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Preparation method of composite nano conductive material

A nano-conductive and distilled water technology is applied in the field of preparation of composite nano-conductive materials, which can solve the problems of undetermined lattice structure and difficult control of nano-conductive material processing, and achieve the effects of easy processing and excellent conductivity.

Inactive Publication Date: 2017-12-22
原晋波
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In recent years, nano-conductive materials have also been included in the scope of nano-material research, but the processing of nano-conductive materials is not easy to control, and there is no definite lattice structure. Therefore, a lot of research is still needed to control and improve it.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of composite nano conductive material, comprising the following steps:

[0020] Step 1: Mix 2 parts of copper chloride, 1 part of aluminum trichloride, 1 part of calcium chloride, 1 part of ferric chloride hexahydrate and 80 parts of ethylene glycol, and use a magnetic stirrer at a speed of 200r / Add 7 parts of anhydrous sodium acetate and 2 parts of polyethylene glycol while stirring under min, and continue stirring for 30 minutes;

[0021] Step 2: Add it into a polytetrafluoroethylene inner kettle, react at 220°C for 7 hours, wash with distilled water and ethanol respectively, put it in an oven to dry, and obtain product A;

[0022] Step 3: Mix and stir 0.2 parts of nano-zinc oxide, 0.3 parts of polysorbate-80, 0.2 parts of diisooctyl sodium sulfosuccinate, 0.1 parts of lauroyl diethanolamine and 80 parts of distilled water, add product A, put into ultrasonic Ultrasonic dispersion was carried out in the instrument for 2 hours;

[0023] Step 4: S...

Embodiment 2

[0027] A preparation method of composite nano conductive material, comprising the following steps:

[0028] Step 1: Mix 2.5 parts of copper chloride, 1.5 parts of aluminum trichloride, 1.5 parts of calcium chloride, 1.5 parts of ferric chloride hexahydrate and 85 parts of ethylene glycol, and use a magnetic stirrer at a speed of 250 r / Add 8 parts of anhydrous sodium acetate and 2.5 parts of polyethylene glycol while stirring under min, and continue stirring for 35 minutes;

[0029] Step 2: Add it into a polytetrafluoroethylene inner kettle, react at 225°C for 7.5 hours, wash with distilled water and ethanol respectively, put it in an oven to dry, and obtain product A;

[0030] Step 3: Mix and stir 0.3 parts of nano-zinc oxide, 0.4 parts of polysorbate-80, 0.25 parts of diisooctyl sodium sulfosuccinate, 0.15 parts of lauroyl diethanolamine and 90 parts of distilled water, add product A, and put into ultrasonic Ultrasonic dispersion was carried out in the instrument for 2.5 ho...

Embodiment 3

[0035] A preparation method of composite nano conductive material, comprising the following steps:

[0036] Step 1: Mix 3 parts of copper chloride, 2 parts of aluminum trichloride, 1.5 parts of calcium chloride, 1.5 parts of ferric chloride hexahydrate and 90 parts of ethylene glycol, and use a magnetic stirrer at a speed of 300r / s after ultrasonication for 25 minutes Add 8 parts of anhydrous sodium acetate and 2.5 parts of polyethylene glycol while stirring under min, and continue stirring for 35 minutes;

[0037] Step 2: Add it into a polytetrafluoroethylene inner kettle, react at 230°C for 8 hours, wash with distilled water and ethanol respectively, put it in an oven to dry, and obtain product A;

[0038] Step 3: Mix and stir 0.35 parts of nano-zinc oxide, 0.5 parts of polysorbate-80, 0.3 parts of diisooctyl sodium sulfosuccinate, 0.2 parts of lauroyl diethanolamine and 100 parts of distilled water, add product A, put into ultrasonic Ultrasonic dispersion was carried out i...

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Abstract

The invention provides a preparation method of a composite nano conductive material. The preparation method comprises the following steps: ultrasonically stirring copper chloride, aluminum trichloride, calcium chloride, ferric chloride hexahydrate and ethylene glycol, and then adding anhydrous sodium acetate and polyethylene glycol; adding polytetrafluoroethylene to perform reaction in a kettle, and performing washing and drying to obtain a product A; mixing and stirring nano-zinc oxide, polysorbate-80, dioctyl sodium sulfosuccinate, lauryl diethanolamine and distilled water, adding the product A, and performing ultrasonic dispersion; stopping stirring, standing, adding dist coconut fatty acid, phytic acid and pyrrole monomer, performing stirring reaction after cooling, and performing filtering, washing and drying to obtain a product B; mixing the product B and the distilled water, adding pentacarbonyl iron, piperidine and ammonium metavanadate, adding formic acid under a water bath, performing stirring reaction, and performing filtering, washing and drying to obtain the composite nano conductive material. The material prepared by using the preparation method of the composite nano conductive material is easy to process, and excellent in electrical conductivity, and has a potential application value to an electric sensor, a solar cell and a super-capacitor.

Description

technical field [0001] The invention relates to a preparation method of a composite nano conductive material. Background technique [0002] Nanotechnology is a technology that has emerged in recent years and has broad development prospects. It has been used in medicine, chemistry, electronic information and machinery to a certain extent. Nanotechnology refers to the science and technology of manufacturing substances with single atoms and molecules, and studies the properties and applications of materials with structural sizes ranging from 0.1 to 100 nanometers. The so-called nanomaterials refer to materials that have at least one dimension in the three-dimensional space that is in the nanometer size (0.1-100 nm) or composed of them as basic units, which is approximately equivalent to the scale of 10-100 atoms closely arranged together. Because its size is close to the coherence length of electrons, its properties have changed greatly due to the self-organization brought abo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L71/02C08K13/02C08K3/16C08K3/22C08K5/42C08K3/18C08K5/3435
CPCC08L71/02C08K2003/162C08K2003/164C08K2003/2296C08K2201/001C08K2201/011C08K2201/014C08L2203/20C08L2205/025C08K13/02C08K3/16C08K3/22C08K5/42C08K3/18C08K5/3435
Inventor 原晋波
Owner 原晋波