Negative-ion, far-infrared, antibacterial and anti-mite compound polyester fibers and manufacturing method thereof
A polyester fiber and far-infrared technology, applied in the field of polyester fiber, can solve the problems of particle size reduction and ineffective effect, and achieve the effect of improving dispersibility, inhibiting agglomeration, and solving the problem of nano-agglomeration.
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[0040] During the preparation of the additive carrier, the pollen was soaked twice in the precursor solution to ensure that the pollen was covered with a uniform layer of TiO 2 Floor;
[0041] Titanium dioxide is a semiconductor material with stable chemical properties. It generally exhibits photocatalytic performance. It is used in photocatalytic self-cleaning materials, or in papermaking, rubber and other products, and is used as a filler and colorant. In this application, it is used TiO was prepared by hydrothermal method using pollen as template 2 Hollow spheres are creatively used as additive carriers. Thanks to their special surface structure, they play a key role in the application of negative ions, far-infrared, antibacterial and mite-removing effects of composite polyester fibers.
[0042] Step 2, prepare negative ion additive
[0043] Add the additive carrier, tourmaline anion powder, and titanate coupling agent into the deionized water, stir well to obtain anion a...
Embodiment 1
[0055] Step 1, preparation of additive carrier
[0056] First, rapeseed flower pollen with a diameter of 50 μm was screened out, 20 g was rinsed with alcohol, and dried; then, 9 g of Ti(SO 4 ) 2 , stirred for 20min, then added 1.2g of ammonium fluoride and 3.8g of urea to the above-mentioned deionized water, stirred for 60min, then added 20g of rape pollen to the above-mentioned deionized water, stirred for 20min, and transferred the above-mentioned deionized water to the hydrothermal In the kettle, it was hydrothermally reacted at 180°C for 20h. After the reaction, the white precipitate in the hydrothermal kettle was collected, cleaned, dried in a drying oven at 60°C for 15h, and then put into a muffle furnace. Anneal at 460°C for 2 hours, anneal at 490°C for 1 hour, and the heating rate is 2°C / min. During the annealing process, the pollen particles will be removed. After the annealing, TiO 2 Hollow sphere is the additive carrier;
[0057] During the preparation of the add...
Embodiment 2
[0069] Step 1, preparation of additive carrier
[0070] First, rapeseed flower pollen with a diameter of 50 μm was screened out, 20 g was rinsed with alcohol, and dried; then, 9 g of Ti(SO 4 ) 2 , stirred for 20min, then added 1.2g of ammonium fluoride and 3.8g of urea to the above-mentioned deionized water, stirred for 60min, then added 20g of rape pollen to the above-mentioned deionized water, stirred for 20min, and transferred the above-mentioned deionized water to the hydrothermal In the kettle, it was hydrothermally reacted at 180°C for 20h. After the reaction, the white precipitate in the hydrothermal kettle was collected, cleaned, dried in a drying oven at 60°C for 15h, and then put into a muffle furnace. Anneal at 460°C for 2 hours, anneal at 490°C for 1 hour, and the heating rate is 2°C / min. During the annealing process, the pollen particles will be removed. After the annealing, TiO 2 Hollow sphere is the additive carrier;
[0071] During the preparation of the add...
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