Molecular sieve ceramic membrane material for olefin purification as well as preparation method and application of molecular sieve ceramic membrane material
A ceramic material and molecular sieve technology, applied in the field of inorganic membrane materials, can solve the problem of inability to deeply purify polar oxygen-containing compounds, and achieve the effects of excellent rigidity and mechanical strength, high heat resistance, and low energy consumption
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[0056] Example 1:
[0057] Ceramic tube pretreatment: the α-Al with an average pore diameter of 2μm and a porosity of 55% 2 O 3 The ceramic tube is baked in a muffle furnace at 200℃ for 1h, cooled to room temperature naturally, and the α-Al 2 O 3 The surface of the ceramic tube is polished smooth, deionized water is ultrasonically cleaned for 2 hours, dried in an oven at 120°C for 3 hours, and cooled for later use. Will polish smooth α-Al 2 O 3 The ceramic tube is immersed in the polydopamine solution: prepare the polydopamine solution at the ratio of 2mL polydopamine (2mg / L) / 100mL TRIS-HCl (10mmol / L), and then place the ceramic tube in the polydopamine solution under continuous stirring Soak at 25℃ for 10h, and finally dry for later use.
[0058] The preparation of molecular sieve seed liquid sol: The aluminum hydroxide, sodium silicate, sodium hydroxide, and deionized water are prepared according to n(Al):n(Si):n(Na):n(H 2 O)=2:3:12:300 The material ratio is mixed at room tempera...
Example Embodiment
[0062] Example 2:
[0063] Ceramic tube pretreatment: the α-Al with an average pore diameter of 0.1μm and a porosity of 20% 2 O 3 The ceramic tube is baked in a muffle furnace at 200℃ for 1h, cooled to room temperature naturally, and the α-Al 2 O 3 The surface of the ceramic tube is polished smooth, deionized water is ultrasonically cleaned for 2 hours, dried in an oven at 120°C for 3 hours, and cooled for later use. Will polish smooth α-Al 2 O 3 The ceramic tube is immersed in the polydopamine solution: prepare the polydopamine solution in the ratio of 2mL polydopamine (2mg / L) / 40ml TRIS-HCl (10mmol / L), and then place the ceramic tube in the polydopamine solution under continuous stirring Soak at 25℃ for 10h, and finally dry for later use.
[0064] The preparation of molecular sieve seed liquid sol: The aluminum hydroxide, sodium silicate, sodium hydroxide, and deionized water are prepared according to n(Al):n(Si):n(Na):n(H 2 O)=2:3:12:300 The material ratio is mixed at room temper...
Example Embodiment
[0068] Example 3:
[0069] Ceramic tube pretreatment: the α-Al with an average pore diameter of 5μm and a porosity of 80% 2 O 3 The ceramic tube is roasted in a muffle furnace at 200℃ for 1h, cooled to room temperature naturally, and α-Al is removed with 1500 mesh sandpaper. 2 O 3 The surface of the ceramic tube is polished smooth, deionized water is ultrasonically cleaned for 2 hours, dried in an oven at 120°C for 3 hours, and cooled for later use. Will polish smooth α-Al 2 O 3 The ceramic tube is immersed in the polydopamine solution: prepare the polydopamine solution at the ratio of 8mL polydopamine (2mg / L) / 100ml TRIS-HCl (10mmol / L), and then place the ceramic tube in the polydopamine solution under continuous stirring Soak at 25℃ for 24h, and finally dry for use.
[0070] The preparation of molecular sieve seed liquid sol: The aluminum hydroxide, sodium silicate, sodium hydroxide, and deionized water are prepared according to n(Al):n(Si):n(Na):n(H 2 O)=2:12:50:300 The material ...
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