Lubricating oil composition and its preparation method and the micro-quantity lubricating oil prepared by the combination

A lubricating oil composition and lubricating oil technology, applied in the field of lubrication, can solve problems such as affecting the health of operators, being unsuitable for the technical field of metal cutting processing, unfriendly to sulfur- and chlorine-containing additives, and the like, achieving remarkable environmental protection effects, The effect of good degradability and excellent biodegradability

Active Publication Date: 2022-02-15
SHANGHAI JINZHAO ENERGY SAVING TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional metal cutting process uses mineral oil or vegetable oil or cutting fluid for a large amount of shower lubrication. The amount of lubricant used is large, which not only wastes resources, but also causes huge pollution to the processing site and the environment, and also seriously affects the health of the operators.
[0003] In order to solve these problems, some progress has been made in the research of micro-quantity lubrication technology recently. The micro-quantity lubrication technology solves the above problems such as large amount of lubricant used and serious pollution. At the same time, in order to make the micro-quantity lubricant used have relatively strong extreme pressure and anti-wear Sex and lubricity, excessive use of sulfur- and chlorine-containing additives that are not friendly to the environment, it is a meaningful research topic to study a micro-lubricant additive that does not contain sulfur and chlorine and has excellent extreme pressure and anti-wear properties. Since the boron-rare earth lubricating oil composition has relatively good self-repairing wear and antirust properties, the research on boron-rare earth lubricating oil composition materials is also of practical significance
[0004] The company's research group has studied rare earth borides as lubricating oil additives, and successfully applied for a related invention patent: intelligent repair micro-lubricating oil and its preparation method ZL201510955039.3, but the rare earth borides selected at that time were nano-lanthanum borate, boric acid Cerium, the prepared trace lubricating oil is actually a nano-suspension, and its application scope is mainly open gears, guide rails, bearings and other open environments that are lubricated with thin oil, and is not suitable for metal cutting processing technology

Method used

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  • Lubricating oil composition and its preparation method and the micro-quantity lubricating oil prepared by the combination
  • Lubricating oil composition and its preparation method and the micro-quantity lubricating oil prepared by the combination
  • Lubricating oil composition and its preparation method and the micro-quantity lubricating oil prepared by the combination

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Step 1: Take 100 g of oleic acid, 10 g of cerium oxide, 8 g of boric acid, 5 g (effective concentration of 85%), and stirred to 120 ° C, stirring for 2 hours.

[0039] Step 2: When the temperature eliminates to 45 ° C or lower, the mixture was added to 2 hours to obtain a translucent substance, that is, a lubricating oil composition.

[0040] It is weighed with the above-mentioned lubricating oil composition 100g, ishylacetinate 800 g, and the polymethyl metodercyl ester 100g of polymethyl metorcrylate is mixed at 40 ° C.

[0041] Method for preparing the polymethyl metorciolate of polymethyl methacrylate:

[0042] Step 1: 86.09 g (1 mol) of methacrylic acid was added to the reaction kettle with a reaction temperature of 1 mol of n-calcium alcohol, and at 180 ° C reaction temperature was 5 h. Acetinate;

[0043] Step 2, the initiator peroxide is added to the reactor, stirred, the reaction temperature is 120 ° C, and the polymerization is 5 hours, and the polymer in the reac...

Embodiment 2

[0045] Step 1: Take 100 g of oleic acid, 8 g of cerium oxide, 5 g of boric acid, 10 g (effective concentration of 50%), and stirred to 100 ° C, stirring for 3 hours.

[0046] Step 2: When the temperature eliminates to 45 ° C or lower, the mixture was added to 1 hour, and the translucent substance was obtained, that is, a lubricating oil composition.

[0047] It is weighed with 50 g of the lubricant composition, ishylacetinate 750 g, and the polymethyl methacrylate 200 g is mixed at 60 ° C.

[0048] Method for preparing lycoool esters of polymethyl methacrylate:

[0049] Step 1: EtOAc EtOAc The pressure discharge moisture, that is, is a nichanol ester of methacrylate;

[0050] Step 2, the initiator tert-butyl hydrazine hydrazine is added to the reactor, and the reaction temperature is 100 ° C, and the polymerization reaction is 8 hours, and the polymer in the reaction kettle is discharged, and the temperature filtrate removal of temperature above 80 ° C. That is, the polymethyl met...

Embodiment 3

[0052] Step 1: Take 100 g of oleic acid, 9 g of lanthanum oxide, 6 g of boric acid, 8 g (effective concentration of 50%) together with stirring, stirring to 110 ° C, and reacted for 2.5 hours.

[0053]Step 2: When the temperature eliminates to 45 ° C or lower, the addition of diethyl ethanol 6g was stirred for 1.5 hours, and the translucent material was obtained, that is, a lubricating oil composition.

[0054] It is weighed with 60 g of the lubricating oil composition, ispulcate 790 g, and the polymethyl methacrylate 150g is mixed at 50 ° C at a temperature of 50 ° C to a trace lubricating oil.

[0055] Preparation method of polymethyl methacrylate lauryl ester:

[0056] Step 1: 86.09 g (1 mol) of methacrylic acid, 205.02 g (1.1 mol), 3 g (effective concentration of 50%), reactive at 200 ° C in the reaction temperature of 200 ° C for 4 hours; reaction pressure after reaction The moisture is discharged, that is, methacrylate, lauryl ester;

[0057] Step 2, adding the initiator cou...

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Abstract

The invention provides a lubricating oil composition, which is characterized in that it is prepared from oleic acid, rare earth oxide, boric acid, phosphoric acid, and diethylaminoethanol, and the weight-number ratio of the components is: oleic acid 100; Rare earth oxide 8‑10; boric acid 5‑8; phosphoric acid 3‑5; diethylaminoethanol 5‑8. The lubricating oil composition prepared by the invention is a boron-phosphorus-rare earth type friction modifier and antirust agent, can effectively modify the life of a tool in metal processing, and has good degradability. The present invention also provides a micro-lubricating oil containing the above-mentioned lubricating oil composition, which is characterized in that it is made of the following components in weight percentage: 5-10% of the lubricating oil composition; 70-70% of isononyl isononanoate 80%; Fatty alcohol polymethacrylate 10‑20%. The micro-quantity lubricating oil prepared by the invention can meet the lubricating cooling, extreme-pressure anti-wear and anti-rust requirements of metal processing; when used in conjunction with a micro-quantity lubrication device, the amount of lubricant used can be saved by more than 95%, and the effect of energy saving, emission reduction and environmental protection is remarkable.

Description

Technical field [0001] The invention belongs to the field of lubrication, and in particular, to a lubricating oil composition and a preparation method thereof and a micro-lubricating oil prepared by the combination. Background technique [0002] Traditional metal cutting processes a large amount of flip lubrication using mineral oil or vegetable oil or cutting fluid, and the amount of use of lubricants is large, not only a waste of resources, causing huge pollution of processing places and the environment, but also seriously affects the health of operators. . [0003] In order to solve these problems, the recent research on trace lubrication techniques has made certain progress, and the micro lubrication technology solves the problem of large use of the above lubricant and severe contamination, and in order to make the use of the micro lubricant with a relatively strong extreme pressure resistance Sexual and lubricity, excessive use contains sulfur-containing and chlorine-contain...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10M169/04C10N30/06C10N30/12C10N40/22
CPCC10M169/04C10M2201/062C10M2201/087C10M2201/085C10M2207/126C10M2207/2815C10M2209/0845C10M2215/042C10N2030/12C10N2030/64C10N2030/06C10N2040/22
Inventor 张乃庆吴启东吴悠蒋宁丁金波刘志强陈洪振
Owner SHANGHAI JINZHAO ENERGY SAVING TECH
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