Titanium modified Fe3O4 magnetic nano-particle, preparation method and application thereof
A magnetic nanoparticle modification technology, applied in chemical instruments and methods, water/sludge/sewage treatment, metal/metal oxide/metal hydroxide catalysts, etc. Waste and other problems, to achieve the effect of low equipment requirements, low consumption, and serious waste of raw materials
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Embodiment 1
[0033] A kind of titanium modified Fe 3 o 4 A method for preparing magnetic nanoparticles, comprising the following steps:
[0034] 1) Weigh 5.586g (0.04mol) of choline chloride and 4.804g of urea (0.08mol) into a 60mL reaction kettle, stir at 50°C until the solid mixture turns into a liquid, and obtain the choline chloride-urea eutectic solvent.
[0035] 2) Add 1.668g (0.0060mol) FeSO to the choline chloride-urea deep eutectic solvent prepared in step 1) 4 ·7H 2 O and 0.584g (0.0104mol) KOH and stirred for 30min, then added 0.408g (0.0012mol) n-butyl titanate and stirred for 5min, finally added 0.420g (0.0075mol) KOH, stirred at 80°C for 30min, then put the reaction kettle Put it in an oven at 110°C for 4 hours to obtain solid particles, centrifuge, wash with distilled water (3×20mL) and ethanol (1×20mL), and dry in air to obtain the product titanium-modified Fe 3 o 4 magnetic nanoparticles.
[0036] The product obtained in this embodiment titanium modified Fe 3 o 4 ...
Embodiment 2
[0042] A kind of titanium modified Fe 3 o 4 A method for preparing magnetic nanoparticles, comprising the following steps:
[0043] 1) Weigh 5.586g (0.04mol) of choline chloride and 4.804g (0.08mol) of urea into a 60mL reaction kettle, stir at 50°C until the solid mixture turns into a liquid, and obtain the choline chloride-urea eutectic solvent.
[0044] 2) Add 1.668g (0.0060mol) FeSO to the choline chloride-urea deep eutectic solvent prepared in step 1) 4 ·7H 2 O and 0.584g (0.0104mol) KOH and stirred for 30min, then added 0.050g (0.00015mol) n-butyl titanate and stirred for 5min, finally added 0.420g (0.0075mol) KOH, stirred at 80°C for 30min, then put the reaction kettle Put it in an oven at 110°C for 4 hours to obtain solid particles, which were centrifuged, washed with distilled water (3×20 mL) and ethanol (1×20 mL), and dried in air to obtain the product.
Embodiment 3
[0046] A kind of titanium modified Fe 3 o 4 A method for preparing magnetic nanoparticles, comprising the following steps:
[0047] 1) Weigh 5.586g (0.04mol) of choline chloride and 4.804g (0.08mol) of urea in a 60mL reactor, and stir at 50°C until the solid mixture turns into a liquid to obtain the choline chloride-urea eutectic solvent.
[0048] 2) Add 1.668g (0.0060mol) FeSO to the choline chloride-urea deep eutectic solvent prepared in step 1) successively 4 ·7H 2 O and 0.584g (0.0104mol) KOH and stirred for 30min, then added 4.080g (0.012mol) of n-butyl titanate and stirred for 5min, finally added 0.420g (0.0075mol) KOH, stirred at 80°C for 30min, then put the reaction kettle Put it in an oven at 110°C for 4 hours to obtain solid particles, which were centrifuged, washed with distilled water (3×20 mL) and ethanol (1×20 mL), and dried in air to obtain the product.
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