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Preparation method of universal fabric antibacterial finishing agent

An antibacterial finishing agent and a general-purpose technology are applied in the field of preparation of general-purpose fabric antibacterial finishing agents, which can solve the problem of high cost of finishing agents, and achieve the effects of good durability, good stability and good bacteriostatic performance.

Inactive Publication Date: 2018-08-17
DONGGUAN JIAQIAN NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Chinese patent (CN101368331A) discloses a kind of inorganic nano antibacterial finishing agent of cotton and linen fabric and preparation method thereof, adds silver nitrate and small molecule organic or inorganic reducing agent in polyethylene glycol, as ascorbic acid, tannic acid, tartaric acid etc., Perform reduction at 5-100°C to obtain nano-silver with good dispersibility and stability, disperse the prepared nano-silver in an aqueous medium to obtain a nano-silver finishing solution, and pad the cotton and linen fabric in the finishing solution, A composite material with excellent antibacterial function is prepared, but the finishing agent is expensive

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] A preparation method of a general-purpose fabric antibacterial finishing agent, comprising the following steps:

[0025] (1) Grind and disperse Dendrobium dendrobium in water with a solid-liquid ratio of 1g:20mL, reflux at 80°C for 1 hour, filter, then add an organic solvent to the filtrate for layering, collect the organic layer, and dry it to obtain Dendrobium polysaccharide powder;

[0026] (2) Sodium alginate and sodium hydroxide solution with a mass concentration of 3% were mixed and stirred until the solid was dissolved, then the dendrobium polysaccharide powder prepared above was added, and after stirring and mixing, the temperature was slowly raised to 40° C., stirred for 1 hour at 3000 rpm, and then Cool to room temperature, filter, precipitate and dry to obtain sodium alginate cross-linked modified dendrobium polysaccharide; wherein, the dosage ratio of the sodium alginate and sodium hydroxide solution is 1g: 15mL; the sodium alginate and dendrobium polysaccha...

Embodiment 2

[0029] A preparation method of a general-purpose fabric antibacterial finishing agent, comprising the following steps:

[0030] (1) Grind and disperse Dendrobium dendrobium in water, the ratio of solid to liquid is 1g:40mL, reflux at 100°C for 5h, filter, then add organic solvent to the filtrate for layering treatment, collect the organic layer, dry, and obtain Dendrobium polysaccharide powder;

[0031] (2) Sodium alginate and sodium hydroxide solution with a mass concentration of 10% were mixed and stirred until the solid was dissolved, and then the dendrobium polysaccharide powder prepared above was added, and after stirring and mixing, the temperature was slowly raised to 60° C., stirred for 2 hours at 5000 rpm, and then Cool to room temperature, filter, precipitate and dry to obtain sodium alginate cross-linked modified dendrobium polysaccharide; wherein, the dosage ratio of the sodium alginate and sodium hydroxide solution is 1g: 35mL; the sodium alginate and dendrobium p...

Embodiment 3

[0034] A preparation method of a general-purpose fabric antibacterial finishing agent, comprising the following steps:

[0035] (1) Grind and disperse Dendrobium dendrobium in water with a solid-liquid ratio of 1g:25mL, reflux at 80°C for 2h, filter, then add an organic solvent to the filtrate for layering, collect the organic layer, and dry it to obtain Dendrobium polysaccharide powder;

[0036] (2) Sodium alginate and sodium hydroxide solution with a mass concentration of 5% were mixed and stirred until the solid was dissolved, then the dendrobium polysaccharide powder prepared above was added, and after stirring and mixing, the temperature was slowly raised to 45°C, and stirred at 3500pm for 1.5h, Then cool to room temperature, filter, precipitate and dry to obtain sodium alginate cross-linked modified dendrobium polysaccharide; wherein, the dosage ratio of the sodium alginate and sodium hydroxide solution is 1g:20mL; the sodium alginate and dendrobium polysaccharide The m...

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Abstract

The invention discloses a preparation method of a universal fabric antibacterial finishing agent. The preparation method particularly includes following steps: using dendrobium as a raw material, andextracting to obtain dendrobium polysaccharide; preparing sodium alginate crosslinked modified dendrobium polysaccharide; dispersing the sodium alginate crosslinked modified dendrobium polysaccharidein deionized water; sequentially adding acrylic resin, chitosan, silane coupling agent, defoamer and thickener, and stirring and mixing well to obtain the antibacterial finishing agent. The finishingagent is high in stability and fabric wettability and capable of effectively improving antibacterial performance and mechanical performance of fabric.

Description

Technical field: [0001] The invention relates to the field of textile auxiliaries, in particular to a preparation method of a general antibacterial fabric finishing agent. Background technique: [0002] Due to its microporous structure, textiles have long been considered by hygienists to be the most suitable breeding grounds for microorganisms such as bacteria and fungi. The body temperature of the wearer, the moisture emitted by the human body, and the metabolites of the skin have further enhanced the vitality of the germs and microorganisms remaining on the fabric. Due to the characteristics of water repellency and low moisture absorption of the fiber itself, synthetic fibers have a certain inhibitory effect on the survival and reproduction of microorganisms. The keratin components in protein fibers and the sugar in cotton fibers can be used as nutrients for most microorganisms under suitable conditions. Soil, electrolytes secreted by the human body, and some finishing a...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06M15/263D06M15/03D06M15/13D06M101/06
CPCD06M15/03D06M15/13D06M15/263D06M16/00D06M2101/06
Inventor 王海燕
Owner DONGGUAN JIAQIAN NEW MATERIAL TECH CO LTD
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