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Preparation method of reactive dye dyeing accelerating functional agent

A technology of reactive dyes and functional agents, applied in the textile field, can solve problems such as different dyeing amounts, natural environmental hazards, and destruction of ecological balance, and achieve the effects of improving anti-wrinkle performance, improving color fastness, and high washing fastness

Inactive Publication Date: 2020-03-27
SUZHOU INST OF TRADE & COMMERCE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Due to the different components of different fabrics and the different structures of different components, the dyeing amount of dyes is also different, and it is easy to cause color difference when dyeing, especially when the color is light, the color difference is more serious. The traditional improvement method is to prolong the dyeing time. A large amount of leveling agent, together with auxiliary processes such as padding to enhance the dyeing effect, requires a large amount of neutral inorganic salts in the dyeing process of reactive dyes to improve the dyeing rate and fixation rate of dyes, because inorganic salts are easy to Pollution of water sources leads to salinization of water and land, which destroys the ecological balance and causes great harm to the natural environment, and the soluble salt in sewage is difficult to deal with
[0003] As the country's requirements for environmental protection and energy conservation and emission reduction in various industries are getting higher and higher, the traditional dyeing process with high energy consumption, water consumption and high pollution can no longer meet the requirements of the modern textile industry.

Method used

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  • Preparation method of reactive dye dyeing accelerating functional agent

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A preparation method of a dyeing accelerator functional agent for reactive dyes, comprising the following steps:

[0020] (1) Add porous silica powder into an aqueous solution containing 7% polyvinylpyrrolidone and 6% polyethylene glycol at a mass ratio of 1:30, stir at room temperature for 15 minutes, and then place it on an ultrasonic instrument for ultrasonic dispersion for 7 minutes to obtain Porous silicon micropowder dispersion; slowly add an acid solution to it under stirring conditions to make the pH of the solution 4.0, slowly raise the temperature to 42°C, keep stirring at this temperature for 1.5h; obtain a filter cake by ultrafiltration, and rinse it with an aqueous solution Washing several times, so that the final eluent is neutral; the obtained filter cake is placed in an oven to dry, and ground and sieved for later use;

[0021] (2) Put 30 parts of the porous silicon micropowder prepared in step (1) into a three-necked flask, add 20 parts of isopropanol s...

Embodiment 2

[0028] A preparation method of a dyeing accelerator functional agent for reactive dyes, comprising the following steps:

[0029] (1) Add porous silica powder into an aqueous solution containing 5% polyvinylpyrrolidone and 4% polyethylene glycol at a mass ratio of 1:20, stir at room temperature for 10 minutes, and then place it on an ultrasonic instrument for ultrasonic dispersion for 5 minutes to obtain Porous silicon micropowder dispersion; slowly add acid solution to it under stirring conditions to make the solution pH 3.0, slowly raise the temperature to 35°C, keep stirring at this temperature for 1 hour; obtain filter cake by ultrafiltration, and rinse it with aqueous solution Multiple times, so that the final eluent is neutral; the obtained filter cake is placed in an oven to dry, and ground and sieved for later use;

[0030] (2) Put 20 parts of the porous silicon micropowder prepared in step (1) into a three-necked flask, add 10 parts of isopropanol solution, and slowly ...

Embodiment 3

[0037] A preparation method of a dyeing accelerator functional agent for reactive dyes, comprising the following steps:

[0038] (1) Add porous silica powder into an aqueous solution containing 6% polyvinylpyrrolidone and 5% polyethylene glycol at a mass ratio of 1:25, stir at room temperature for 12 minutes, and then place it on an ultrasonic instrument for ultrasonic dispersion for 6 minutes to obtain Porous silicon micropowder dispersion; slowly add an acid solution to it under stirring conditions to make the solution pH 3.5, slowly raise the temperature to 40°C, keep stirring at this temperature for 1.2h; obtain a filter cake by ultrafiltration, and rinse it with an aqueous solution Washing several times, so that the final eluent is neutral; the obtained filter cake is placed in an oven to dry, and ground and sieved for later use;

[0039] (2) Put 25 parts of the porous silicon micropowder prepared in step (1) into a three-necked flask, add 15 parts of isopropanol solution...

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Abstract

The invention provides a preparation method of a reactive dye dyeing accelerating functional agent. The preparation method comprises the following steps of (1) treating porous silicon micropowder by an acid solution; (2) modifying the porous silicon micropowder prepared in the step (1) by 2,3-epoxypropyltrimethylammonium chloride to obtain modified porous silicon micropowder; (3) mixing the modified micropowder prepared in the step (2), trifluoroacetic acid, sodium alginate, sodium polyacrylate, polyacrylamide, sodium hexametaphosphate, guar gum, ethylene glycol dimethyl ether, an emulsifier and water; and performing heating and stirring, and dispersion by a high-speed dispersing machine to obtain the dyeing accelerating functional agent. The dyeing accelerating functional agent prepared by the method plays an important role in the dyeing process of reactive dyes; the dye uptake of the dyes is improved; the color depth of the dyed fabric is increased; the dyed fabric has high washing fastness; and the fixation performance of the dye is good, so that the reactive dye dyeing accelerating functional agent prepared by the preparation method has an important application value in the textile field.

Description

technical field [0001] The invention belongs to the technical field of textiles, and in particular relates to a preparation method of a reactive dye dyeing accelerator functional agent. Background technique [0002] Due to the different components of different fabrics and the different structures of different components, the dyeing amount of dyes is also different, and it is easy to cause color difference when dyeing, especially when the color is light, the color difference is more serious. The traditional improvement method is to prolong the dyeing time. A large amount of leveling agent, together with auxiliary processes such as padding to enhance the dyeing effect, requires a large amount of neutral inorganic salts in the dyeing process of reactive dyes to improve the dyeing rate and fixation rate of dyes, because inorganic salts are easy to Water sources are polluted, water salinization and land salinization destroy the ecological balance, causing great harm to the natura...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/38D06P1/673D06P1/52D06P1/48D06P1/66
CPCD06P1/38D06P1/48D06P1/5257D06P1/66D06P1/67383
Inventor 杭伟明
Owner SUZHOU INST OF TRADE & COMMERCE