Burdock polyphenol-loaded aquatic product coating fresh-keeping liquid as well as preparation method and use method thereof
A technology for coating fresh-keeping and aquatic products, which is applied in the fields of food preservation, preservation of meat/fish with a coating protective layer, preservation of food ingredients as anti-microbials, etc. Good, long-lasting antioxidant effect
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[0039] The schematic block diagram of the overall technical route of the present invention is as figure 1 Shown, the present invention carries the preparation method of the aquatic product coating fresh-keeping liquid of burdock polyphenol, comprises the steps:
[0040] Step 1: preparing burdock polyphenols,
[0041] Step 1.1: Slice the fresh burdock root and put it in boiling water for 10-15s, then take it out and drain the water,
[0042] Step 1.2: Place the drained burdock root slices in an oven at 40-50°C to dry,
[0043] Step 1.3: After the dried burdock root slices are pulverized, 40 mesh sieves are obtained to obtain burdock root powder.
[0044] Step 1.4: Mix burdock root powder and ethanol with a volume fraction of 40-60% according to a ratio of 1:(10-30)(g / mL) to obtain a mixed solution, and reflux the mixed solution at 50-60°C Extract 2-3h to the end of reflux,
[0045] Step 1.5: freeze-dry the mixed solution under negative pressure to remove the organic solvent...
Embodiment 1
[0062] Step 1: Preparation of Burdock Polyphenols
[0063] Take fresh burdock root slices, blanching them in boiling water for 15 seconds, drain the water after taking them out; oven-dry the burdock root slices at 45°C, crush them with a tissue grinder, and pass them through a 40-mesh sieve for later use; : a solid-liquid ratio of 20 (g / mL) is mixed with an ethanol solution with a volume fraction of 50%, and extracted under reflux for 3 hours at 55° C.; after removing the organic solvent under reduced pressure, lyophilize in a freeze dryer to obtain burdock polyphenols;
[0064] Step 2: Preparation of burdock polyphenol nanostructured lipid carrier
[0065] Weigh 5% glyceryl tristearate and 5% medium-chain triglycerides and mix them, heat at 90°C to make the complex lipids in a molten state, add 0.10% burdock polyphenols, and dissolve them in the complex lipids Medium; 5% Tween 20 was completely dissolved in the water phase (accounting for 84.90% of the total mass of the syst...
Embodiment 2
[0071] Step 1: Preparation of Burdock Polyphenols
[0072] Take fresh burdock root slices, blanching them in boiling water for 15 seconds, take them out and drain the water; dry the burdock root slices in an oven at 50°C, grind them with a tissue grinder, and pass them through a 40-mesh sieve for later use; : a solid-liquid ratio of 10 (g / mL) is mixed with ethanol with a volume fraction of 60%, reflux extraction at 60° C. for 2 h; after removing the organic solvent under reduced pressure, lyophilize in a freeze dryer to obtain burdock polyphenols;
[0073] Step 2: Preparation of burdock polyphenol nanostructured lipid carrier
[0074] Weigh 10% glyceryl behenate and 5% oleic acid and mix them, heat at 90°C to make the complex lipids in a molten state, add 0.15% burdock polyphenols to dissolve them in the complex lipids; 7% Tween 80 was completely dissolved in the water phase (accounting for 77.85% of the total mass of the system), and preheated at 90°C; the water phase was ad...
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