Removing method for benzopyrene in edible vegetable oil
A technology of edible vegetable oil and benzopyrene, which is applied in the direction of fat oil/fat refining and fat production, etc. It can solve problems such as food-grade solvents not being completely removed, oil drying not in time, and benzopyrene exceeding the standard, so as to eliminate potential safety hazards, Short heating time and good removal effect
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Embodiment 1
[0020] The method for removing benzopyrene in edible vegetable oil specifically includes the following steps:
[0021] (1) Degumming: select edible grade citric acid as degumming agent, add degumming agent according to 0.5% of edible vegetable oil weight, control degumming temperature 40 ℃, stirring speed 180r / min, degumming time is 50min;
[0022] (2) Deacidification: input the degummed edible vegetable oil into the molecular distillation equipment, control the vacuum degree to 2Pa, and the heating temperature to 200°C to separate free fatty acids;
[0023] (3) Preparation of adsorbent: Add twice the weight of hydrochloric acid solution with a mass fraction of 10% to diatomite, ultrasonically oscillate for 30 minutes, and then add sodium dodecylsulfonate accounting for 2-4% by weight of diatomite , continue to ultrasonically oscillate for 30 minutes, and then centrifuge to collect the precipitate; put the precipitate into 50°C water for 30 minutes, take it out, place it at 35...
Embodiment 2
[0028] The method for removing benzopyrene in edible vegetable oil specifically includes the following steps:
[0029] (1) Degumming: select edible grade citric acid as degumming agent, add degumming agent according to 0.6% of edible vegetable oil weight, control degumming temperature 45 ℃, stirring speed 180-200r / min, degumming time is 45min;
[0030] (2) Deacidification: input the degummed edible vegetable oil into the molecular distillation equipment, control the vacuum degree to 3Pa, and the heating temperature to 180°C to separate free fatty acids;
[0031] (3) Preparation of adsorbent: add twice the weight of hydrochloric acid solution with a mass fraction of 10% to diatomite, ultrasonically oscillate for 35 minutes, then add sodium dodecylsulfonate accounting for 3% by weight of diatomite, and continue Ultrasonic oscillation for 35 minutes, and then centrifuge to collect the precipitate; put the precipitate into 55°C water for 30 minutes, take it out, put it in 380°C fo...
Embodiment 3
[0036] The method for removing benzopyrene in edible vegetable oil specifically includes the following steps:
[0037] (1) Degumming: select edible grade citric acid as degumming agent, add degumming agent according to 0.8% of edible vegetable oil weight, control degumming temperature 50 ℃, stirring speed 180r / min, degumming time is 50min;
[0038] (2) Deacidification: Input the degummed edible vegetable oil into the molecular distillation equipment, control the vacuum degree to 5Pa, and the heating temperature to 170°C to separate free fatty acids;
[0039] (3) Prepare the adsorbent: add twice the weight of hydrochloric acid solution with a mass fraction of 10% to the diatomite, ultrasonically oscillate for 40 minutes, then add sodium dodecylsulfonate accounting for 4% by weight of diatomite, and continue Ultrasonic vibration for 40 minutes, and then centrifuge to collect the precipitate; put the precipitate into 60°C water for 30 minutes, take it out, place it at 400°C for 3...
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