Preparation method of nano-fiber scaffold for promoting cardiac muscle cell reconstruction
A nanofiber, cardiomyocyte technology, applied in conductive/antistatic filament manufacturing, medical science, prosthesis, etc., can solve the problem that polydimethylsiloxane is difficult to manufacture nanofiber structure, poor biocompatibility, limitation Clinical application and other issues, to achieve the effect of improving cell compatibility, improving electrical conductivity, and good biocompatibility
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Embodiment 1
[0024] (1) Dissolving polyaniline (PANI) and camphorsulfonic acid (CSA) with a weight average molecular weight of 20,000 in hexafluoroisopropanol, stirring evenly to obtain a polyaniline mass percentage concentration of 1.5%, and camphorsulfonic acid mass percent A mixed solution with a concentration of 0.5%;
[0025] (2) adding polycaprolactone (PCL) with a weight average molecular weight of 100,000 to the mixed solution obtained in step (1), stirring evenly to obtain a spinning solution with a polymer concentration of 20 wt %;
[0026] (3) Input the spinning solution in step (2) to the spinneret of the electrospinning equipment at a propulsion speed of 15 μL / min, and connect the spinneret to a 21KV power supply for electrospinning to prepare a composite nanometer with a diameter of 600 nm. For fiber, collect electrospun nanofibers with a stainless steel drum with a rotating speed of 200rpm / min, and the receiving distance between the stainless steel drum and the spinneret is ...
Embodiment 2
[0029] (1) Dissolving polyaniline (PANI) and camphorsulfonic acid (CSA) with a weight average molecular weight of 10,000 in hexafluoroisopropanol, stirring evenly to obtain a polyaniline mass percentage concentration of 0.5%, and camphorsulfonic acid mass percent A mixed solution with a concentration of 0.2%;
[0030] (2) adding poly-L-lactide with a weight average molecular weight of 60,000 to the mixed solution obtained in step (1), stirring evenly to obtain a spinning solution with a polymer concentration of 10wt%;
[0031] (3) Input the spinning solution in step (2) to the spinneret of the electrospinning equipment at a propulsion speed of 20 μL / min, and at the same time connect the spinneret to a 17KV power supply for electrospinning to prepare a composite nanotube with a diameter of 450 nm. Fiber, collect the electrospun nanofiber with the stainless steel roller of rotating speed 300rpm / min, the receiving distance between stainless steel roller and spinneret is 21cm;
...
Embodiment 3
[0034] (1) Dissolving polyaniline (PANI) and camphorsulfonic acid (CSA) with a weight average molecular weight of 30,000 in hexafluoroisopropanol, stirring evenly to obtain a polyaniline mass percentage concentration of 4%, and camphorsulfonic acid mass percent The concentration is 0.8% mixed solution;
[0035] (2) Adding poly(glycolactide) with a weight average molecular weight of 200,000 to the mixed solution obtained in step (1), stirring evenly to obtain a spinning solution with a polymer concentration of 30wt%;
[0036] (3) Input the spinning solution in step (2) to the spinneret of the electrospinning equipment at a propulsion speed of 10 μL / min, and at the same time connect the spinneret to a 28KV power supply for electrospinning to prepare a composite nanotube with a diameter of 900 nm. For fibers, collect electrospun nanofibers with a stainless steel drum with a rotating speed of 100rpm / min, and the receiving distance between the stainless steel drum and the spinneret...
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