Preparation for self-crosslinking compound solid electrolyte and all-solid lithium ion battery composed of self-crosslinking compound solid electrolyte
A solid-state electrolyte and lithium-ion battery technology, which is applied in the manufacture of electrolyte batteries, non-aqueous electrolyte batteries, solid electrolytes, etc., can solve the problems of electrolyte mechanical performance deviation, complex preparation process, and influence on electrolyte electrochemical performance, and achieve product shrinkage. Small size, simple preparation process, and good ion conductivity
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Embodiment 1
[0032] Polypropylene oxide (number-average molecular weight=12000) of 3g terminal silane-terminated polyether, 3g Li 7 La 3 ZrO 12 , 4ml of acetonitrile and 4ml of tetraethylene glycol dimethyl ether were evenly mixed; adding 3g of lithium hexafluorophosphate (LiPF 6 ) mixed evenly; the uniformly stirred mixed solution was scraped onto the polytetrafluoroethylene mold, heated at 60°C for 8 hours in a blast drying oven, and transferred to a vacuum oven at 80°C for curing for 4 hours to form a film.
Embodiment 2
[0034] The polypropylene oxide (number average molecular weight=12000) of 1.5g terminal silane-terminated polyether, the PEO after 1g acid treatment, 2ml propylene carbonate and 30ml tetrahydrofuran are evenly mixed; Add 0.8g lithium hexafluorophosphate (LiPF 6 ) and mix evenly; scrape-coat the mixed solution evenly on the polytetrafluoroethylene mold, heat it at 60°C for 8 hours in a blast drying oven, and transfer it to a vacuum drying oven at 80°C for curing for 4 hours to form a film.
Embodiment 3
[0036] With 2.2g polypropylene oxide (number-average molecular weight=12000) of capped polyether, SiO after 2.8g alkaline treatment 2 Mix evenly with 4ml triethylene glycol dimethyl ether; add 1.4g lithium bistrifluoromethanesulfonylimide (LiTFSI) and mix evenly; scrape the evenly stirred mixed solution on the polytetrafluoroethylene mold, and dry it in the blast Heat at 60°C for 8 hours in the oven, transfer to a vacuum drying oven at 80°C for 4 hours to form a film.
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