Graphene nano composite material and preparation method thereof

A nano-composite material and graphene technology, which is applied in the field of graphene nano-composite materials and its preparation, can solve the problems of poor mechanical properties of graphene-graphene nano-composite materials, and achieve the goal of improving adhesion, reducing wear and improving dispersibility Effect

Inactive Publication Date: 2017-10-13
成都玺旺科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] Aiming at the above-mentioned deficiencies in the prior art, the present invention provides a graphene nanocomposite material and a preparation method thereof, whi

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] A kind of graphene nanocomposite material, its preparation method comprises the following steps:

[0030] (1) Disperse graphite oxide in water under ultrasonic treatment conditions to obtain a uniformly dispersed graphite oxide suspension with a concentration of 1 mg / mL;

[0031] Among them, graphite oxide is prepared by the following method: at 0°C, slowly add 1 g of graphite to 25 mL of 95% concentrated sulfuric acid under stirring, stir for 20 min, then add 0.8 sodium nitrate, stir for 20 min, then add 4 g of high Potassium manganate, stirred and reacted for 1.5h, then moved into a 35°C constant temperature water bath, stirred and reacted for 60min, then added 50mL of deionized water, raised the temperature to 95°C, reacted for 30min, then added dropwise 120mL of 10% H 2 o 2 , Stir the reaction until the color of the system turns from golden yellow to black, add 50mL of 0.5mol / L HCl, stir for 10min, then filter with suction, wash the filter cake with 0.5mol / L HCl un...

Embodiment 2

[0037] A kind of graphene nanocomposite material, its preparation method comprises the following steps:

[0038] (1) Disperse graphite oxide in water under ultrasonic treatment conditions to obtain a uniformly dispersed graphite oxide suspension with a concentration of 2.5 mg / mL;

[0039]Among them, graphite oxide is prepared by the following method: at 0°C, slowly add 1 g of graphite to 25 mL of 95% concentrated sulfuric acid under stirring, stir for 20 min, then add 0.8 sodium nitrate, stir for 20 min, then add 4 g of high Potassium manganate, stirred and reacted for 1.5h, then moved into a 35°C constant temperature water bath, stirred and reacted for 60min, then added 50mL of deionized water, raised the temperature to 95°C, reacted for 30min, then added dropwise 120mL of 10% H 2 o 2 , Stir the reaction until the color of the system turns from golden yellow to black, add 50mL of 0.5mol / L HCl, stir for 10min, then filter with suction, wash the filter cake with 0.5mol / L HCl u...

Embodiment 3

[0045] A kind of graphene nanocomposite material, its preparation method comprises the following steps:

[0046] (1) Disperse graphite oxide in water under ultrasonic treatment conditions to obtain a uniformly dispersed graphite oxide suspension with a concentration of 1.5 mg / mL;

[0047] Among them, graphite oxide is prepared by the following method: at 0°C, slowly add 1 g of graphite to 25 mL of 95% concentrated sulfuric acid under stirring, stir for 20 min, then add 0.8 sodium nitrate, stir for 20 min, then add 4 g of high Potassium manganate, stirred and reacted for 1.5h, then moved into a 35°C constant temperature water bath, stirred and reacted for 60min, then added 50mL of deionized water, raised the temperature to 95°C, reacted for 30min, then added dropwise 120mL of 10% H 2 o 2 , Stir the reaction until the color of the system turns from golden yellow to black, add 50mL of 0.5mol / L HCl, stir for 10-2min, then filter with suction, wash the filter cake with 0.5mol / L HC...

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Abstract

The invention discloses a graphene nano composite material. The preparation method of the graphene nano composite material comprises the following steps: (1) preparing a graphite oxide suspension; (2) performing a reaction on the graphite oxide suspension and a copper lysine complex, adding hydrazine hydrate and NaBH4, and performing reduction; (3) adding disodium EDTA to remover copper; (4) mixing the product obtained in the step (3), an E-42 epoxy resin, ethylene glycol diglycidyl ether, poly(ethylene glycol) diglycidyl ether, KH560 and nano boehmite, and performing ultrasonic dispersion; and (5) performing a reaction on the product obtained in the step (4), C12-C14 aliphatic glycidyl ethers, nano titanium dioxide, glass microspheres and camphor at 70-80 DEG C for 2-3 hours. The graphene nano composite material disclosed by the invention effectively solves the problem of dispersity in graphene; the adhesive force, wear resistance and antibacterial effect of the composite material are enhanced; and the graphene nano composite material can be used for preparing environment-friendly paints.

Description

technical field [0001] The invention belongs to the technical field of graphene composite materials, and in particular relates to a graphene nanocomposite material and a preparation method thereof. Background technique [0002] Graphene is a new type of carbonaceous material in which a single layer of carbon atoms is arranged in a two-dimensional honeycomb lattice structure. It is considered to be the basic unit of all other dimensional carbonaceous materials, such as fullerenes that can be packed into zero dimensions. , rolled into one-dimensional carbon nanotubes, stacked into three-dimensional graphite, etc. Graphene is made of carbon atoms with sp 2 The monoatomic carbon layer formed by hybridization has a very stable structure and has excellent mechanical properties, peculiar electrical properties and good thermal properties. However, when preparing graphene nanocomposites, due to the superhydrophobicity of the graphene surface and the inherent van der Waals force bet...

Claims

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Application Information

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IPC IPC(8): C08L63/00C08K13/04C08K3/04C08K3/22C08K7/20C08K5/5435C09D163/00C09D5/14C09D7/12C01B32/184C01B32/19C01B32/194B82Y30/00B82Y40/00
CPCC08K13/04B82Y30/00B82Y40/00C08K3/04C08K3/22C08K5/5435C08K7/20C08K2003/2227C08K2003/2241C08K2201/011C09D5/14C09D163/00C08L63/00
Inventor 黄俊尹振宇
Owner 成都玺旺科技有限公司
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