Production method of nickel-iron-phosphorus amorphous alloy catalytic reactor
A catalytic reactor, amorphous alloy technology, used in chemical instruments and methods, chemical/physical processes, metal material coating processes, etc. The effect of improving utilization efficiency
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Embodiment 1
[0031] Embodiment 1: the production technology of nickel-iron-phosphorus amorphous alloy catalytic reactor
[0032] (1) Surface treatment of fibers: using φ 0.04 mm polypropylene fiber, chemical degreasing and degreasing with sodium hydroxide solution;
[0033] (2) Coarsening of polypropylene fibers, the proportion of the coarsening aqueous solution is 80g / L chromic anhydride, 300ml / L sulfuric acid, the roughening treatment temperature is 60°C, and the roughening treatment time is 20min;
[0034] (3) For fiber sensitization, the composition of the sensitization solution is 8g / L tin chloride, 40ml / L hydrochloric acid, and the sensitization treatment time is 3min;
[0035] (4) Silver nitrate and ammonia solution are used to activate the fiber surface, and the activated fiber is reduced by formaldehyde solution;
[0036] (5) Electroless plating of treated fibers, the solution composition is: nickel chloride 0.45mol / L, tartaric acid 0.3mol / L, sodium hypophosphite 0.2mol / L, pota...
Embodiment 2
[0042] Embodiment 2: the production method of nickel-iron-phosphorus amorphous alloy catalytic reactor
[0043] (1) Surface treatment of fibers: using 0.02×1 mm polypropylene thin strip, chemically degreased and degreased with sodium hydroxide solution;
[0044] (2) The ratio of the roughened aqueous solution of the polypropylene thin strip is 65g / L chromic anhydride, 250ml / L sulfuric acid, the roughening treatment temperature is 60°C, and the roughening treatment time is 30min;
[0045] (3) For fiber sensitization, the composition of the sensitization solution is tin chloride 6.5g / L, hydrochloric acid 30ml / L, and the sensitization treatment time is 2min;
[0046] (4) Silver nitrate and ammonia solution are used to activate the fiber surface, and the activated fiber is reduced by formaldehyde solution;
[0047] (5) Electroless plating of treated fibers, the solution composition is: nickel sulfate 0.4mol / L, ferrous sulfate 0.08mol / L, tartaric acid 0.35mol / L, sodium hypophosph...
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