Preparation method of adsorption type biological enzyme soaping agent for reactive dyes

A reactive dye and adsorption-type technology, applied in the direction of non-surface active detergent composition, detergent compounding agent, chemical equipment and methods, etc., can solve the problems of reduced soaping effect, stripping, and excessive foaming, etc., to prevent re- The effects of staining fabrics, reducing washing water consumption, and removing residual floating colors

Inactive Publication Date: 2017-11-24
朱文杰
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The main technical problem to be solved by the present invention is that traditional soaping agents have stripping phenomenon, which greatly reduces the soaping effect, and surfactant soaping agents have more foams, which are difficult to wash off during the printing and dyeing process, and need to consume a lot of water for washing , the defect of large energy consumption, a preparation method of an adsorption-type biological enzyme soaping agent for reactive dyes is provided

Method used

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  • Preparation method of adsorption type biological enzyme soaping agent for reactive dyes

Examples

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Effect test

example 1

[0020] Weigh 50g ammonium chloride, 1.5g potassium dihydrogen phosphate, 1.0g copper sulfate pentahydrate, 1g sodium chloride, 0.8g magnesium sulfate, 100g bran, 10g corn flour, 15g sucrose, 0.5g calcium chloride, add 1.0 In L deionized water, stir at 200r / min for 20min to obtain a fermentation medium, then adjust the pH of the medium to 9.0 with a mass fraction of 1% sodium hydroxide solution, and inoculate the white rot fungus into the fermentation medium according to the inoculum size of 10%. At 30°C, shake and ferment at 200r / min for 8 days, then add 9L of deionized water, shake at 28°C at 200r / min for 2h to obtain a fermentation broth, then place the fermentation broth in a high-speed centrifuge, Centrifuge at 10000r / min for 8min, collect the supernatant to obtain a crude enzyme solution, then add 2.0L tert-butanol and 200g ammonium sulfate to the crude enzyme solution, let it stand at 25°C for 1h, then transfer it to a centrifuge, / min centrifuge for 12min, collect the p...

example 2

[0021]Weigh 53g ammonium chloride, 1.8g potassium dihydrogen phosphate, 1.1g copper sulfate pentahydrate, 1g sodium chloride, 0.9g magnesium sulfate, 110g bran, 11g corn flour, 18g sucrose, 0.7g calcium chloride, add 1.1 In L deionized water, stir at 250r / min for 25min to obtain a fermentation medium, then adjust the pH of the medium to 9.3 with a mass fraction of 1% sodium hydroxide solution, and inoculate the white rot fungus into the fermentation medium according to the inoculum size of 13%. At 31°C, shake and ferment at 220r / min for 9 days, then add 9L of deionized water, and shake at 220r / min for 2h at 29°C to obtain a fermented liquid, then place the fermented liquid in a high-speed centrifuge, Centrifuge at 11000r / min for 9min, collect the supernatant to obtain a crude enzyme solution, then add 2.2L tert-butanol and 210g ammonium sulfate to the crude enzyme solution, let it stand at 28°C for 1h, then transfer it to a centrifuge, / min centrifuge for 14min, collect the pr...

example 3

[0022] Weigh 55g ammonium chloride, 2.0g potassium dihydrogen phosphate, 1.2g copper sulfate pentahydrate, 2g sodium chloride, 1.0g magnesium sulfate, 120g bran, 12g corn flour, 20g sucrose, 0.8g calcium chloride, add 1.2 Stir in L deionized water for 30 min at 300 r / min to obtain a fermentation medium, then adjust the pH of the medium to 9.5 with a mass fraction of 1% sodium hydroxide solution, and inoculate the white rot fungus into the fermentation medium according to the inoculum size of 15%. At 32°C, shake and ferment at 240r / min for 10 days, then add 10L of deionized water, and shake at 240r / min for 3h at 30°C to obtain a fermented liquid, then place the fermented liquid in a high-speed centrifuge, Centrifuge at 12000r / min for 10min, collect the supernatant to obtain a crude enzyme solution, then add 2.4L tert-butanol and 220g ammonium sulfate to the crude enzyme solution, let it stand at 30°C for 2h, then transfer it to a centrifuge, / min centrifuge for 15min, collect t...

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Abstract

The invention discloses a preparation method of an adsorption type biological enzyme soaping agent for reactive dyes, belonging to the technical field of preparation of printing and dyeing auxiliary agents. The preparation method comprises the following steps of firstly, culturing and fermenting white-rot fungi by using a homemade fermentation medium, centrifuging the prepared fermented liquid to obtain crude enzyme liquid, and then preparing alkaline laccase by taking the crude enzyme liquid as a raw material; preparing a wool keratin solution by taking wool as a raw material, modifying the prepared wool keratin solution, then mixing the modified solution with the alkaline laccase, Tween-80/liquid paraffin, and the like, and carrying out centrifugal separation; after that, collecting precipitate, and washing the precipitate with acetone and isopropyl alcohol; finally, drying to obtain the adsorption type biological enzyme soaping agent for the reactive dyes. The soaping agent prepared by the method has a better soaping effect and a better anti-staining effect, thus enabling the color fastness to soaping and fastness to rubbing of fabrics subjected to soaping to reach three-level or above; furthermore, the soaping agent provided by the invention does not generate foam in a soaping process, so that the washing times of the fabrics can be reduced, and the energy consumption is greatly reduced.

Description

technical field [0001] The invention discloses a preparation method of an adsorption-type biological enzyme soaping agent for reactive dyes, and belongs to the technical field of preparation of printing and dyeing auxiliaries. Background technique [0002] There are unfixed or hydrolyzed dyes (often called floating colors), size and chemical auxiliaries on the surface of the fabric after dyeing or printing. If these dyes, sizing agents and chemical auxiliaries are not removed, the color fastness and vividness of the fabric will be affected, so the dyed fabric must be soaped, and as a post-processing aid in the printing and dyeing process, soaping Agents play an important role in the soaping process. [0003] In the soaping process, the soaping agent reacts chemically with the dye to wash away the reactive dye that is not firmly combined with the fiber and remove the printing paste, and at the same time prevent the removed dye from sticking to the cloth surface, so as to imp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11D7/46C11D7/42D06L4/40
CPCC11D3/38672C11D7/46D06L4/40
Inventor 许双健王之霖潘宏梅
Owner 朱文杰
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