Method for rapidly preparing carbon fiber reinforced titanium alloy layered composite material

A layered composite material and titanium alloy technology, which is applied in the direction of metal material coating process, coating, liquid chemical plating, etc., can solve the problems of severe interface reaction, carbon fiber reinforced titanium and the reduction of mechanical properties of composite materials, etc. Effects of improved performance, increased preparation speed, and short holding time

Inactive Publication Date: 2019-10-11
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Due to the reaction between titanium alloy and most toughened fibers in high temperature environment, the interfacial products will affect the performance of the material, resulting in the decrease of the mechanical properties of carbon fiber reinforced titanium and composite materi

Method used

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  • Method for rapidly preparing carbon fiber reinforced titanium alloy layered composite material
  • Method for rapidly preparing carbon fiber reinforced titanium alloy layered composite material
  • Method for rapidly preparing carbon fiber reinforced titanium alloy layered composite material

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0029] Example 1

[0030] This embodiment includes the following steps:

[0031] Step 1. Put the carbon fiber cloth into absolute ethanol for ultrasonic cleaning for 10 minutes, and then dry it for 10 hours at a temperature of 100°C;

[0032] Step 2. The carbon fiber cloth dried in step 1 is sensitized with a sensitizing solution, then activated with an activation solution, and then reduced with a 10g / L sodium hypophosphite aqueous solution, washed with distilled water and dried Dry; the sensitizing solution is made of SnCl 2 , The mass concentration of 37% hydrochloric acid solution and distilled water composition, SnCl in the sensitizing solution 2 The concentration is 1g / L, the mass percentage of the hydrochloric acid solution is 1%, and the activation solution is made of PdCl 2 , Ethanol and distilled water, PdCl in the activation solution 2 The concentration is 0.1g / L;

[0033] Step 3. Put the carbon fiber cloth dried in step 2 into the nickel plating solution, then heat to 60°C ...

Example Embodiment

[0051] Example 2

[0052] This embodiment includes the following steps:

[0053] Step 1. Put the carbon fiber cloth in absolute ethanol for 30 minutes of ultrasonic cleaning, and then dry it at a temperature of 100°C for 20 hours;

[0054] Step 2. The carbon fiber cloth dried in step 1 is sensitized with a sensitizing solution, then activated with an activation solution, and then reduced with a 10g / L sodium hypophosphite aqueous solution, washed with distilled water and dried Dry; the sensitizing solution is made of SnCl 2 , The mass concentration of 37% hydrochloric acid solution and distilled water composition, SnCl in the sensitizing solution 2 The concentration is 20g / L, the mass percentage of the hydrochloric acid solution is 5%, and the activation solution is made of PdCl 2 , Ethanol and distilled water, PdCl in the activation solution 2 The concentration is 0.6g / L;

[0055] Step 3. Put the carbon fiber cloth dried in step 2 into the nickel plating solution, then heat to 90°C fo...

Example Embodiment

[0057] Example 3

[0058] This embodiment includes the following steps:

[0059] Step 1. Put the carbon fiber cloth into absolute ethanol for ultrasonic cleaning for 20 minutes, and then dry it for 15 hours at a temperature of 100°C;

[0060] Step 2. The carbon fiber cloth dried in step 1 is sensitized with a sensitizing solution, then activated with an activation solution, and then reduced with a 10g / L sodium hypophosphite aqueous solution, washed with distilled water and dried Dry; the sensitizing solution is made of SnCl 2 , The mass concentration of 37% hydrochloric acid solution and distilled water composition, SnCl in the sensitizing solution 2 The concentration is 10g / L, the mass percentage of the hydrochloric acid solution is 3%, and the activation solution is made of PdCl 2 , Ethanol and distilled water, PdCl in the activation solution 2 The concentration is 0.3g / L;

[0061] Step 3. Put the carbon fiber cloth dried in step 2 into the nickel plating solution, then heat to 80°C...

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Abstract

The invention discloses a method for rapidly preparing a carbon fiber reinforced titanium alloy layered composite material. The method comprises the following steps of S1, ultrasonically cleaning carbon fiber cloth and drying; S2, sequentially carrying out sensitization, activation and reduction on the dried carbon fiber cloth, and cleaning and drying; S3, plating nickel on the dried carbon fibercloth to obtain nickel-plated carbon fiber cloth; and S4, laying a nickel-plated carbon fiber cloth layer after the titanium alloy powder is laid on a plasma hot-pressing sintering mold, and then laying a titanium alloy powder layer, sequentially repeating the powder layer and the cloth layer paving process, and obtaining the carbon fiber reinforced titanium alloy layered composite material through discharge plasma hot-pressing sintering. According to the method, due to the fact that the heating rate is high, the heat preservation time is short and the pressure is high in the discharge plasmahot-pressing sintering process, and the isolation effect of the nickel-plated layer on the surface of the nickel-plated carbon fiber cloth to the the carbon fiber and the titanium alloy powder, the carbon fiber reinforced titanium alloy laminar composite material can be rapidly prepared, so that the integrity of the carbon fiber is ensured, and the mechanical property of the carbon fiber reinforced titanium alloy layered composite material is improved.

Description

technical field [0001] The invention belongs to the technical field of material preparation, and in particular relates to a method for rapidly preparing a carbon fiber reinforced titanium alloy layered composite material. Background technique [0002] As lightweight structural materials with excellent performance, titanium and titanium alloys have high specific strength, specific stiffness, good processability, corrosion resistance and high temperature resistance, so they are widely used in aerospace, marine vehicles, weapon engineering, medical equipment, etc. It has broad application prospects in many fields such as chemical energy and chemical energy. However, the disadvantages of titanium and titanium alloys such as poor wear resistance and low hardness hinder their application in engineering. In order to meet various needs accompanied by the rapid development of high-tech, it is urgent to develop new titanium alloy composite materials to meet the needs of aerospace ind...

Claims

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Application Information

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IPC IPC(8): B22F7/04B22F3/14
CPCB22F3/14B22F7/04B22F2003/1051B22F2998/10C23C18/1889C23C18/36
Inventor 刘跃霍望图张于胜卢金文董龙龙张伟杜岩李亮
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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