Halogen-free rubber foam insulation material and preparation method thereof

A technology for rubber-plastic foaming and thermal insulation materials, applied in the field of thermal insulation materials, can solve the problems of flammability, environmental pollution, unfavorable environmental protection and sustainable development, and achieve the effect of high closed cell rate and small pores

Inactive Publication Date: 2017-12-29
FOSHAN FEISHIDA NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At the same time, in order to solve the problem of its flammability, the flame retardant effect is often achieved by adding halogen flame retardants, but

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] S1: Mix 30 parts of EPDM rubber, 10 parts of ethylene-vinyl acetate copolymer, 20 parts of hexanediol and 10-20 parts of ethylene propylene rubber, adjust the temperature to 110°C and stir for 20 minutes at a rate of 400r / min;

[0023] S2: Then add 10 parts of polyvinyl chloride, 5 parts of polydipentanone, and 2 parts of methylmagnesium chloride, adjust the temperature to 120 ° C, and react for 15 minutes; then add 6 parts of polycaprolactone and 3 parts of trioctyl phosphate, adjust The temperature reaches 128°C, and the reaction is continued for 20 minutes;

[0024] S3: Add 5 parts of 2-methyl-6-isopropylaniline, 2 parts of aluminum silicate and 6 parts of azodicarbonamide, and stand for reaction at a temperature of 135° C. for 30 minutes;

[0025] S4: Stir and react at a rate of 800r / min for 20min; after the reaction is cooled, dry at a temperature of 140°C for 2h and granulate to obtain the halogen-free rubber and plastic foam insulation material.

Embodiment 2

[0027] S1: Mix 35 parts of EPDM rubber, 15 parts of ethylene-vinyl acetate copolymer, 30 parts of hexanediol and 20 parts of ethylene propylene rubber, adjust the temperature to 120°C, and stir and react at a rate of 500r / min for 30min;

[0028] S2: Then add 15 parts of polyvinyl chloride, 10 parts of polydipentanone, and 5 parts of methylmagnesium chloride, adjust the temperature to 125 ° C, and react for 25 minutes; then add 10 parts of polycaprolactone and 5 parts of trioctyl phosphate, adjust The temperature reaches 132°C, and the reaction is continued for 30 minutes;

[0029] S3: Add 10 parts of 2-methyl-6-isopropylaniline, 5 parts of aluminum silicate and 10 parts of azodicarbonamide, and stand for reaction at a temperature of 140° C. for 40 minutes;

[0030] S4: Stir and react at a speed of 900r / min for 30min; after the reaction is cooled, dry at a temperature of 140°C for 2h and granulate to obtain the halogen-free rubber and plastic foam insulation material.

Embodiment 3

[0032] S1: Mix 32 parts of EPDM rubber, 12 parts of ethylene-vinyl acetate copolymer, 25 parts of hexanediol and 12 parts of ethylene propylene rubber, adjust the temperature to 115°C, and stir at a rate of 450r / min for 25 minutes;

[0033] S2: Then add 12 parts of polyvinyl chloride, 7 parts of polydipentanone, and 2 parts of methyl magnesium chloride, adjust the temperature to 122 ° C, and react for 20 minutes; then add 7 parts of polycaprolactone and 5 parts of trioctyl phosphate, adjust The temperature reaches 130°C, and the reaction is continued for 28 minutes;

[0034] S3: Add 6 parts of 2-methyl-6-isopropylaniline, 3 parts of aluminum silicate and 7 parts of azodicarbonamide, and stand for reaction at a temperature of 138° C. for 35 minutes;

[0035] S4: Stir and react at a speed of 800 r / min for 25 minutes; after the reaction is cooled, dry at a temperature of 140° C. for 2 hours and granulate to obtain the halogen-free rubber and plastic foam insulation material.

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PUM

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Abstract

The invention discloses a preparation method of a halogen-free rubber foam insulation material. The preparation method comprises the following steps: mixing an ethylene-propylene-diene monomer with ethylene propylene, adjusting the temperature to 110-120 DEG C, and performing a stirring reaction for 20-30 minutes; further adding polyvinyl chloride, polydipentanone and methyl magnesium chloride, adjusting the temperature to 120-125 DEG C, and performing a reaction for 15-25 minutes; further adding polycaprolactone and trioctyl phosphate, adjusting the temperature to 128-132 DEG C, and performing a reaction for 20-30 minutes continuously; adding 2-methyl-6-isopropyl phenylamine, aluminum silicate and azodicarbonamide, and leaving to stand at 135-140 DEG C to react for 30-40 minutes; further performing a stirring reaction for 20-30 minutes at a velocity of 800-900r/minute; cooling after the reaction, drying, and pelletizing, thereby obtaining the halogen-free rubber foam insulation material. The halogen-free rubber foam insulation material prepared by using the method is good in both flame retardancy and heat preservation.

Description

technical field [0001] The invention belongs to the field of thermal insulation materials, in particular to a halogen-free rubber and plastic foam thermal insulation material and a preparation method thereof. Background technique [0002] The traditional thermal insulation materials are mainly to increase the gas phase void ratio and reduce the thermal conductivity and conductivity coefficient. In order to increase convective heat transfer and radiation heat transfer in the use environment, fiber-based thermal insulation materials must have a thicker coating; while profile-based inorganic thermal insulation materials need to be assembled and constructed, there are many seams, which damage the appearance and waterproof. Poor performance, short service life and other defects. The promulgation and implementation of rubber and plastic insulation materials and products, and energy-saving regulations are the influencing factors affecting building energy conservation, involving a ...

Claims

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Application Information

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IPC IPC(8): C08L23/16C08L27/06C08L67/04C08K5/521C08K5/18C08K3/34C08K13/02C08J9/10
CPCC08L23/16C08J9/103C08J2203/04C08J2205/052C08J2323/16C08J2427/06C08L2201/02C08L2201/22C08L2203/14C08L2205/025C08L2205/035C08L23/0853C08L27/06C08L67/04C08K5/521C08K5/18C08K3/34C08K5/053C08K13/02
Inventor 陈兴建
Owner FOSHAN FEISHIDA NEW MATERIAL TECH CO LTD
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