Preparing method of beryllia ceramic polishing substrate for thin film circuit
A beryllium oxide ceramic and thin-film circuit technology, which is applied to surface-polished machine tools, grinding/polishing equipment, manufacturing tools, etc., can solve the problems of scrapping thin-film circuits/devices, difficult to achieve mirror effect, and short-circuiting thin-film circuits, etc. The effect of product surface quality, avoiding secondary grain growth, and increasing ceramic porosity
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Embodiment 1
[0058] Weigh 20kg of ultra-high-purity beryllium oxide raw powder, load the beryllium oxide powder with a firing bowl and a firing plate as a temperature-resistant container, and put it into a kiln with a final temperature of 1320°C and a temperature difference of ±10°C. The temperature was raised at a rate of ℃ / h, and the temperature was kept for 4 hours for calcination. After calcining, weigh 100kg of 99% beryllium oxide ceramic balls with a diameter of φ15mm to 20mm, 20kg of deionized water, and 600g of AR-grade magnesium silicate pentahydrate for use. Pour it into a ball mill, and after ball milling for 30 minutes, add 20kg of calcined beryllium oxide material, and after ball milling for 12 hours, pass the ceramic slurry through a 200-mesh nylon screen for later use.
[0059] Weigh 10kg of ceramic slurry, 300g of 10% PVA (polyvinyl alcohol PVB-88) aqueous solution, 500g of n-octanol, and 100g of herring oil, pour them into a stirring tank, stir slowly at a speed of 20r / min...
Embodiment 2
[0065] Weigh 20kg of ultra-high-purity beryllium oxide raw powder, load the beryllium oxide powder with a firing bowl and a firing plate as a temperature-resistant container, and put it into a kiln with a final temperature of 1320°C and a temperature difference of ±10°C. The temperature is raised at a rate of ℃ / h, and the temperature is kept for 6 hours for calcination. After calcining, weigh 100kg of 99% beryllium oxide ceramic balls with a diameter of φ15mm to 20mm, 25kg of deionized water, and 1000g of AR grade magnesium silicate pentahydrate for use. Pour it into a ball mill, and after ball milling for 30 minutes, add 20kg of calcined beryllium oxide material, and after ball milling for 12 hours, pass the ceramic slurry through a 200-mesh nylon screen for later use.
[0066] Weigh 10kg of ceramic slurry, 300g of 10% PVA (polyvinyl alcohol PVB-88) aqueous solution, 500g of n-octanol, and 200g of herring oil, pour them into a stirring tank, stir slowly at a speed of 20r / min ...
Embodiment 3
[0072] Weigh 20 kg of ultra-high-purity beryllium oxide raw powder, load the beryllium oxide powder with a firing bowl and a firing plate as a temperature-resistant container, and put it into a kiln with a final temperature of 1350 °C and a temperature difference of ±10 °C. The temperature was raised at a rate of ℃ / h, and the temperature was kept for 4 hours for calcination. After calcining, weigh 100kg of 99% beryllium oxide ceramic balls with a diameter of φ15mm to 20mm, 25kg of deionized water, and 1000g of AR grade magnesium silicate pentahydrate for use. Pour it into a ball mill, and after ball milling for 30 minutes, add 20kg of calcined beryllium oxide material, and after ball milling for 12 hours, pass the ceramic slurry through a 200-mesh nylon screen for later use.
[0073] Weigh 10kg of ceramic slurry, 300g of 10% PVA (polyvinyl alcohol PVB-88) aqueous solution, 500g of n-octanol, and 200g of herring oil, pour them into a stirring tank, stir slowly at a speed of 20r...
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