Water-based cutting fluid and preparation method thereof
A cutting fluid, water-based technology, applied in the petroleum industry, additives, lubricating compositions, etc., can solve the problems of water pollution, poor biodegradability, high cost, high lubricity, anti-rust ability, and good biodegradability , the effect of reducing the mass content
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Embodiment 1
[0037] Take 100g of commercial tungoleic acid (purchased from Anhui Ruifengde Oil Deep Processing Co., Ltd., model: T160) into a 250mL four-neck flask, add 0.5g of tert-butylhydroquinone at the same time, purging with nitrogen for 30min, stirring at 300rpm, Raise the temperature to 220° C. for 4 h, stop heating, and cool to room temperature in ice water to obtain a crude product of dimer acid. The molecular distillation instrument controls the temperature at 150°C and the pressure ≤ 2Pa to collect the heavy component product; the heavy component product is distilled again, and the molecular distillation instrument is controlled to control the temperature at 250°C and the pressure ≤ 2Pa, and the outflowing light component is tung oil dimer acid, distillate Polyacid content ≥ 98%.
[0038]First, mix 4 parts of tung oil dimer acid and 1 part of triethanolamine, heat up to 110°C to react, stir until dissolved and transparent, and place it at room temperature, then add 2 parts of N...
Embodiment 2
[0040] Take 100g of commercial tungoleic acid (purchased from Anhui Ruifengde Oil Deep Processing Co., Ltd., model: T160) into a 250mL four-neck flask, add 0.5g of tert-butylhydroquinone at the same time, purging with nitrogen for 30min, stirring at 300rpm, Raise the temperature to 220° C. for 4 h, stop heating, and cool to room temperature in ice water to obtain a crude product of dimer acid. The molecular distillation instrument controls the temperature at 150°C and the pressure ≤ 2Pa to collect the heavy component product; the heavy component product is distilled again, and the molecular distillation instrument is controlled to control the temperature at 250°C and the pressure ≤ 2Pa, and the outflowing light component is tung oil dimer acid, distillate Polyacid content ≥ 98%.
[0041] First, mix 8 parts of tung oil dimer acid and 3 parts of triethanolamine, heat up to 130°C for reaction, stir until dissolved and transparent, place it at room temperature, then add 2.3 parts ...
Embodiment 3
[0043] Take 100g of commercial tungoleic acid (purchased from Anhui Ruifengde Oil Deep Processing Co., Ltd., model: T160) into a 250mL four-neck flask, add 0.5g of tert-butylhydroquinone at the same time, purging with nitrogen for 30min, stirring at 300rpm, Raise the temperature to 220° C. for 4 h, stop heating, and cool to room temperature in ice water to obtain a crude product of dimer acid. The molecular distillation instrument controls the temperature at 150°C and the pressure ≤ 2Pa to collect the heavy component product; the heavy component product is distilled again, and the molecular distillation instrument is controlled to control the temperature at 250°C and the pressure ≤ 2Pa, and the outflowing light component is tung oil dimer acid, distillate Polyacid content ≥ 98%.
[0044] First, mix 2 parts of tung oil dimer acid and 3 parts of triethanolamine, heat up to 120°C for reaction, stir until dissolved and transparent, place it at room temperature, then add 3 parts of...
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