Preparation method of sewage treatment agent
A technology of sewage treatment agent and bentonite, which is applied in the field of preparation of sewage treatment agent, can solve the problems of weak inorganic flocculant partial sewage treatment capacity, difficulty of inorganic flocculant and high molecular polymer, and poor physical method treatment effect, etc. Good biocompatibility, balanced sedimentation velocity, and the effect of adsorption performance protection
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Embodiment 1
[0022] A kind of preparation method of sewage treatment agent, comprises the following steps:
[0023] S1. In parts by weight, 20 parts of sodium bentonite and 2 parts of hydrochloric acid with a mass fraction of 20% are added to 50 parts of sodium lauryl sulfate with a mass fraction of 1.6%, and then ultrasonicated at 82°C for 30 minutes, and the ultrasonication ends Finally, filter, then wash to neutrality, and obtain modified bentonite after drying;
[0024] S2. In parts by weight, add 4 parts of chitosan to 50 parts of acetic acid aqueous solution with a mass fraction of 1.2%, stir for 20min, then add 12 parts of modified bentonite, stir at 90°C for 1.5h, then filter and wash , drying and pulverizing to obtain intercalation bentonite;
[0025] S3. In parts by weight, add 0.13 parts of ammonium persulfate to 6 parts of deionized water to dissolve, then add 20 parts of intercalation bentonite, stir evenly, and leave it in a sealed place in the dark at 15°C for 30 minutes to...
Embodiment 2
[0029] A kind of preparation method of sewage treatment agent, comprises the following steps:
[0030] S1. In parts by weight, add 20 parts of sodium bentonite and 4 parts of hydrochloric acid with a mass fraction of 20% to 50 parts of sodium lauryl sulfate with a mass fraction of 1.5%, and then ultrasonicate at 80°C for 45min, and the ultrasonication ends Finally, filter, then wash to neutrality, and obtain modified bentonite after drying;
[0031] S2. In parts by weight, add 3 parts of chitosan into 50 parts of chitosan in 1.1% aqueous acetic acid solution, stir for 30 minutes, then add 10 parts of modified bentonite, stir for 2 hours at 88° C., then filter, wash, Drying and crushing to obtain intercalated bentonite;
[0032] S3. In parts by weight, add 0.12 parts of ammonium persulfate to 6 parts of deionized water to dissolve, then add 19 parts of intercalated bentonite, stir evenly, and leave it in a sealed place in the dark at 30°C for 20 minutes to obtain polymerized s...
Embodiment 3
[0036] A kind of preparation method of sewage treatment agent, comprises the following steps:
[0037] S1. In parts by weight, add 20 parts of sodium bentonite and 3 parts of hydrochloric acid with a mass fraction of 20% to 50 parts of sodium lauryl sulfate with a mass fraction of 2%, and then sonicate at 76°C for 40min, and the sonication ends Finally, filter, then wash to neutrality, and obtain modified bentonite after drying;
[0038] S2. In parts by weight, add 5 parts of chitosan to 50 parts of acetic acid aqueous solution with a mass fraction of 1%, stir for 25 minutes, then add 13 parts of modified bentonite, stir at 85°C for 1.8 hours, then filter and wash , drying and pulverizing to obtain intercalation bentonite;
[0039] S3. In parts by weight, add 0.14 parts of ammonium persulfate to 6 parts of deionized water to dissolve, then add 18 parts of intercalated bentonite, stir evenly, and leave it in a sealed place in the dark at 17°C for 35 minutes to obtain polymeriz...
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