A kind of resin type artificial stone and preparation method thereof
A technology of artificial stone and resin type, applied in the field of artificial stone, can solve the problems of destroying the original pattern of resin type artificial stone, affecting the appearance, and affecting the strength of resin type artificial stone, so as to reduce the curing shrinkage rate, increase the service life and improve the toughness Effect
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Embodiment 1
[0047] The preparation of embodiment 1 novel resin type artificial stone
[0048] Raw material composition:
[0049] 20 parts of polyurethane modified unsaturated polyester / phase change energy storage microcapsule composite material;
[0050] 50 parts of calcite crushed stone;
[0051] 10 parts of triethylenetetramine;
[0052] 10 parts of N,N-dimethyl-p-methylaniline;
[0053] Coupling agent DL1715 parts;
[0054] 1 part of phenyl o-hydroxybenzoate;
[0055]1 part chrome yellow.
[0056] The polyurethane modified unsaturated polyester / phase change energy storage microcapsule composite is prepared by the following method:
[0057] Step 1. Synthesis of prepolymer: Put polyester diol in a vacuum oven at 150°C for 5h, cool down to 50°C, add an equal amount of diisocyanate under stirring, react for 2h, cool down to 30°C, and obtain a prepolymer ;
[0058] Step 2. Synthesis of polyurethane-modified unsaturated polyester: add dicyclopentadiene-type unsaturated polyester liqu...
Embodiment 2
[0063] The preparation of embodiment 2 novel resin type artificial stone
[0064] Raw material composition:
[0065] 60 parts of polyurethane modified unsaturated polyester / phase change energy storage microcapsule composite material;
[0066] Shell and oyster shell powder 90 parts;
[0067] 20 parts of 2-methylimidazole;
[0068] 15 parts of triethylamine;
[0069] 10 copies of coupling agent DL602;
[0070] 5 parts of 2-hydroxy-4-n-octyloxybenzophenone;
[0071] 10 parts of titanium dioxide.
[0072] The polyurethane modified unsaturated polyester / phase change energy storage microcapsule composite is prepared by the following method:
[0073] Step 1. Synthesis of prepolymer: Put polyester diol in a vacuum oven at 150°C for 5 hours, cool down to 50°C, add an equal amount of diisocyanate under stirring, react for 3 hours, and cool down to 30°C to obtain a prepolymer ;
[0074] Step 2. Synthesis of polyurethane-modified unsaturated polyester: add hexaacetic acid-type uns...
Embodiment 3
[0079] The preparation of embodiment 3 novel resin type artificial stone
[0080] Raw material composition:
[0081] 30 parts of polyurethane modified unsaturated polyester / phase change energy storage microcapsule composite material;
[0082] 60 parts of marble gravel;
[0083] 12 parts of polyazelaic anhydride;
[0084] 12 parts of zinc isooctanoate;
[0085] Coupling agent KH5706 parts;
[0086] 2 parts of 2-(2'-hydroxy-3',5'-di-tert-phenyl)-5-chlorinated benzotriazole;
[0087] Iron oxide red 1 part, iron oxide yellow 2 parts.
[0088] The polyurethane modified unsaturated polyester / phase change energy storage microcapsule composite is prepared by the following method:
[0089] Step 1. Synthesis of prepolymer: Put polyester diol in a vacuum oven at 150°C for 5h, cool down to 50°C, add an equal amount of diisocyanate under stirring, react for 2h, cool down to 30°C, and obtain a prepolymer ;
[0090] Step 2. Synthesis of polyurethane-modified unsaturated polyester: ad...
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