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A silicone sealant with a temperature resistance of 500°C and its preparation and use method

A technology of sealing glue and silicone, applied in the field of sealing glue, can solve the problems that affect the production progress and military needs, cannot guarantee the production demand, and purchase difficulties, etc., and achieve the effects of good application, foreign exchange saving, and feasible process

Active Publication Date: 2022-04-22
SHENYANG LIMING AERO-ENGINE GROUP CORPORATION
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The sealing glue involved in the present invention is mainly aimed at the special purpose of the engine. It is a necessary material for engine overhaul. It is an imported material: there is no ready-made technical standard, and due to the short storage period, it brings certain difficulties for procurement and cannot guarantee production. Requirements; In an aero-engine, there is always a gap between the joint surfaces of its parts. In order to ensure the normal operation of the engine and maintain the normal operating pressure and safety of the system, the joint surface must be sealed to prevent oil leakage, air leakage, Water leakage, etc., the sealant is mainly used for parts where the sealing gap is very small, such as the joint surface of the engine combustion chamber casing installation side and the high-pressure turbine guide inner installation side (including the adjustment ring), the joint surface of the high-conductivity inner ring and the swirler (including sealing components), the joint surface of the heat exchanger shell and the heat exchange element, the joint surface of the pneumatic actuator shell and the joint, the oil leakage valve with adjustable nozzle (shell, gasket, valve), the final assembly Transferred thermocouples, nozzles, pressure sensors and other parts; imported sealants are used in the existing technology, and imported materials take time to order, produce, and customs, and will be damaged to varying degrees due to temperature differences and uncontrollable factors. Affect the production schedule and military needs; and the colloid is a fluid, there are hidden dangers in the transportation process

Method used

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  • A silicone sealant with a temperature resistance of 500°C and its preparation and use method
  • A silicone sealant with a temperature resistance of 500°C and its preparation and use method
  • A silicone sealant with a temperature resistance of 500°C and its preparation and use method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] (1) Preparation of hydrolyzed ethyl silicate silicon-40

[0057] Measure 66ml of ethyl silicate-40 and mix it with 35ml of hydrolyzed alcohol; then measure 0.92ml of hydrochloric acid and dissolve it in the remaining 35ml of hydrolyzed alcohol, and add it to the remaining 34ml of ethyl silicate-40 at the same time; The mixed solution is mixed together again, and the hydrolyzed ethyl silicate 40 is obtained after stirring evenly.

[0058] (2) Preparation of silicone sealant

[0059] After preparing hydrolyzed ethyl silicate silicon 40, taking 100g as an example, weigh:

[0060] Epoxy silicone heat-resistant paint H61-1 component 1: 64.5g

[0061] Hydrolyzed ethyl silicate silicon-40: 9g

[0062] Talc powder: 6.4g

[0063] Fumed silica: 0.7g

[0064] Epoxy silicone heat-resistant paint H61-1 component three: 13g

[0065] Epoxy paint thinner X—7: 6g;

[0066] (3) Take component one of epoxy silicone heat-resistant paint H61-1, after thickening treatment, add it to c...

Embodiment 2

[0073] (1) Preparation of hydrolyzed ethyl silicate silicon-40

[0074] Measure 66ml of ethyl silicate-40 and mix it with 35ml of hydrolyzed alcohol; then measure 0.92ml of hydrochloric acid and dissolve it in the remaining 35ml of hydrolyzed alcohol, and add it to the remaining 34ml of ethyl silicate-40 at the same time; The mixed solution is mixed together again, and the hydrolyzed ethyl silicate 40 is obtained after stirring evenly.

[0075] (2) Preparation of silicone sealant

[0076] After preparing hydrolyzed ethyl silicate silicon-40, taking 100g as an example, weigh:

[0077] Epoxy silicone heat-resistant paint H61-1 component 1: 69g

[0078] Hydrolyzed ethyl silicate silicon-40: 11g

[0079] Talc powder: 6.8g

[0080] Fumed silica: 0.9g

[0081] Epoxy silicone heat-resistant paint H61-1 component three: 16g

[0082] Epoxy paint thinner X—7:6.4g

[0083] Steps (3)-(5) are the same as in Example 1 to prepare silicone sealant.

[0084] The prepared silicone seala...

Embodiment 3

[0088] (1) Preparation of hydrolyzed ethyl silicate silicon-40

[0089] Measure 66ml of ethyl silicate-40 and mix it with 35ml of hydrolyzed alcohol; then measure 0.92ml of hydrochloric acid and dissolve it in the remaining 35ml of hydrolyzed alcohol, and add it to the remaining 34ml of ethyl silicate-40 at the same time; The mixed solution is mixed together again, and the hydrolyzed ethyl silicate 40 is obtained after stirring evenly.

[0090] (2) Preparation of silicone sealant

[0091] After preparing hydrolyzed ethyl silicate silicon-40, taking 100g as an example, weigh:

[0092] Epoxy silicone heat-resistant paint H61-1 component 1: 60g

[0093] Hydrolyzed ethyl silicate silicon-40: 7g

[0094] Talc powder: 6.0g

[0095] Fumed silica: 0.5g

[0096] Epoxy silicone heat-resistant paint H61-1 component three: 10g

[0097] Epoxy paint thinner X—7:5g

[0098] Steps (3)-(5) are the same as in Example 1 to prepare silicone sealant.

[0099] The prepared silicone sealant ...

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Abstract

A silicone sealant with a temperature resistance of 500°C of the present invention and its preparation and use method, the sealant includes epoxy silicone resin, hydrolyzed ethyl silicate-40, filler, pigment and diluent agent. During preparation, after the hydrolyzed ethyl silicate 40 is prepared, the epoxy silicone resin is thickened, the pigment is added to form a B1 mixed liquid; the hydrolyzed ethyl silicate 40 is added to form a B2 mixed liquid; the filler is dissolved in the X-7 ring Oxygen paint thinner, form B3 mixed liquid; after mixing B2 and B3 mixed solution, vibrate to form silicone sealant. When using the sealant, wipe and wait for the bonding surface to dry, adjust the viscosity of the sealant, apply it evenly, assemble the parts, and assemble after curing. The sealant prepared by the method of the present invention fully meets the design requirements for the sealability of engine-related parts through assessment tests on material appearance, dryness, heat resistance, sealing performance, corrosion, and sealing effect of typical engine parts.

Description

Technical field: [0001] The invention belongs to the technical field, and in particular relates to a sealant, in particular to a silicone sealant with a temperature resistance of 500°C and a preparation and use method thereof. Background technique: [0002] The sealing glue involved in the present invention is mainly aimed at the special purpose of the engine. It is a necessary material for engine overhaul. It is an imported material: there is no ready-made technical standard, and due to the short storage period, it brings certain difficulties for procurement and cannot guarantee production. Requirements; In an aero-engine, there is always a gap between the joint surfaces of its parts. In order to ensure the normal operation of the engine and maintain the normal operating pressure and safety of the system, the joint surface must be sealed to prevent oil leakage, air leakage, Water leakage, etc., the sealant is mainly used for parts where the sealing gap is very small, such a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09J183/06C09J11/04C09J5/02
CPCC09J183/06C09J11/04C09J5/02C08K7/26C08K3/34C08K3/36
Inventor 王杰徐琪刘翔邢彬张丽娜
Owner SHENYANG LIMING AERO-ENGINE GROUP CORPORATION