Preparation method of fish oil soft capsules
A soft capsule and fish oil technology, which is applied in the fields of fat oil/fat refining, food shaping, fat oil/fat separation, etc., can solve the problems of DHA and EPA loss of function, easy to be oxidized, and low enthusiasm for eating, so as to increase palatability, Prevents oxidation of fish oil and enhances efficacy
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Embodiment 1
[0036] Salmon liver homogenate: remove the liver from the salmon, wash it three times in normal saline, homogenize the washed salmon liver at -3°C, and store the homogenate in a freezer.
[0037] Thorn wine residue: Ziqiu thorn grape, Hunan Huachun Manor Winery Co., Ltd.
[0038] Compound nutrient: in parts by mass, 12 parts of propolis, 4 parts of angelica, 3 parts of aloe, and 2 parts of wolfberry are mixed, ground and homogenized to obtain a compound nutrient.
[0039] (1) Take the salmon liver homogenate and add distilled water at a mass ratio of 1:2, adjust the pH to 8, add phosphatase with 2% mass of the salmon liver homogenate, heat up to 40°C, stir and mix at 300 r / min, and enzymatically hydrolyze for 4 hours , then inactivate the enzyme at 90°C for 5 min, centrifuge at 8000 r / min for 10 min, take the supernatant A and add distilled water at 50°C according to the mass ratio of 1:8, shake and shake well, centrifuge again at 8000 r / min for 10 min, and collect the supernata...
Embodiment 2
[0045] Salmon liver homogenate: remove the liver from the salmon, wash it 4 times in normal saline, homogenize the washed salmon liver at -2°C, and store the homogenate in a freezer.
[0046] Thorn wine residue: Ziqiu thorn grape, Hunan Huachun Manor Winery Co., Ltd.
[0047] Compound nutrient: in parts by mass, 13 parts of propolis, 4 parts of angelica, 4 parts of aloe, and 3 parts of wolfberry are mixed, ground and homogenized to obtain a compound nutrient.
[0048] (1) Take the salmon liver homogenate and add distilled water at a mass ratio of 1:2, adjust the pH to 8.2, add phosphatase with 2-5% of the mass of the salmon liver homogenate, raise the temperature to 43°C, stir and mix at 300 r / min, the enzyme Solution for 4 hours, then inactivate the enzyme at 93°C for 10 minutes, centrifuge at 8000 r / min for 10 minutes, take the supernatant A and add distilled water at 60°C at a mass ratio of 1:8, shake well, centrifuge again at 8000r / min for 12 minutes, and collect the super...
Embodiment 3
[0054] Salmon liver homogenate: remove the liver from the salmon, wash it 5 times in normal saline, homogenize the washed salmon liver at 4°C, and store the homogenate in a freezer.
[0055] Thorn wine residue: Ziqiu thorn grape, Hunan Huachun Manor Winery Co., Ltd.
[0056] Compound nutrient: in parts by mass, 15 parts of propolis, 5 parts of angelica, 6 parts of aloe, and 4 parts of wolfberry are mixed, ground and homogenized to obtain a compound nutrient.
[0057] (1) Take the salmon liver homogenate and add distilled water at a mass ratio of 1:2, adjust the pH to 8.5, add phosphatase with 5% mass of the salmon liver homogenate, heat up to 45°C, stir and mix at 300 r / min, and enzymatically hydrolyze for 5 h, then inactivate the enzyme at 95°C for 15 min, centrifuge at 8000 r / min for 10 min, take the supernatant A and add distilled water at 70°C according to the mass ratio of 1:8, shake and shake well, centrifuge again at 8000 r / min for 15 min, and collect the supernatant L...
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