A silicone sealant with a temperature resistance of 500°C and its preparation and use method
A technology of sealing glue and silicone, applied in the field of sealing glue, can solve the problems that affect the production progress and military needs, cannot guarantee the production demand, and purchase difficulties, etc., and achieve the effects of good application, foreign exchange saving, and feasible process
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Embodiment 1
[0056] (1) Preparation of hydrolyzed ethyl silicate silicon-40
[0057] Measure 66ml of ethyl silicate-40 and mix it with 35ml of hydrolyzed alcohol; then measure 0.92ml of hydrochloric acid and dissolve it in the remaining 35ml of hydrolyzed alcohol, and add it to the remaining 34ml of ethyl silicate-40 at the same time; The mixed solution is mixed together again, and the hydrolyzed ethyl silicate 40 is obtained after stirring evenly.
[0058] (2) Preparation of silicone sealant
[0059] After preparing hydrolyzed ethyl silicate silicon 40, taking 100g as an example, weigh:
[0060] Epoxy silicone heat-resistant paint H61-1 component 1: 64.5g
[0061] Hydrolyzed ethyl silicate silicon-40: 9g
[0063] Fumed silica: 0.7g
[0064] Epoxy silicone heat-resistant paint H61-1 component three: 13g
[0065] Epoxy paint thinner X—7: 6g;
[0066] (3) Take component one of epoxy silicone heat-resistant paint H61-1, after thickening treatment, add it to c...
Embodiment 2
[0073] (1) Preparation of hydrolyzed ethyl silicate silicon-40
[0074] Measure 66ml of ethyl silicate-40 and mix it with 35ml of hydrolyzed alcohol; then measure 0.92ml of hydrochloric acid and dissolve it in the remaining 35ml of hydrolyzed alcohol, and add it to the remaining 34ml of ethyl silicate-40 at the same time; The mixed solution is mixed together again, and the hydrolyzed ethyl silicate 40 is obtained after stirring evenly.
[0075] (2) Preparation of silicone sealant
[0076] After preparing hydrolyzed ethyl silicate silicon-40, taking 100g as an example, weigh:
[0077] Epoxy silicone heat-resistant paint H61-1 component 1: 69g
[0078] Hydrolyzed ethyl silicate silicon-40: 11g
[0080] Fumed silica: 0.9g
[0081] Epoxy silicone heat-resistant paint H61-1 component three: 16g
[0082] Epoxy paint thinner X—7:6.4g
[0083] Steps (3)-(5) are the same as in Example 1 to prepare silicone sealant.
[0084] The prepared silicone seala...
Embodiment 3
[0088] (1) Preparation of hydrolyzed ethyl silicate silicon-40
[0089] Measure 66ml of ethyl silicate-40 and mix it with 35ml of hydrolyzed alcohol; then measure 0.92ml of hydrochloric acid and dissolve it in the remaining 35ml of hydrolyzed alcohol, and add it to the remaining 34ml of ethyl silicate-40 at the same time; The mixed solution is mixed together again, and the hydrolyzed ethyl silicate 40 is obtained after stirring evenly.
[0090] (2) Preparation of silicone sealant
[0091] After preparing hydrolyzed ethyl silicate silicon-40, taking 100g as an example, weigh:
[0092] Epoxy silicone heat-resistant paint H61-1 component 1: 60g
[0093] Hydrolyzed ethyl silicate silicon-40: 7g
[0095] Fumed silica: 0.5g
[0096] Epoxy silicone heat-resistant paint H61-1 component three: 10g
[0097] Epoxy paint thinner X—7:5g
[0098] Steps (3)-(5) are the same as in Example 1 to prepare silicone sealant.
[0099] The prepared silicone sealant ...
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