Preparation method of reactive dye dyeing accelerating functional agent
A technology of reactive dyes and functional agents, applied in the textile field, can solve problems such as different dyeing amounts, natural environmental hazards, and destruction of ecological balance, and achieve the effects of improving anti-wrinkle performance, improving color fastness, and high washing fastness
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0019] A preparation method of a dyeing accelerator functional agent for reactive dyes, comprising the following steps:
[0020] (1) Add porous silica powder into an aqueous solution containing 7% polyvinylpyrrolidone and 6% polyethylene glycol at a mass ratio of 1:30, stir at room temperature for 15 minutes, and then place it on an ultrasonic instrument for ultrasonic dispersion for 7 minutes to obtain Porous silicon micropowder dispersion; slowly add an acid solution to it under stirring conditions to make the pH of the solution 4.0, slowly raise the temperature to 42°C, keep stirring at this temperature for 1.5h; obtain a filter cake by ultrafiltration, and rinse it with an aqueous solution Washing several times, so that the final eluent is neutral; the obtained filter cake is placed in an oven to dry, and ground and sieved for later use;
[0021] (2) Put 30 parts of the porous silicon micropowder prepared in step (1) into a three-necked flask, add 20 parts of isopropanol s...
Embodiment 2
[0028] A preparation method of a dyeing accelerator functional agent for reactive dyes, comprising the following steps:
[0029] (1) Add porous silica powder into an aqueous solution containing 5% polyvinylpyrrolidone and 4% polyethylene glycol at a mass ratio of 1:20, stir at room temperature for 10 minutes, and then place it on an ultrasonic instrument for ultrasonic dispersion for 5 minutes to obtain Porous silicon micropowder dispersion; slowly add acid solution to it under stirring conditions to make the solution pH 3.0, slowly raise the temperature to 35°C, keep stirring at this temperature for 1 hour; obtain filter cake by ultrafiltration, and rinse it with aqueous solution Multiple times, so that the final eluent is neutral; the obtained filter cake is placed in an oven to dry, and ground and sieved for later use;
[0030] (2) Put 20 parts of the porous silicon micropowder prepared in step (1) into a three-necked flask, add 10 parts of isopropanol solution, and slowly ...
Embodiment 3
[0037] A preparation method of a dyeing accelerator functional agent for reactive dyes, comprising the following steps:
[0038] (1) Add porous silica powder into an aqueous solution containing 6% polyvinylpyrrolidone and 5% polyethylene glycol at a mass ratio of 1:25, stir at room temperature for 12 minutes, and then place it on an ultrasonic instrument for ultrasonic dispersion for 6 minutes to obtain Porous silicon micropowder dispersion; slowly add an acid solution to it under stirring conditions to make the solution pH 3.5, slowly raise the temperature to 40°C, keep stirring at this temperature for 1.2h; obtain a filter cake by ultrafiltration, and rinse it with an aqueous solution Washing several times, so that the final eluent is neutral; the obtained filter cake is placed in an oven to dry, and ground and sieved for later use;
[0039] (2) Put 25 parts of the porous silicon micropowder prepared in step (1) into a three-necked flask, add 15 parts of isopropanol solution...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More 
