hydrous iron oxide, under the action of water, oxygen and electrolytes in the environment. Applying anti-corrosion coatings is one of the most basic methods for metal anti-corrosion. The anti-corrosion coating is evenly and densely coated on the metal surface, and its shielding effect can effectively prevent the direct contact between the corrosive medium and the metal surfac...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D161/16C09D5/08C09D7/12C08G8/02B05D7/24
CPCB05D7/24C08G8/02C08L2205/025C09D5/08C09D7/65C09D161/16C08L61/16
Inventor 关绍巍张吉亮张云鹤李庆伟祝世洋
Owner JILIN UNIV