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Production method of light yellow quartz glass tube

The technology of a quartz glass tube and a production method, which is applied in the production field of light yellow quartz glass tube, can solve the problems of affecting the laser, high scrap rate, insufficient strength, etc., and achieve the effects of high material strength, improved strength, and high color purity.

Active Publication Date: 2017-05-31
连云港市盛昌照明电器有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Light yellow quartz tubes are mostly used in lasers, which can completely filter out ultraviolet rays in invisible light, avoid color centers and optical distortions in working substances, reduce corrosion of silver reflective layers, and greatly improve laser generation efficiency , but the production technology of the light yellow quartz glass tube is still not mature enough, the color of the quartz glass tube is not pure, it is prone to variegated colors, and there is a situation of insufficient strength, the scrap rate is high, and the use of the laser is affected, so a kind of color purity is invented The production method of light yellow quartz glass tube with high material strength has become extremely urgent

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The invention provides a technical solution, a production method of a light yellow quartz glass tube, the production method comprising the following steps:

[0025] S1, taking a quartz stone raw material with a SiO2 content of more than 99% and an impurity content of less than 20 ppm, crushing the quartz stone raw material to obtain a 60-mesh quartz stone material;

[0026] S2, move the quartz stone in S1 to the washing pool for the first time to remove impurities, wash away the sediment, dry the washed quartz stone, add sodium nitrate and potassium nitrate in a ratio of 1:2 to the quartz stone and Stirring, the weight of the sodium nitrate and potassium nitrate mixture is 0.020% of the quartz stone weight, to obtain the quartz stone mixture;

[0027] S3, putting the quartz stone mixture obtained in S2 into a roasting furnace, roasting at 800-1000°C for 1-2h, after the roasting is completed, quickly put the quartz block into pure water below 20°C for 50s, and let it cra...

Embodiment 2

[0034] The invention provides a technical solution, a production method of a light yellow quartz glass tube, the production method comprising the following steps:

[0035] S1, taking a quartz stone raw material with a SiO2 content of more than 99% and an impurity content of less than 20 ppm, crushing the quartz stone raw material to obtain a quartz stone material with a specification of 50 mesh;

[0036] S2, move the quartz stone in S1 to the washing pool for the first time to remove impurities, wash away the sediment, dry the washed quartz stone, add sodium nitrate and potassium nitrate in a ratio of 1:2 to the quartz stone and Stirring, the weight of the sodium nitrate and potassium nitrate mixture is 0.010% of the quartz stone weight, to obtain the quartz stone mixture;

[0037] S3, put the mixed quartz stone material obtained in S2 into a roasting furnace, and roast it at 800°C for 1-2h. The final quartz stone is put into a pulverizer for fine powder to obtain 150 mesh qu...

Embodiment 3

[0044] The invention provides a technical solution, a production method of a light yellow quartz glass tube, the production method comprising the following steps:

[0045] S1, taking a quartz stone raw material with a SiO2 content of more than 99% and an impurity content lower than 20 ppm, crushing the quartz stone raw material to obtain a quartz stone material with a specification of 70 mesh;

[0046] S2, move the quartz stone in S1 to the washing pool for the first time to remove impurities, wash away the sediment, dry the washed quartz stone, add sodium nitrate and potassium nitrate in a ratio of 1:2 to the quartz stone and Stirring, the weight of the sodium nitrate and potassium nitrate mixture is 0.020% of the quartz stone weight, to obtain the quartz stone mixture;

[0047] S3, put the mixed quartz stone material obtained in S2 into a roasting furnace, and roast it at 1000°C for 1-2h. The final quartz stone is put into a pulverizer for fine powder to obtain 200 mesh qua...

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Abstract

The invention discloses a production method of a light yellow quartz glass tube. The production method comprises the following steps: (S1) taking a quartzite raw material containing over 99% of SiO2 and lower than 20ppm of impurities, and breaking the quartzite raw material to obtain a quartzite material of 50-70 meshes; and (S2) transferring the quartzite in the step (S1) into a flushing tank for primary cleaning, flushing off the sediment, and airing the flushed quartzite material; and adding sodium nitrate and potassium nitrate in a ratio of 1:2 into the quartzite material and stirring to obtain a quartzite mixed material. According to the invention, a solution A is prepared by adding hydrochloric acid into europium oxide, vanadium pentoxide, yttrium oxide, praseodymium oxide and lanthanum oxide in (S5); a solution B is prepared by adding water into sodium nitrate and ammonium metavanadate; and the solution A and solution B are mixed and roasted with the quartzite material, the quartzite material is fully colored, mixed color is avoided, and a quartz glass tube with high-purity color can be obtained.

Description

technical field [0001] The invention relates to the technical field, in particular to a production method of a light yellow quartz glass tube. Background technique [0002] Quartz glass tube is a special industrial technical glass made of silica. It is a very good basic material (silicon content 9999). Quartz glass has a series of excellent physical and chemical properties, such as: [0003] 1. High temperature resistance. The softening point temperature of quartz glass is about 1730°C, and it can be used for a long time at 1100°C, and the highest service temperature for a short time can reach 1450°C. 2. Corrosion resistance. In addition to hydrofluoric acid, quartz glass hardly reacts with other acids, and its acid resistance is 30 times that of ceramics and 150 times that of stainless steel, especially its chemical stability at high temperatures, which cannot be achieved by any other engineering materials. In comparison, 3. Good thermal stability. The thermal expansion ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C4/02C03C3/06C03C1/04C03C1/02
CPCC03C1/026C03C1/04C03C3/06C03C4/02
Inventor 孙国方沈敏
Owner 连云港市盛昌照明电器有限公司
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