Dental composite-resin high-strength fiber periodontal bundle band and preparation method thereof
A technology of composite resin and high-strength fiber, which is applied in fiber type, fiber treatment, medical science, etc., can solve the problems of restricting the application of PBO fiber, the fiber is not easy to infiltrate, and the failure of treatment, so as to achieve good biological safety and aesthetic performance, and improve the overall The effect of improving mechanical strength and overall mechanical properties
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Embodiment 1
[0029] Example 1: Preparation of grooved high-strength fiber resin composite material
[0030] Raw materials: 2,5-dihydroxyterephthalic acid (MeTHPA, analytically pure); tetraaminopyridine trihydrochloride monohydrate (MeTHPA, analytically pure); polyphosphoric acid (MeTHPA, analytically pure); Phosphorus (MeTHPA, analytically pure); terephthalic acid; 4,6-diaminoresorcinol hydrochloride; silane coupling agent (Z-6040, Dow Corning, USA); bisphenol A glycidyl methacrylate Ester (Bis-GMA, chemically pure, Aldrich Company); Triethylene glycol dimethacrylate (TEGDMA, chemically pure, Aldrich Company); Catalyst camphorol (CQ, chemically pure, Aldrich Company); Initiate auxiliary agent N , N-dimethylaminoethyl methacrylate (DMAEMA, Aldrich); nano-TiO 2 (Particle size 25nm, Sigma company, USA).
[0031] (1) Preparation of PIPD / PBO blended fiber
[0032] A, preparation of PIPD / PPA polymer solution
[0033] Put 2,5-dihydroxyterephthalic acid, tetraaminopyridine trihydrochloride mon...
Embodiment 2
[0057] Example 2: Flexural properties and elastic modulus tests of four different periodontal fiber bands
[0058] Materials: Top 100 periodontal retaining fiber (French Blue Company), connect ultra-strong fiber band (Kerr Company in the United States), everStick PERIO (Finnish Stick Tech Company), self-made PBO composite resin high-strength fiber periodontal band, the selected models are all 5cm×2.5mm×0.15mm.
[0059] (1) For each group of 10 samples, use an electronic digital caliper to measure the width and height of each group of samples at three points, and calculate the average value to obtain the average width and height of the sample.
[0060] (2) According to the IS04049 standard, a three-point flexural strength test was carried out to test its flexural strength (MPa) and elastic modulus (GPa). Fix the specimen on the measuring platform and clamp it tightly. According to the product manual, use a curing light to cure the specimen. Keep the indoor temperature (22±1)°...
Embodiment 3
[0069] Example 3: Self-made periodontal bands for fixing loose teeth
[0070] Materials: loose tooth model, self-made periodontal fiber band, self-etching two-step bonding system (3MESPE, USA), flowable resin (3MESPE, USA), light curing machine (Destsply, Germany).
[0071] Prepare a periodontal band as follows:
[0072] (1) Measure the length of the required fiber bundle.
[0073] (2) Cut to get the required length.
[0074] (3) Apply the etchant for about 30 seconds, rinse thoroughly and dry.
[0075] (4) Apply adhesive on the surface of the acid-etched teeth, keep it for 15 seconds, then blow it with air for 3 seconds, and irradiate it with a light curing lamp for 20 seconds.
[0076] (5) Place the flowing resin about 2mm at the far end of one side, and then cover it with a fiber tape, and light-cure for 30 seconds.
[0077] (6) Coat the entire surface of the fiber tape with flowing resin, cure the entire surface, and polish.
[0078] The periodontal band prepared acco...
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