Self-lubricating high-strength nylon plate preparation method
A self-lubricating, high-strength technology, applied in the field of self-lubricating high-strength nylon sheet preparation, can solve problems such as poor heat resistance, increased factory production costs, low mechanical strength, low hardness, etc., achieve smooth and straight interface, and reduce frictional resistance Effect
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Embodiment 1
[0030] The catalyst is: sodium hydroxide
[0031] The activator is: toluene diisocyanate
[0032] Preparation of self-lubricating capsules:
[0033] Add 20g of urea and 70mL of formaldehyde solution with a mass fraction of 35% into the Erlenmeyer flask, stir until the urea is completely dissolved, then use triethanolamine to adjust the pH of the reaction system in the Erlenmeyer flask to 8, put the Erlenmeyer flask into a water bath, Heating to 70°C, keeping it warm for 40 minutes to obtain a viscous transparent liquid, after cooling to room temperature, adjusting the pH to 6.8 with 10% hydrochloric acid to obtain a urea-formaldehyde prepolymer for later use;
[0034] Mix the fluorocarbon resin masterbatch and the E-51 type epoxy resin masterbatch at a mass ratio of 3:2 to obtain an oil-soluble capsule core, and add 100mL of dodecylbenzenesulfonate with a mass fraction of 3% to the four-necked flask Sodium acid solution, 40g oil-soluble capsule core and 0.5mL n-butanol, star...
Embodiment 2
[0041] Catalyst: Potassium Hydroxide
[0042] The activator is: hexamethylene diisocyanate
[0043] Preparation of self-lubricating capsules:
[0044] Add 25g of urea and 72mL of formaldehyde solution with a mass fraction of 35% into the Erlenmeyer flask, stir until the urea is completely dissolved, then use triethanolamine to adjust the pH of the reaction system in the Erlenmeyer flask to 8, put the Erlenmeyer flask into a water bath, Heating to 75°C, keeping it warm for 45 minutes to obtain a viscous transparent liquid, after cooling to room temperature, adjusting the pH to 6.9 with 10% hydrochloric acid to obtain a urea-formaldehyde prepolymer, which is ready for use;
[0045] Mix the fluorocarbon resin masterbatch and the E-51 epoxy resin masterbatch at a mass ratio of 3:2 to obtain an oil-soluble capsule core, and add 110mL of dodecylbenzenesulfonate with a mass fraction of 3% to the four-necked flask Sodium acid solution, 42g oil-soluble capsule core and 0.7mL n-butano...
Embodiment 3
[0052] The catalyst is: sodium carbonate
[0053] The activator is: caprolactam-terminated diisocyanate
[0054] Preparation of self-lubricating capsules:
[0055] Add 30g of urea and 75mL of formaldehyde solution with a mass fraction of 35% into the Erlenmeyer flask, stir until the urea is completely dissolved, then use triethanolamine to adjust the pH of the reaction system in the Erlenmeyer flask to 9, put the Erlenmeyer flask into a water bath, Heating to 80°C, keeping it warm for 50 minutes to obtain a viscous transparent liquid, after cooling to room temperature, adjusting the pH to 7.0 with 10% hydrochloric acid to obtain a urea-formaldehyde prepolymer for later use;
[0056] Mix the fluorocarbon resin masterbatch and the E-51 type epoxy resin masterbatch at a mass ratio of 3:2 to obtain an oil-soluble capsule core, and add 120mL of dodecylbenzenesulfonate with a mass fraction of 3% to the four-necked flask Sodium acid solution, 45g oil-soluble capsule core and 1.0mL ...
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