A new type of sacrificial fuel cell and its preparation method and the application of the paired synthesis method to the reuse of carbon dioxide
A fuel cell and carbon dioxide technology, applied in the field of fuel cells, can solve problems such as being easily corroded, affecting catalytic performance and service life, and achieving the effect of efficient reduction of carbon dioxide and simple synthesis methods
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0023] Example 1: Preparation of novel sacrificial fuel cell electrodes
[0024] TiO in this example 2 / ITO electrode, prepared by the following method:
[0025] (1) Weigh 30mg TiO 2 Ultrasonic disperse in 2mL of ethanol for one hour, take 1mL of the dispersion and use the pulling method to obtain TiO 2 / ITO electrode;
[0026] (2) TiO 2 / ITO electrodes are placed in an oven and dried at a constant temperature of 35-45°C to obtain TiO 2 / ITO electrode.
[0027] The Pt-Cu of this embodiment 2 O electrode, prepared by the following method:
[0028] TiO prepared by 2 The / ITO electrode is used as the anode, and the ITO electrode is used as the cathode. Add 0.1mol / L sodium sulfite solution (electrolyte solution) and 1.0mol / L glucose (fuel) to the anode pool, add 0.4mol / L copper acetate solution (copper source) to the cathode pool, and use saturated potassium chloride between the two pools Salt bridge connection, prepared Cu under UV light irradiation 2 O electrode, foll...
Embodiment 2
[0029] Example 2: Construction of a novel sacrificial fuel cell
[0030] TiO prepared by 2 / ITO electrode as anode, Pt-Cu 2 O composite electrode as cathode. Add 0.1mol / L sodium sulfate solution (electrolyte solution) and 0.25mol / L sodium sulfide-sodium sulfite solution (fuel) to the anode pool, and add 0.1mol / L Na 2 CO 3 and 0.1mol / L NaHCO 3 A certain proportion of oxygen and carbon dioxide is introduced, and the two pools are connected by a saturated potassium chloride salt bridge, and carbon dioxide is photoelectrically reduced under the irradiation of an ultraviolet lamp.
Embodiment 3
[0031] Example 3: Performance test of new sacrificial fuel cell
[0032] To the test of the photocatalytic fuel cell performance that embodiment 2 builds, specific operation steps are as follows:
[0033] Adjust the resistance value of the resistance box connected between the anode and the cathode of the photocatalytic fuel cell, measure and calculate the change curve of the current density and power density of the photocatalytic fuel cell with voltage, the result is as follows figure 1 shown.
[0034] Under ultraviolet light irradiation, the novel sacrificial fuel cell constructed in Example 2 is fed with oxygen and nitrogen in different proportions of the atmosphere, when pure oxygen is fed with a flow rate of 60mL / min or oxygen and carbon dioxide are simultaneously fed with a flow rate of 60mL / min Time short circuit photocurrent density (curve 1) 0.06mAcm -2 , (curve 2) 0.04mAcm -2 , the battery power is 3.6μWcm -2 , 2.6μWcm -2 . It can be seen from the curve in the f...
PUM
Login to View More Abstract
Description
Claims
Application Information
Login to View More 


