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Zinc stearate sol low in free acid content and preparation method thereof

A technology of stearic acid and acid content, applied in the directions of carboxylate preparation, carboxylate preparation, chemical instruments and methods, etc., can solve the problems of limited water catalytic activity, incomplete reaction, high free acid content, and achieve process control Simplified, no safety risk, high yield

Inactive Publication Date: 2017-10-17
江苏三瑞生物技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The advantage is that water is used as the catalyst, and there is no generation of three wastes; the disadvantage is that the catalytic activity of water is limited, the reaction cannot be complete, the content of free acid is high, and the viscosity of the finished product is too high, which limits its application range

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] A kind of zinc stearate sol of low free acid content, the zinc stearate sol of described low free acid content is by krfft× obtained by reacting at a model temperature of 2°C;

[0041] The weight percentages of stearic acid emulsion and zinc oxide dispersion liquid are respectively:

[0042] Starting material stearic acid emulsion: 86.7%, of which

[0043] Stearic acid: 28%

[0044] Surfactant A: 1.8%

[0045] Surfactant B: 2.3%

[0046] Surfactant C: 4.5%

[0047] Defoamer: 0.1%

[0048] Deionized water: 50.0%

[0049] Zinc oxide dispersion: 13.3, of which

[0050] Zinc Oxide: 4%

[0051] Dispersant: 1%

[0052] Multifunctional catalyst: 0.1%

[0053] Defoamer: 0.1%

[0054] Environmental fungicide: 0.1%

[0055] Deionized water: 8%

[0056] The present invention also provides a kind of preparation method of zinc stearate sol with low free acid content, comprises the steps:

[0057]Step 1: In a multi-functional reactor, first put stearic acid into the mel...

Embodiment 2

[0062] A kind of zinc stearate sol of low free acid content, the zinc stearate sol of described low free acid content is by krfft× obtained by reacting at a model temperature of 2°C;

[0063] The weight percentages of stearic acid emulsion and zinc oxide dispersion liquid are respectively:

[0064] Starting material stearic acid emulsion: 84%, of which

[0065] Stearic acid: 28%

[0066] Surfactant A: 1.5%

[0067] Surfactant B: 2.5%

[0068] Surfactant C: 4%

[0069] Defoamer: 0.1%

[0070] Deionized water: 47.9%

[0071] Zinc oxide dispersion: 16, of which

[0072] Zinc Oxide: 4.5%

[0073] Dispersant: 1.0%

[0074] Multifunctional catalyst: 0.3%

[0075] Defoamer: 0.1%

[0076] Environmental fungicide: 0.1%

[0077] Deionized water: 10%

[0078] The present invention also provides a kind of preparation method of zinc stearate sol with low free acid content, comprises the steps:

[0079] Step 1: In the multifunctional reactor, first put stearic acid into the me...

Embodiment 3

[0084] A kind of zinc stearate sol of low free acid content, the zinc stearate sol of described low free acid content is by krfft× obtained by reacting at a model temperature of 2°C;

[0085] The weight percentages of stearic acid emulsion and zinc oxide dispersion liquid are respectively:

[0086] Starting material stearic acid emulsion: 85%, of which

[0087] Stearic acid: 28%

[0088] Surfactant A: 1.0%

[0089] Surfactant B: 2.0%

[0090] Surfactant C: 4.0%

[0091] Defoamer: 0.2%

[0092] Deionized water: 49.8%

[0093] Zinc oxide dispersion: 15, of which

[0094] Zinc Oxide: 4%

[0095] Dispersant: 1%

[0096] Multifunctional catalyst: 0.2%

[0097] Defoamer: 0.2%

[0098] Environmental fungicide: 0.2%

[0099] Deionized water: 9.4%

[0100] The present invention also provides a kind of preparation method of zinc stearate sol with low free acid content, comprises the steps:

[0101] Step 1: In the multi-functional reactor, first put stearic acid into the me...

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PUM

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Abstract

The invention discloses zinc stearate sol low in free acid content and a preparation method thereof. The zinc stearate sol is prepared by reaction under model temperature of krfft*2 DEG C. The zinc stearate sol comprises, by weight percentage, 86.7% of stearic acid emulsion and 13.3% of zinc oxide dispersion liquid, wherein the zinc oxide dispersion liquid comprises, by weight percentage, 4% of zinc oxide, 1% of dispersing agent, 0.1% of multifunctional catalyst, 0.1% of defoaming agent, 0.1% of environment-friendly sterilizing agent and 8% of deionized water. The preparation method has the advantages that the reaction is complete, the generation of three wastes is avoided, reaction byproducts are avoided, the prepared zinc stearate sol is low in free fatty acid content, pure in component and small in particle size, and the low viscosity of high-solid-content products is guaranteed; independent catalyst pollution is avoided, and low fatty acid residues are achieved; the conversion rate and fineness of zinc stearate are increased; the method is high in yield, minimum in energy consumption and simplified in process control, and the prepared zinc stearate sol is low in particle size distribution.

Description

technical field [0001] The invention relates to the technical field of camellia oleifera, in particular to a zinc stearate sol with low free acid content and a preparation method. Background technique [0002] Zinc stearate is a widely used fine chemical material, but its application is limited due to its strong hydrophobicity. Zinc stearate sol is a water-soluble product that expands applications and improves use efficiency, and is widely used in rubber, plastics, coatings, inks, paints, thermal paper, cosmetics and other industries. At present, my country's coatings, papermaking, and cosmetics industries, which consume a large amount and have high quality requirements, almost use imported products from Japan and Germany. The prices are relatively high, and there is no room for negotiation on prices. The reason is that imported products have low free acid content, good dispersibility, small particle size, high effective content, pure ingredients, and stable and reliable qu...

Claims

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Application Information

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IPC IPC(8): C07C51/41C07C53/126D21H21/14C09D7/12C08K5/098A61K8/36A61Q19/00
CPCA61K8/361A61K2800/10A61Q19/00C07C51/412C08K5/098D21H21/14C07C53/126
Inventor 叶洲许宏涛周颖顾浩
Owner 江苏三瑞生物技术有限公司
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