Reinforced and modified PBT (polybutylene terephthalate) material with epoxy resin bonding performance and preparation method for reinforced and modified PBT material
A technology of epoxy resin and adhesion, which is applied in the field of reinforced modified PBT materials and its preparation, can solve the problems of reduced packaging efficiency, difficulty in controlling the curing process of epoxy resin viscosity changes, etc., and achieve improved adhesion and excellent interface bonding effect
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[0029] Weighing: 70 kg of PBT, 18 kg of cardanolamine, 18 kg of polyvinyl alcohol microspheres, 6 kg of sodium dodecyl sulfonate, 6 kg of gelatin, 8 kg of reinforcing agent, 2 kg of calcium stearate, and toughening agent AX8900 2 kg;
[0030] The reinforcing agent comprises the following components in parts by weight: 2 parts of nano-zirconium carbide, 2 parts of aluminum titanate fiber, and 4 parts of halloysite nanotubes pretreated with a silane coupling agent.
[0031] Specific steps are as follows:
[0032] (1), preparation of microcapsule curing agent:
[0033] ①. Under stirring conditions, add 0.5wt% gelatin aqueous solution and 0.5wt% sodium dodecylsulfonate aqueous solution, and disperse for 40 minutes under mechanical stirring at 800 rpm to obtain an aqueous phase;
[0034] 2. In the dichloromethane solvent, add cardanolamine and polyvinyl alcohol microspheres, and disperse evenly in an ultrasonic instrument to obtain an oil phase, and gradually add the water phase ...
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