Zinc stearate sol low in free acid content and preparation method thereof
A technology of stearic acid and acid content, applied in the directions of carboxylate preparation, carboxylate preparation, chemical instruments and methods, etc., can solve the problems of limited water catalytic activity, incomplete reaction, high free acid content, and achieve process control Simplified, no safety risk, high yield
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[0039] Example 1
[0040] A zinc stearate sol with low free acid content. The zinc stearate sol with low free acid content is prepared from a pre-prepared stearic acid emulsion and zinc oxide dispersion in the presence of a multifunctional catalyst primary amine. Obtained by reaction at a model temperature of 2°C;
[0041] The weight percentages of stearic acid emulsion and zinc oxide dispersion are:
[0042] Starting material stearic acid emulsion: 86.7%, of which
[0043] Stearic acid: 28%
[0044] Surfactant A: 1.8%
[0045] Surfactant B: 2.3%
[0046] Surfactant C: 4.5%
[0047] Defoamer: 0.1%
[0048] Deionized water: 50.0%
[0049] Zinc oxide dispersion: 13.3, of which
[0050] Zinc oxide: 4%
[0051] Dispersant: 1%
[0052] Multifunctional catalyst: 0.1%
[0053] Defoamer: 0.1%
[0054] Environmental protection fungicide: 0.1%
[0055] Deionized water: 8%
[0056] The present invention also provides a method for preparing zinc stearate sol with low free acid content, which includes the foll...
Example Embodiment
[0061] Example 2
[0062] A zinc stearate sol with low free acid content. The zinc stearate sol with low free acid content is prepared from a pre-prepared stearic acid emulsion and zinc oxide dispersion in the presence of a multifunctional catalyst primary amine. Obtained by reaction at a model temperature of 2°C;
[0063] The weight percentages of stearic acid emulsion and zinc oxide dispersion are:
[0064] Starting material stearic acid emulsion: 84%, of which
[0065] Stearic acid: 28%
[0066] Surfactant A: 1.5%
[0067] Surfactant B: 2.5%
[0068] Surfactant C: 4%
[0069] Defoamer: 0.1%
[0070] Deionized water: 47.9%
[0071] Zinc oxide dispersion: 16, of which
[0072] Zinc oxide: 4.5%
[0073] Dispersant: 1.0%
[0074] Multifunctional catalyst: 0.3%
[0075] Defoamer: 0.1%
[0076] Environmental protection fungicide: 0.1%
[0077] Deionized water: 10%
[0078] The present invention also provides a method for preparing zinc stearate sol with low free acid content, which includes the follo...
Example Embodiment
[0083] Example 3
[0084] A zinc stearate sol with low free acid content. The zinc stearate sol with low free acid content is prepared from a pre-prepared stearic acid emulsion and zinc oxide dispersion in the presence of a multifunctional catalyst primary amine. Obtained by reaction at a model temperature of 2°C;
[0085] The weight percentages of stearic acid emulsion and zinc oxide dispersion are:
[0086] Starting material stearic acid emulsion: 85% of which
[0087] Stearic acid: 28%
[0088] Surfactant A: 1.0%
[0089] Surfactant B: 2.0%
[0090] Surfactant C: 4.0%
[0091] Defoamer: 0.2%
[0092] Deionized water: 49.8%
[0093] Zinc oxide dispersion: 15, of which
[0094] Zinc oxide: 4%
[0095] Dispersant: 1%
[0096] Multifunctional catalyst: 0.2%
[0097] Defoamer: 0.2%
[0098] Environmental protection fungicide: 0.2%
[0099] Deionized water: 9.4%
[0100] The present invention also provides a method for preparing zinc stearate sol with low free acid content, which includes the followi...
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