Preparing method for oxygen-free copper belt used for solar cell module
A technology of solar cells and oxygen-free copper, applied in the direction of liquid chemical plating, coating, metal material coating process, etc., can solve the problems of serious surface oxidation, uneven thickness, easy discoloration of tin-plated copper strips, etc., to prevent Oxidation, high purity effect
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example 1
[0019] Weigh 2kg of red copper sheet and cut it into small pieces of 3cm×1cm. Place the cut pieces in a beaker filled with 2L hydrochloric acid with a mass fraction of 15%. After soaking for 40min, filter to obtain filter residue. After washing with ethanol for 5 times, put the cleaned filter residue in a tube furnace with an induction furnace connected to the valve at the end, and then use an air pump to evacuate the tube furnace to a vacuum of 1.5kPa. Inject argon, control the rate of argon inflow to 100mL / min, and let it in for 20min. Into the light atomic weight gas for 10 to 15 minutes, and after vacuuming the vacuum induction furnace to 80Pa, open the valve at the end of the tube furnace to allow the gas in the tube furnace to enter the vacuum induction furnace for 15 minutes, then close the tube furnace The valve at the end allows the gas to be cooled into powder in the vacuum induction furnace, and then the vacuum induction furnace is programmed to heat up to 1200°C at...
example 2
[0021]Weigh 1 kg of red copper sheet and cut it into small pieces of 3cm×1cm. Place the cut pieces in a beaker filled with 1L hydrochloric acid with a mass fraction of 15%. After soaking for 30 minutes, filter to obtain the filter residue. After washing with ethanol for 3 times, put the cleaned filter residue in a tube furnace with an induction furnace connected to the valve at the end, and then use an air pump to evacuate the tube furnace to a vacuum degree of 1.3kPa, and then pass it into the tube furnace. Inject nitrogen, control the rate of nitrogen inflow to 100mL / min, and pass in for 15min. After the nitrogen inflow is completed, heat the tube furnace to 1800°C, keep warm for 20min, and continue to flow in the tube furnace at a rate of 100mL / min. Nitrogen for 10 minutes, and after vacuuming the vacuum induction furnace to 60Pa, open the valve at the end of the tube furnace to allow the gas in the tube furnace to enter the vacuum induction furnace for 10 minutes, then clos...
example 3
[0023] Weigh 2kg of red copper sheet and cut it into small pieces of 3cm×1cm. Place the cut pieces in a beaker filled with 1L of hydrochloric acid with a mass fraction of 15%. After soaking for 35min, filter to obtain the filter residue. After washing with ethanol for 4 times, put the cleaned filter residue in a tube furnace with an induction furnace connected to the valve at the end, and then use an air pump to vacuumize the tube furnace to a vacuum of 1.4kPa, and then pass it into the tube furnace. Inject nitrogen, control the rate of nitrogen inflow to 100mL / min, and let it in for 17min. After the inflow of nitrogen is over, heat the tube furnace to 1850°C, keep it warm for 25min, and continue to feed in the tube furnace at a rate of 100mL / min. Argon for 12 minutes, and after vacuuming the vacuum induction furnace to 70Pa, open the valve at the end of the tube furnace to allow the gas in the tube furnace to enter the vacuum induction furnace. After 12 minutes, close the valv...
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