Method for preparing heating membrane for heat supply
A heating film and heating technology, applied in electric heating devices, ohmic resistance heating, electrical components, etc., can solve the problems of low electrothermal conversion rate, high temperature brittleness of heating film, low heating efficiency, etc., to improve insulation performance and high temperature strength. , The effect of enhancing surface elasticity and improving heating efficiency
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Embodiment 1
[0029] Preparation of ceramic powder:
[0030]In parts by weight, add 70 parts of butyl titanate into a beaker containing 200 parts of ethylene glycol solution with a mass fraction of 25%, heat up to 80°C, add 40 parts of citric acid into the beaker, start the stirrer, Stir and disperse at a speed of 300r / min until the citric acid is completely dissolved to obtain a titanium dioxide precursor glue;
[0031] In parts by weight, 20 parts of neodymium oxide and 30 parts of lanthanum oxide are dissolved in 200 parts of nitric acid solution with a mass fraction of 30%, and 70 parts of the above-mentioned titanium dioxide precursor glue, 4 parts of calcium carbonate, and 6 parts of lithium carbonate are added , 40 parts of zirconia were mixed and placed in a water bath, heated to 80°C, kept for 2h, continued to heat up to 130°C, kept for 1h, to obtain a viscous complex;
[0032] Put the above-mentioned viscous complex into a coking furnace, feed in nitrogen, heat up to 230°C, heat-...
Embodiment 2
[0040] Preparation of ceramic powder:
[0041] In parts by weight, 75 parts of butyl titanate were added to a beaker containing 210 parts of ethylene glycol solution with a mass fraction of 25%, heated to 90°C, 42 parts of citric acid were added to the beaker, and the stirrer was started. Stir and disperse at a speed of 320r / min until the citric acid is completely dissolved to obtain a titanium dioxide precursor glue;
[0042] In parts by weight, 22 parts of neodymium oxide and 32 parts of lanthanum oxide are dissolved in 220 parts of nitric acid solution with a mass fraction of 30%, and 75 parts of the above-mentioned titanium dioxide precursor glue, 4 parts of calcium carbonate, and 6 parts of lithium carbonate are added , 45 parts of zirconia were mixed and placed in a water bath, heated to 82°C, kept for 2.5h, continued to heat up to 140°C, kept for 1.5h, to obtain a viscous complex;
[0043] Put the above-mentioned viscous complex into a coking furnace, feed nitrogen, he...
Embodiment 3
[0051] Preparation of ceramic powder:
[0052] In parts by weight, add 80 parts of butyl titanate into a beaker containing 220 parts of ethylene glycol solution with a mass fraction of 25%, heat up to 100°C, add 45 parts of citric acid into the beaker, and start the stirrer. Stir and disperse at a speed of 350r / min until the citric acid is completely dissolved to obtain a titanium dioxide precursor glue;
[0053] In parts by weight, 25 parts of neodymium oxide and 35 parts of lanthanum oxide are dissolved in 250 parts of nitric acid solution with a mass fraction of 30%, and 80 parts of the above-mentioned titanium dioxide precursor glue, 5 parts of calcium carbonate, and 7 parts of lithium carbonate are added , 50 parts of zirconia were mixed and placed in a water bath, heated to 85°C, kept for 3h, continued to heat up to 150°C, kept for 2h, to obtain a viscous complex;
[0054] Put the above-mentioned viscous complex into a coking furnace, feed in nitrogen, heat up to 250°C,...
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